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The high resolution of the SEM is especially useful for qualitative and quantitative applications for both nanotechnology and nanomanufacturing. But, should users be concerned about the imaging and measurements made with this instrument? Perhaps one should
Michael T. Postek, Andras Vladar, Premsagar P. Kavuri
The scanning electron microscope (SEM) has gone through a tremendous evolution to become a critical tool for many and diverse scientific and industrial applications. The improvements that have been made have significantly improved the overall SEM
Pooneh Taghizadeh-Saheli, R. K. Rowe, Elijah Petersen, Denis O'Carroll
Carbon nanotubes are used in a wide range of consumer products. During the last few years, the applications for, and production of, carbon nanotubes has increased substantially. Due to their potential environmental and human health risks and eventual
Babak Nikoobakht, Xudong Wang, Andrew A. Herzing, Jian Shib
On integrating one-dimensional (1D) nanocrystals (nanowires) to useful devices, in this review article, we provide a background on growth processes and how they impact device integration strategies. Successful integration of nanowires to devices and their
Scott A. Wight, Simeon K. Adesina, Emmanuel O. Akala
Factors influencing size and other characteristics of nanoparticles prepared by free radical dispersion polymerization are discussed. Further, the results of optimization studies designed to minimize the size of crosslinked biodegradable stealth polymeric
Amber Nagy, Jennifer A. Hollingsworth, Bin Hu, Andrea Steinbruck, Peter C. Stark, Cristina Rios Valdez, Momchilo Vuyisich, Michael H. Stewart, Donald H. Atha, Bryant C. Nelson, Rashi Iyer
Quantum dots (QDs) are semiconductor nanocrystals exhibiting unique optical properties which can be exploited for many practical applications ranging from photovoltaics to biomedical imaging and drug delivery. They are increasingly manufactured in large
Kela Weber, Elijah Petersen, Sonja Bissegger, Lars Rehmann, Iris Koch, Jun Zhang, Kenneth Reimer, Robin Slawson, Raymond Legge, Denis O'Carroll
With an increasing utilization of nanoparticles (NPs) in consumer products, the potential for release to the environment also increases. It is therefore imperative that methods to test their potential effects in ecosystems are developed. This study
This interim report summarizes research results to date under the FY2012 interagency agreement between CPSC and NIST to develop testing and measurement protocols for determining the quantities and properties of nanoparticles released from flooring finishes
Jenny R. Roberts, Walt McKinney, Hong Kan, Kristine Krajnak, David G. Frazer, Treye Thomas, Stacey Waugh, Allison Kenyon, Robert I. MacCuspie, Vincent A. Hackley, Vincent Castranova
Rats were exposed by inhalation to filtered air or to a low (100 ug/m3 using a commercial antimicrobial product [20 mg/L silver]) or high (1000 ug/m3 using a suspension [200 mg/L silver] synthesized to have a similar size distribution) concentration of
De-Hao D. Tsai, Frank W. DelRio, John M. Pettibone, Pin A. Lin, Jiaojie Tan, Michael R. Zachariah, Vincent A. Hackley
In this study, an electrospray-differential mobility analyzer (ES-DMA) was operated with an aerosol flow-mode, temperature-programmed approach to enhance its ability to characterize the particle size distributions (PSDs) of nanoscale particles (NPs) in the
The TSOM method provides three-dimensional nanoscale metrology using a conventional optical microscope. Substantial improvements in defect detectability using the TSOM method will be presented. The TSOM method shows potential to (i) detect phase defects on
Michael T. Postek, Robert J. Moon, Alan Rudie, Michael Bilodeau
Production and Applications of Cellulosic Nanomaterials was intended to help organize and highlight the wide range of research being conducted worldwide on the science and technology of cellulose nanomaterials. The format of this book consists of short
Bryan M. Barnes, Martin Y. Sohn, Francois R. Goasmat, Hui Zhou, Richard M. Silver, Abraham Arceo
Experimental imaging at =193 nm of sub-resolved defects performed at several focus positions yields a volume of spatial and intensity data. Defects are located in a differential volume, given a reference, with up to 5x increase in sensitivity.
Cellulose nanocrystals are one group of nanoparticles that have high potential economic value but, also present many basic research and manufacturing challenges. These challenges are not only in development of the fundamental processes needed for the
Ravikiran Attota, Benjamin D. Bunday, Victor Vertanian
We present results using simulations and experiments to demonstrate metrological applications of the through-focus scanning optical microscopy (TSOM) down to features at and well below the International Technology Roadmap for Semiconductors' 22 nm node
Julian S. Taurozzi, Vincent A. Hackley, Mark R. Wiesner
Toxicity and fate assessment are key elements in the evaluation of the environmental, health and safety risks of engineered nanomaterials (ENMs). While significant effort and resources have been devoted to the toxicological evaluation of many ENMs
Accurate characterization of nanomaterial properties is a critical component of any nanotoxicology testing strategy. Data that describes the performance of various laboratories to measure the characteristics of the same nanomaterial is scarce. We conducted
Shmuel Barzilai, Francesca M. Tavazza, Lyle E. Levine
Gold nanowire chains are considered a good candidate for nanoelectronic devices because they exhibit remarkable structural and electrical properties. A previous study shows that the beryllium terminated BeO (0001) surface may be a useful platform for
Mauro Zammarano, Rick D. Davis, Yeon S. Kim, Richard H. Harris Jr., Marc R. Nyden, Jeffrey W. Gilman, Nasir M. Uddin
Nanoparticles can effectively reduce polymer flammability; however, the impact of nanoparticles on environmental and health safety is still unclear. The purpose of this study is twofold: (1) to develop and investigate the effect of nanoparticle-rich
Justin M. Gorham, Tinh Nguyen, Deborah S. Jacobs, Coralie Bernard, Richard D. Holbrook
Silica nanoparticles (SiNPs) incorporated into a polymeric matrix, or silica nanocomposites (SiNCs), are used in a wide variety of commercially available products in numerous natural and artificial environments. Environmental factors, such as light, may
Elijah J. Petersen, Xiaomin X. Tu, M Miral Dizdar, Ming Zheng, Bryant C. Nelson
Ultrasonication is a physical process known to generate abundant levels of oxygen-derived species such as hydroxyl radicals, hydrogen atoms, and hydrogen peroxide. When used to process DNA solutions, these highly reactive hydroxyl radicals can react with
Elijah J. Petersen, Bryce Marquis, Pawel Jaruga, M Miral Dizdar, Bryant C. Nelson
Hyphenated mass spectrometry techniques have been employed as one of the primary analytical tools for investigating the effects of ionizing radiation, chemical/biological carcinogens, and oxygen derived free radicals on the induction and subsequent repair
Bryant C. Nelson, Bryce J. Marquis, Piper R. Hunt, Katherine M. Tyner, Sean Conklin, Nicholas Olejnik, Robert L. Sprando
The utility of C. elegans as an alternative model to assess nanomaterial toxicity was evaluated using 10 nm silver particles (10nmAg). Endpoints of nanomaterial uptake and localization, larval growth, morphology, and DNA damage were assessed. Orally
Mohammad Olfatnia, Siddharth Sood, Jason J. Gorman, Shorya Awtar
This paper reports in-plane electrostatic combdrive actuators with stroke as large as 245 μm that is achieved by employing a novel Clamped Paired Double Parallelogram (C-DPDP) flexure mechanism. The C-DP-DP flexure mechanism design offers high bearing