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Using an ion source based on photoionization of laser-cooled lithium atoms, we have developed a scanning ion microscope with probe sizes of a few tens of nanometers and beam energies from 500 eV to 5 keV. These beam energies are much lower than the typical
Duming Zhang, Hongwoo H. Baek, Jeonghoon Ha, Tong Zhang, Jonathan E. Wyrick, Albert Davydov, Young Kuk, Joseph A. Stroscio
Recently, the topological classification of electronic states has been extended to a new class of matter known as topological crystalline insulators. Similar to topological insulators, topological crystalline insulators also have spin-momentum locked
Wyatt N. Vreeland, Anne A. Galyean, James J. Filliben, Richard D. Holbrook, Dean C. Ripple, Howard S. Weinberg
The development of standardized and optimized methods to characterize polydisperse nanoparticles in complex matrixes is considered a critical component in many fields. Robust, rigorously optimized methods are currently lacking, in part because of matrix
Savelas A. Rabb, Deborah S. Jacobs, Li Piin Sung, Tinh Nguyen, Lee L. Yu
The impact of nanoparticles on the environment and, more importantly, the human population has been of great interest for the past few years. Release of these nanoparticles from different materials from wear or climate exposure has been explored to aid in
Scanning Electron Microscopy (SEM) and Confocal Raman Microscopy (CRM) were employed to characterize the 3D state of disperison of carbon nanotubes (CNT) in a polymer matrix. First, non-destructive subsurface imaging on CNT-polymer was conducted by charge
We present an experimental method, based on analytical hydrodynamic theory, to accurately predict the inertial and viscous fluid loading forces at arbitrary frequencies in a contact resonance atomic force microscope system. Knowledge of the fluid loading
Karen E. Murphy, Jingyu Liu, William F. Guthrie, Justin M. Gorham, John E. Bonevich, Andrew J. Allen, Michael R. Winchester, Vincent A. Hackley, Robert MacCuspie
In this study we use inductively coupled plasma mass spectrometry operated in single particle mode (spICP-MS) to simultaneously characterize the size distribution and dissolved silver fraction of a new silver nanoparticle (AgNP) candidate reference
The intermittent contact resonance atomic force microscopy (ICR-AFM) mode proposed here is a new frequency modulation technique performed in scanning force controlled AFM modes like force volume or peak force tapping. It consists of tracking the change in
A cavity perturbation method is used to determine conductance of small volume nano-carbon materials. These are the building blocks of nanostructured materials and devices, and therefore their electrical characteristics are important in the materials
Bonghwan Chon, Kimberly Briggman, Jeeseong C. Hwang
We report on an experimental procedure in confocal single molecule fluorescence lifetime correlation spectroscopy (FLCS) to determine the range of excitation power and molecule concentration in solution under which the application of an unmodified model
C W. Teplin, Sachit Grover, Adrian Chitu, Alexander Limanov, Monical Chalal, James Im, Daniel Amkreutz, Stefan Gall, Heayoung Yoon, Vincenzo Lasalvia, H M. Branz, Paul Stradins, Kim M. Jones, Andrew G. Norman, David L. Young, Benjamin Lee
We fabricate thin epitaxial c-Si solar cells on display glass and fused silica substrates overcoated with a Si seed layer. We achieve an open circuit voltage (VOC) of 586 mV and 6.5% efficiency using a 2 µm thick absorber on a (100) monocrystalline layer
Christopher W. Szakal, Steve Roberts, Paul Westerhoff, Andrew Bartholomaeus, Neil Buck, Ian Illuminato, Richard Canady, Michael Rogers
Risks and benefits of nanomaterials related to food receive conflicting attention in news media, research, and across expert stakeholder groups internationally. Current nanomaterial analysis is complicated by broad definitions that include traditional food
In 2013 the ITRS Metrology Technical Working Group worked on updating the text and tables of the metrology chapter. New additions include a section on 3D nanometrology, a revised lithography metrology table, and an updated Interconnect section. The
Richard M. Silver, Bryan Barnes, Nien F. Zhang, Hui Zhou, Andras Vladar, John S. Villarrubia, Regis J. Kline, Daniel Sunday, Alok Vaid
There has been significant interest in hybrid metrology as a novel method for reducing overall measurement uncertainty and optimizing measurement throughput (speed) through rigorous combinations of two or more different measurement techniques into a single
Bryan M. Barnes, Francois R. Goasmat, Martin Y. Sohn, Hui Zhou, Richard M. Silver, Andras Vladar, Abraham Arceo
We have previously introduced a new data analysis method that more thoroughly utilizes scattered optical intensity data collected during defect inspection using bright-field microscopy. This volumetric approach allows conversion of focus resolved 2-D
Paul T. Blanchard, Kristine A. Bertness, Todd E. Harvey, Norman A. Sanford
Contact resistivity ρ c is an important figure of merit in evaluating and improving the performance of electronic and optoelectronic devices. Due to the small size, unique morphology, and uncertain transport properties of semiconductor nanowires (NWs)
Justin M. Gorham, Anne B. Rohlfing, Katrice A. Lippa, Robert I. MacCuspie, Amy Hemmati, Richard D. Holbrook
A critical but often overlooked component of silver nanoparticle (AgNPs) suspensions involves their behavior following short- and long-term storage. The current study investigates the integrity of citrate-capped AgNP suspensions, nominally 20 nm in
We analysed the resonance frequency, amplitude, and phase response of the first two eigenmodes of two contact-resonance atomic force microscopy (CR-AFM) configurations, differing in the method used to excite the system (cantilever base vs. sample
Andrew D. Gamalski, Peter W. Voorhees, Renu Sharma, Caterina Ducati, Stephan Hofmann
We observe a twin plane re-entrant based growth mechanism for Au catalyzed Ge nanowire growth using video-rate lattice-resolved environmental transmission electron microscopy. For a [112] growth direction, we find a convex, V-shaped liquid catalyst
Christopher W. Szakal, Melissa S. Ugelow, Justin M. Gorham, Andrew R. Konicek, Richard D. Holbrook
We demonstrate the ability to visualize nanoparticle dissolution while simultaneously providing chemical signatures that differentiate between citrate-capped silver nanoparticles (AgNPs), AgNPs forced into dissolution via exposure to UV radiation, silver
De-Hao D. Tsai, Tae Joon Cho, Frank W. DelRio, Justin Gorham, Jiwen Zheng, Jiaojie Tan, Michael R. Zachariah, Vincent A. Hackley
We report a systematic study of the controlled formation of discrete-size gold nanoparticle clusters (GNCs) by interaction with the reducing agent dithiothreitol (DTT). Asymmetric-flow field flow fractionation and electrospray differential mobility
Jingyu Liu, Karen E. Murphy, Robert I. MacCuspie, Michael R. Winchester
The increasing application of engineered nanomaterials in consumer and medical products has motivated the development of single particle inductively coupled plasma mass spectrometry (spICP-MS) for characterizing nanomaterials under realistic environmental