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Chun-Chieh Tien, Ching-Hsuan Chang, Bernard Hao-Chih Liu, Deborah Jacobs, Savelas A. Rabb, Lee L. Yu, Tinh Nguyen, Li Piin Sung
Polymer nanocoatings are increasingly used outdoors and in harsh environments. However, because most common polymers degraded by the weathering elements, nanoparticles in polymer nanocoatings may be released into the environments. Such nanoparticle release
Elijah Petersen, Thomas F. Lam, Justin Gorham, Keana Scott, Chris Long, Renu Sharma, Li Piin Sung, James Alexander Liddle, Tinh Nguyen
Nanomaterials can be used as nanofillers to enhance the properties of polymeric materials. However, the effect of weathering on nanocomposites and the potential for nanomaterial release is not yet well understood. Multiple analytical methods are needed to
Wyatt N. Vreeland, Anne A. Galyean, James J. Filliben, Richard D. Holbrook, Dean C. Ripple, Howard S. Weinberg
The development of standardized and optimized methods to characterize polydisperse nanoparticles in complex matrixes is considered a critical component in many fields. Robust, rigorously optimized methods are currently lacking, in part because of matrix
Karen E. Murphy, Jingyu Liu, William F. Guthrie, Justin M. Gorham, John E. Bonevich, Andrew J. Allen, Michael R. Winchester, Vincent A. Hackley, Robert MacCuspie
In this study we use inductively coupled plasma mass spectrometry operated in single particle mode (spICP-MS) to simultaneously characterize the size distribution and dissolved silver fraction of a new silver nanoparticle (AgNP) candidate reference
Michael T. Postek, Andras Vladar, Premsagar P. Kavuri
The scanning electron microscope (SEM)has gone through a tremendous evolution to become indispensable for many and diverse scientific and industrial applications. The improvements have significantly enriched and augmented the overall SEM performance and
Randolph E. Elmquist, Fan-Hung Liu, Lung-I Huang, Yasuhiro Fukuyama, Chi-Te Liang, Yanfei Yang
We study the quantum corrections caused by electron-electron (e-e) interactions and localization to the conductivity in few-layer epitaxial graphene, in which the carriers responsible for transport are massive. Our results demonstrate that the diffusive
C. J. Zhu, X Zhao, Guoxiang Huang, Lu Deng, Edward W. Hagley, Yan Ren
We show that coherent broadband surface mixing-wave (SMW) by a hyper-Raman process can be efficiently generated near a metallic surface abutting a quasi-three-level gain medium. The generation process is significantly enhanced by the amplified surface
Bonghwan Chon, Kimberly Briggman, Jeeseong C. Hwang
We report on an experimental procedure in confocal single molecule fluorescence lifetime correlation spectroscopy (FLCS) to determine the range of excitation power and molecule concentration in solution under which the application of an unmodified model
Guangjun Cheng, Brent A. Sperling, James E. Maslar, Curt A. Richter, Angela R. Hight Walker
We present an investigation on tearing and scrolling of the transferred graphene on a Si/SiO2 substrate. Graphene grown by chemical vapor deposition (CVD) is transferred onto a Si/SiO2 substrate using a wet polymer-mediated process. Upon the removal of
Iulia A. Sacui, Jeffrey W. Gilman, Ryan C. Nieuwendaal, Stephan J. Stranick, Henryk Szmacinski, Mehdi Jorfi, Christopher Weder, Johan Foster, Richard Olsson, Daniel Burnett
This work describes the study and characterization of native cellulose nanocrystals and nanofibrils (CNCs, CNFs), whose crystallinity, morphology, aspect ratio, and surface chemistry depend on the raw material source and hydrolysis conditions. Measurement
Ming Zheng, Min Zhang, Constantine Y. Khripin, Jeffrey Fagan, Yoichiro Ito
Development of simple processes to fractionate synthetic mixtures of single-wall carbon nanotubes (SWCNTs) into individual species is crucial to many applications. Existing methods for single- chirality SWCNT purification are cumbersome, often requiring
Michael Campbell, Qingkun Liu, Aric Sanders, Julian Evans, Ivan I. Smalyukh
Using liquid crystalline self-assembly of cellulose nanocrystals, we achieve long-range alignment of anisotropic metal nanoparticles in colloidal nanocrystal dispersions that are then used to deposit thin structured films with ordering features highly
Paul T. Blanchard, Kristine A. Bertness, Todd E. Harvey, Norman A. Sanford
Contact resistivity ρ c is an important figure of merit in evaluating and improving the performance of electronic and optoelectronic devices. Due to the small size, unique morphology, and uncertain transport properties of semiconductor nanowires (NWs)
Katherine P. Rice, Robert R. Keller, Mark Stoykovich
We report the effects of varying specimen thickness onthe generation of transmission Kikuchi patterns in the scanning electron microscope. Diffraction patterns sufficient for automated indexing were observed from films spanning nearly three orders of
Justin M. Gorham, Anne B. Rohlfing, Katrice A. Lippa, Robert I. MacCuspie, Amy Hemmati, Richard D. Holbrook
A critical but often overlooked component of silver nanoparticle (AgNPs) suspensions involves their behavior following short- and long-term storage. The current study investigates the integrity of citrate-capped AgNP suspensions, nominally 20 nm in
Tae Joon Cho, Robert I. MacCuspie, Julien C. Gigault, Justin M. Gorham, John T. Elliott, Vincent A. Hackley
We report the development of a novel cationic dendron (TAG1-PCD) and a positively charged gold nanoparticle-dendron conjugate (PCD-AuNP). TAG1-PCD was designed by considering the reactivity, hydrophilicity, and cationic nature that is required to yield a
We analysed the resonance frequency, amplitude, and phase response of the first two eigenmodes of two contact-resonance atomic force microscopy (CR-AFM) configurations, differing in the method used to excite the system (cantilever base vs. sample
Jingyu Liu, Karen E. Murphy, Robert I. MacCuspie, Michael R. Winchester
The increasing application of engineered nanomaterials in consumer and medical products has motivated the development of single particle inductively coupled plasma mass spectrometry (spICP-MS) for characterizing nanomaterials under realistic environmental
Michael T. Postek, Andras Vladar, Bin Ming, Bunday Benjamin
Reference Material (RM) 8820 is a multipurpose instrument calibration standard available from NIST. This is a dimensional standard initially developed to replace the out of stock RM 8090 used for X and Y scale calibrations of scanned particle beam
Thomas J. Silva, Justin M. Shaw, Hans T. Nembach, Mike Mallary, Kumar Srinivasan, Gerado Bertero, Dan Wolf, Christian Kaiser, Michael Chaplin, Mahendra Pakala, Leng Qunwen, Yiming Wang, Carl Elliot, Lui Francis
A specific design for Microwave Assisted Magnetic Recording (MAMR) at about 3Tb/in 2 (0.47 Tb/cm 2 or 4.7 Pb/m 2) is discussed in detail to highlight the challenges of MAMR and to contrast its requirements with conventional Perpendicular Magnetic Recording
Ryan McCaffrey, Hai Long, Yinghua Jin, Aric Sanders, Wounjhang Park, Wei Zhang
We report a novel strategy for the controlled synthesis of gold nanoparticles (AuNPs) with narrow size distribution (1.9 plus or minus} 0.4 nm) through NP nucleation and growth inside the cavity of a well-defined three-dimensional, shape-persistent organic
The scanning electron microscope (SEM) has gone through a tremendous evolution to become a critical tool for many and diverse scientific and industrial applications. The high resolution of the SEM is especially suited for both qualitative and quantitative
Elijah Petersen, Thomas F. Lam, Justin Gorham, Keana Scott, Chris Long, Deborah Jacobs, Renu Sharma, James Alexander Liddle, Tinh Nguyen
One of the most promising applications of nanomaterials is as nanofillers to enhance the properties of polymeric materials. However, the effect of nanofillers on polymers subject to typical environmental stresses, such as ultraviolet (UV) radiation, high