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Santiago D. Solares Rivera, Sang M. An, Chris Long
We present an exploratory study of multimodal tapping-mode atomic force microscopy driving more than three cantilever eigenmodes. We present tetramodal (4-eigenmode) imaging experiments conducted on a thin Teflon film and computational simulations of
Jurgen Kraus, Robert Reichelt, Sebastian Gunther, Luca Gregoratti, Tang Lin Teo, Maya Kiskinova, Alexander Yulaev, Ivan Vlassiouk, Andrei Kolmakov
Photoelectron spectroscopy (PES) and microscopy are highly demanded for exploring morphologically complex solid-gas and solid-liquid interfaces under realistic conditions but the very small electron mean free path inside the dense media imposes serious
Ndubuisi G. Orji, Ronald G. Dixson, Hiroshi Itoh, Chumei Wang
In atomic force microscopy (AFM) metrology, the scanning tip is a major source of uncertainty. Images taken with an AFM show an apparent broadening of feature dimensions due to the finite size of the tip. An AFM image is a combination of the feature shape
Katherine P. Rice, Andrew Paterson, Mark Stoykovich
The low-temperature oxidation of ~10 nm diameter copper nanocrystals was characterized using in-situ UV-vis absorbance spectroscopy and observed to lead to hollow copper oxide shells via the nanoscale Kirkendall effect. The kinetics of the oxidation of
Tyler R. Harvey, Jordan S. Pierce, Amit Agrawal, Benjamin McMorran, Peter Ercius, Martin Linck
Electron diffraction gratings can be used to imprint well-defined phase structure onto an electron beam. For example, diffraction gratings have been used to prepare electron beams with unique phase dislocations, such as electron vortex beams, which hold
Andrew L. Balk, Lamar O. Mair, Pramod Mathai, Paul N. Patrone, Wei Wang, Suzanne Ahmed, Thomas Mallouk, James A. Liddle, Samuel M. Stavis
We measure the microvortical flows around gold nanorods propelled by ultrasound in water using polystyrene nanoparticles as optical tracers. We infer the rotational frequencies of such nanomotors assuming a hydrodynamic model of this interaction. In this
Electrical modes of scanning probe microscopes have found considerable metrology applications in integrated circuits and emerging nano-electronic devices. This paper will review the critical metrology needs that electrical SPMs have addressed in the
Shuze Zhu, Yinjun Huang, Nikolai Klimov, David B. Newell, Nikolai Zhitenev, Joseph A. Stroscio, Santiago D. Solares Rivera, Teng Li
Recent experiments reveal that a scanning tunneling microscopy (STM) probe tip can generate a highly localized strain field in a graphene drumhead, which in turn leads to pseudomagnetic fields in the graphene that can spatially confine graphene charge
Solomon I. Woods, Snorri Ingvarsson, Shouheng Sun, John Kirtley
Expressions for the thermal noise from a collection of exchange-biased magnetic nanoparticles are derived and used to analyze the magnetic noise from thin films of partially oxidized nanoparticles. Functionalized Co nanoparticles with diameters between 3
Critical dimension atomic force microscopes (CD-AFMs) use flared tips and two-dimensional sensing and position control of the tip-sample interaction to enable scanning of features with near-vertical or reentrant sidewalls. Sidewall sensing usually involves
Some of the most critical issues facing the nanocomposite community include the need for multi-scale imaging of hierarchical structures, effective methods for controlling nanoparticle chemistry and surface-energy, and efficient processing methods for
Sujitra J. Pookpanratana, Joseph W. Robertson, Curt A. Richter, Christina A. Hacker, Lee J. Richter, Julia Savchenko, Steven Cummings, Tong Ren
We report the formation of molecular monolayers containing redox-active diruthenium(II,III) compound to gold and silicon surfaces via click chemistry. The use of Cu-catalyzed azide-alkyne cycloaddition enables modular design of molecular surfaces and
Combining heated-tip atomic force microscopy (HT-AFM) with quantitative methods for determining surface mechanical properties creates an avenue for nanoscale thermomechanical property characterization. For nanomechanical methods that employ an atomic force
Aaron M. Katzenmeyer, Jungseok Chae, Richard Kasica, Glenn Holland, Basudev Lahiri, Andrea Centrone
The collective oscillation of conduction electrons in plasmonic nanomaterials allows the coupling of propagating light waves with nanoscale volumes of matter ("hot spots") and allows engineering their optical response from the UV to THz as a function of
We experimentally demonstrate that the three-dimensional (3-D) shape variations of nanometer-scale objects can be resolved and measured with sub-nanometer scale sensitivity using conventional optical microscopes by analyzing 3-D optical data using the
Nathan D. Orloff, Jan Obrzut, Christian J. Long, Thomas F. Lam, James C. Booth, David R. Novotny, James A. Liddle, Pavel Kabos
The non-uniform fields that occur due to the slot in the cavity through which the sample is inserted and those due to the sample geometry itself decrease the accuracy of dielectric characterization by cavity perturbation at microwave frequencies. To
Seung H. Ko, Luis F. Vargas Lara, Paul Patrone, Samuel Stavis, Francis W. Starr, Jack F. Douglas, James Alexander Liddle
DNA origami is a powerful platform for assembling gold nanoparticle constructs, an important class of nanostructure with numerous applications. Such constructs are assembled by the association of complementary DNA oligomers. These association reactions
Josh Ballard, Stephen McDonnell, Don Dick, Maia Bischof, Joseph Fu, D Jaeger, James Owen , w Owen, Justin Alexander, Udi Fuchs, Pradeep Namboodiri, Kai Li, John Randall, Robert Wallace, Yves Chabal, Richard Reidy, Richard M. Silver
Reducing the scale of etched nanostructures below the 10 nm range eventually will require an atomic scale understanding of the masks being used in order to maintain exquisite control over both feature size and feature density. Here, we demonstrate a method
Ann C. Chiaramonti Debay, Sten Vollebregt, Sarbajit Banerjee, Kees Beenakker, R. Ishihara
While carbon nanotubes (CNT) have been suggested as thermal management mate- rial for integrated circuits, the thermal properties and especially the thermal bound- ary resistance (TBR) of as-grown CNT have hardly been investigated. Here the thermal
Andrew Herzing, Steven A. Hawks, Jordan C. Aguirre, Laura T. Schelhas, Robert Thompson, Rachel Huber, Amy Ferreira, Guangye Zhang, Robert A. Street, Sarah Tolbert, Benjamin Schwartz
Efficient bulk heterojunction (BHJ) solar cells based on polymer:fullerene photoactive layers can be created either by traditional blend casting (BC), where the components are mixed together in solution before being cast, or by solution-sequential
Heayoung Yoon, Christopher C. Bohn, Youngmin Lee, Seung H. Ko, Jonathan S. Steckel, Seth Coe-Sullivan, Nikolai B. Zhitenev
A thin film of quantum dots (QD) was used to visualize the local photo-response of polycrystalline CdTe solar cells by down-converting an electron beam of high energy to photons of visible light. The efficient photon generation in the QD film is compared
Atif A. Imtiaz, Thomas M. Wallis, Joel C. Weber, Kevin J. Coakley, Matthew D. Brubaker, Paul T. Blanchard, Kristine A. Bertness, Norman A. Sanford
We used a broadband, atomic-force-microscope-based, scanning microwave microscope (AFM-SMM) to probe the axial dependence of the depletion in a GaN nanowire (NW) p-n junction structure. The NWs were c-axis oriented and grown by molecular beam epitaxy. The