An official website of the United States government
Here’s how you know
Official websites use .gov
A .gov website belongs to an official government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you’ve safely connected to the .gov website. Share sensitive information only on official, secure websites.
Jing Qin, Richard M. Silver, Bryan M. Barnes, Hui Zhou, Francois R. Goasmat
There has been much recent work in developing advanced optical metrology methods that use imaging optics for critical dimension measurements and defect detection. Sensitivity to nanometer scale changes has been observed when measuring critical dimensions
Thao M. Nguyen, Julien C. Gigault, Vincent A. Hackley
The development of highly efficient asymmetric-flow field flow fractionation (A4F) methodology for biocompatible PEGylated gold nanorods (GNR) without the need for surfactants in the mobile phase is presented. We report on the potential of A4F for rapid
Gheorghe Stan, Sean King, Jeff Bielefeld, Gaunghai Xu, William Lanford, Yusuke Matsuda, Reinhold Dauskardt, Jonathan F. Stebbins, Donald Hondongwa, Lauren Olasov, Brian Daly, Ming Liu, Dhanadeep Dutta, David W. Gidley
As demand for lower power and higher performance nano-electronic products increases, the semiconductor industry must adopt insulating materials with progressively lower dielectric constants (i.e. low-k) in order to minimize capacitive related power losses
De-Hao D. Tsai, Frank W. DelRio, John M. Pettibone, Pin A. Lin, Jiaojie Tan, Michael R. Zachariah, Vincent A. Hackley
In this study, an electrospray-differential mobility analyzer (ES-DMA) was operated with an aerosol flow-mode, temperature-programmed approach to enhance its ability to characterize the particle size distributions (PSDs) of nanoscale particles (NPs) in the
The TSOM method provides three-dimensional nanoscale metrology using a conventional optical microscope. Substantial improvements in defect detectability using the TSOM method will be presented. The TSOM method shows potential to (i) detect phase defects on
Recently, an AFM-based approach for quantifying the number of biological molecules conjugated to a nanoparticle surface at low number densities was reported. By using antibody-mediated self-limiting self-assembly to decorate the analyte nanoparticles with
Joseph A. Stroscio, Jeonghoon Ha, Niv Levy, Young Kuk, Tong Zhang
We studied the response of the surface state spectrum of epitaxial Sb2Te3 thin films to applied gate electric fields by low temperature scanning tunneling microscopy. The gate dependence of the shift in the Fermi level and screening effect from bulk
Brenton J. Knuffman, Adam V. Steele, Jabez J. McClelland
We report measurements and modeling performed on an ion source based on ionization of a laser-cooled atomic beam. We show a high brightness and a low energy spread, suitable for use in next-generation, high-resolution focused ion beam (FIB) systems. Our
Sanghee Cho, Stephen D. Kang, Wondong Kim, Eui-Sup Lee, Sung-Jae Woo, Ki-Jeong Kong, Ilyou Kim, Hyeong-Do Kim, Tong Zhang, Joseph A. Stroscio, Yong-Hyun Kim, Ho-Ki Lyeo
Many structural defects and strain fields develop during the preparation of thin films and nanostructures, with their origins being at the atomic level1,2. Sensitively detecting these subtle features with high sensitivity and resolution, and their
Basudev Lahiri, Glenn E. Holland, Vladimir A. Aksyuk, Andrea Centrone
The collective oscillation of conduction electrons, responsible for the LSPRs, enables engineering nanomaterials by tuning their optical response from the visible to THz as a function of nanostructure size, shape and environment. While theoretical
We present a method to improve accuracy in measurements of nanoscale viscoelastic material properties with contact resonance (CR) AFM methods. Through the use of the two-dimensional hydrodynamic function, we obtain a more precise estimate of the fluid
The field of electron microscopy, by its very diverse nature, abounds with acronyms: AEM, EF-TEM, ESEM, FE-SEM, HREM, HRTEM, HVEM, SEM, STEM, TEM, and VP-SEM, to name some instruments alone. Add in the different forms of data that these instruments might
Matthew D. Brubaker, Kristine A. Bertness, Norman A. Sanford, Brian Gorman, David R. Diercks, R Kirchofer
GaN has seen use in many applications such as photovoltaics, blue and ultraviolet lasers, and light-emitting diodes with additional research into expanded and new applications. GaN in the form of nanowires present additional possibilities due to their high
Bryan M. Barnes, Martin Y. Sohn, Francois R. Goasmat, Hui Zhou, Richard M. Silver, Abraham Arceo
Experimental imaging at =193 nm of sub-resolved defects performed at several focus positions yields a volume of spatial and intensity data. Defects are located in a differential volume, given a reference, with up to 5x increase in sensitivity.
Christopher Soles, Hyun W. Ro, Aaron Forster, Dave J. Krug, Vera Popova, Richard M. Laine
In this manuscript a series of cubic silsequioxane monomers with their eight vertices functionalized with different organic ligands terminated with triethoxysilane groups were acid hydrolyzed, spin cast into thin films, and then vitrified into hard
Heayoung Yoon, Youngmin Lee, Christopher C. Bohn, Seung H. Ko, Anthony G. Gianfrancesco, Jonathan S. Steckel, Seth Coe-Sullivan, Albert A. Talin, Nikolai B. Zhitenev
We report a fast, versatile photocurrent imaging technique to visualize the local photo response of solar energy devices and optoelectronics using near-field cathodoluminescence (CL) from a homogeneous quantum dot layer. This approach is quantitatively
Ravikiran Attota, Benjamin D. Bunday, Victor Vertanian
We present results using simulations and experiments to demonstrate metrological applications of the through-focus scanning optical microscopy (TSOM) down to features at and well below the International Technology Roadmap for Semiconductors' 22 nm node
Julian S. Taurozzi, Vincent A. Hackley, Mark R. Wiesner
Toxicity and fate assessment are key elements in the evaluation of the environmental, health and safety risks of engineered nanomaterials (ENMs). While significant effort and resources have been devoted to the toxicological evaluation of many ENMs
Julian S. Taurozzi, Vincent A. Hackley, Mark R. Wiesner
We describe a comprehensive optimization study culminating in a standardized and validated approach for the preparation of titanium dioxide (TiO2) nanoparticle dispersions in relevant biological media (PBS and DMEM-FBS). This study utilizes a candidate
Accurate characterization of nanomaterial properties is a critical component of any nanotoxicology testing strategy. Data that describes the performance of various laboratories to measure the characteristics of the same nanomaterial is scarce. We conducted
In this work we highlight the size-independent influence of the material properties of nanoparticles on their retention behavior in asymmetric-flow field-flow fractionation (A4F). The phenomena described here suggest there are limits to the effectiveness
Nikolai B. Zhitenev, Behrang H. Hamadani, Paul M. Haney
Photogenerated charge transport in bulk heterojunction (BHJ) solar cells is strongly dependent on the active layer nanomorphology. Local probes have been extensively employed to understand the correlation between 2D and 3D morphology and device efficiency
John M. Pettibone, William A. Osborn, Konrad Rykaczewski, Albert A. Talin, John E. Bonevich, Jeffrey W. Hudgens
The unique properties of metallic nanoclusters are attractive for numerous commercial and industrial applications but are generally less stable than nanocrystals. Thus, developing methodologies for stabilizing nanoclusters and retaining their enhanced
A general solution of the linear passive microwave network is presented, for the characterization of thin film materials at high microwave frequencies. The mathematical formulas that correlate scattering parameters S11 and S21 with the distributed circuit