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A technique for determining the in-plane modulus and the coefficient of thermal expansion (CTE) of supported thin films has been developed. The modulus and CTE are calculated by solving two coupled equations that relate the curvature of film samples
Daniel A. Fischer, S Sambasivan, A Kuperman, Y Platonov, J L. Wood
Fluorescence yield x-ray absorption spectroscopy of the low Z elements C, N, O, and F is a powerful tool for understanding the local structure and chemistry of diverse materials, even in the presence of reactive atmospheres. This technique uses tunable
The surface crack in flexure method uses a Knoop indenter to create small semi elliptical surface pre cracks in beam specimens. Lateral cracks may interfere with and cause errors in measurements of fracture toughness particularly for materials whose
P M. McGuiggan, C S. Bhatia, D Bogy, W Fong, Stephen M. Hsu
The friction force as a function of humidity was measured between 5 nm thick carbon films coated onto mica surfaces. The friction was found to be proportional to the area of contact. The shear stress at 0%, 33%, and 100% humidity was measured to be 25 +6
Walter G. McDonough, Joy Dunkers, Gale A. Holmes, E Feresenbet, Y H. Kim, Richard~undefined~undefined~undefined~undefined~undefined Parnas
The single fiber fragmentation test was used to investigate the effect of gelation time on interfacial shear properties of fast reacting resin systems. We developed a processing system capable of producing single fiber fragmentation samples with gelation
V Ferreiro, Jack F. Douglas, James A. Warren, Alamgir Karim
The crystallization of polymeric and metallic materials normally occurs under conditions far from equilibrium. The morphologies formed reflect a competition between order associated with the symmetries of the equilibrium crystal geometry and disorder
E J. Nelson, Joseph C. Woicik, P Pianetta, I A. Vartanyants, J W. Cooper
Near an x-ray Bragg reflection, two x-ray beams (incident and reflected) with opposite wavevectors exist within the crystal to create an x-ray standing wave (XSW) interference field. The part of the photoelectron yield depending on quadrupole (and higher
Results from DSC, SAXS and WAXD show some new insights into the evolution of structural variables during Curie transition in PVDF/TrFE copolymer. The differences of long period evolution between the melt-crystallized samples in the paraelectric phase (> 80
Strontium- and magnesium-doped lanthanum gallate (LSGM) was deliberately prepared to give A-site deficient non-stoichiometry with compositions (La 0.9Sr 0.1)z(Ga 0.8Mg 0.2)O 3-delta (z =1.0,0.98, and 0.95). Creep tests in four-point 950 C 75 Mpa in air
J Ilavsky, Andrew J. Allen, Gabrielle G. Long, P Jemain
Small-angle scattering is widely used for measuring materials microstructure in the 1 nm to 100 nm size range. Ultra-small-angle x-ray scattering (USAXS), typically achieved through crystal collimation, extends this size range to include features over 1 mm
Experimental evidence has been given for the comparison of zeta potential as measured with the electrokinetic sonic amplitude (ESA) method and streaming potential as measured with the particle charge detection (PCD) method. The measurements have been
Daniel A. Fischer, S Sambasivan, A Kuperman, Y Platonov, J L. Wood
Fluorescence yield carbon K edge soft x-ray absorption measurements of mixed element samples are impeded by background scattered x-rays and fluorescence from non carbon atoms within the sample induced by the incident x-ray beam (first and higher orders)
Charles E. Bouldin, A L. Ankudinov, J J. Rehr, James S. Sims, Howard Hung
Real space multiple scattering calculations of the elctronic density of states and x-ray spectra in solids typically scale as the cube of the system and basis set size, and hence are highly demanding computationally. For example, calculations near the Si K
Interfacial resistivity (p) is crucial in limiting the maximum current density (J n max) in certain superconductor/metal junctions: as p decreases, J n max keeps rising until ultimately limited by the superconductor's critical current density. This little
A pre-existing microcrack is considered to grow in steady state along a grain boundary of an interconnect line under the action of an applied electric field. Consistent with electromigration, the mechanism of crack growth is assumed via diffusive transport
L Gamble, Bruce Ravel, Daniel A. Fischer, David G. Castner
Near edge X-ray absorption fine structure (NEXAFS) experiments have provided information about the orientation of adsorbed small molecules, self-assembled monolayers, and polymers. Long fluorocarbon chains are known to have a twisted (or helical) structure
M Mihalkovic, I Al-Lehyani, Eric J. Cockayne, C L. Henley, N Moghadam, J A. Moriarty, Yijun Wang, M Widom
Quasicrystals are metal alloys whose noncrystallographic symmetry and lack of structural periodicity challenge methods of both experimental structure determination and theoretical structural prediction. Here we employ total energy calculations and Monte
A materials perspective of layered dental material systems representing tooth and crown structures is presented. In this study, failure modes in model bilayers and trilayers with relatively hard, brittle ceramic (veneer and veneer/core) outerlayers on soft
Autocorrelation is shown to be useful in describing the periodic patterns found in high-resolution mass spectra of synthetic polymers. Examples of this usefulness are described for a simple linear homopolymer to demonstrate the method fundamentals, a
Lubrication is an art that has been practiced for thousands of years from the early days of our human civilization. The study of lubricatin as a science began in the 17th century with the development of bearings and axles. In the early 20th century, the
Nearly fully dense polycrystalline TiB 2 can be produced by a variety of processing methods, including sintering, hot pressing, hot isostatic pressing, microwave sintering, and dynamic compaction. The relatively strong covalent bonding of the constituents
Fourteen laboratories participated in an ubterkabiratirt study to establish the within- and between-laboratory repeatability of tensile creep rupture of silicon nitride. In air at 1375 C at 200 Mpa the times to failure ranged over a factor of 50, and the
Supercurrent dissipation and strain-induced damage in Bi-2223/Ag high temperature superconductor composite tape, at 77 K in self-field, are studied by IV curve analysis. Five dissipation models are considered, and differently processed tapes are compared
The inhomogeneous morphology of the surface asperities generated during metal forming causes strain localization resulting in tearing during metal forming, and increasing friction between mating die surfaces. Much of the data in the literature do not
Throughout the past century NBS/NIST supported a great variety of research studies in crystallography where the aim was the highest attainable accuracy in measurement. While avoiding overlap with other papers in this volume, this article summarizes results