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Chemistry

Analytical chemistry

Projects/Programs

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High-Precision Isotopic Reference Materials

Ongoing

A new generation of multi-collector IRMS, utilizing both inductively coupled plasma and thermal ionization sample sources, is now capable of measuring isotope ratios with extremely high precision – a few parts in 10 6. This new measurement capability has caused a minor revolution in the use of...

High-Sensitivity IR Spectroscopy of Proteins

Ongoing

Infrared (IR) absorption spectroscopy has been widely used as a non-invasive, label-free characterization method of chemical identification and structure for complex biomolecules. Conventional IR spectroscopy, e.g., Fourier-transform IR (FT-IR) technology, can characterize proteins and other...

Identification, Suitability Testing, and Property Determination from Untargeted Measurements

Ongoing

In many applications, detailed knowledge of a fluid mixture’s physical behavior is needed. This can include physical properties such as viscosity and qualitative properties such as solubility. For instance, a dissolved polymer may suddenly precipitate out of solution when exposed to saline, and if...

Figure with five interlocking puzzle pieces representing different aspects of the measurement process.

Improving High-Performance Inductively-Coupled Plasma Optical Emission Spectrometry (HP-ICP-OES) Through Exact Matching

Ongoing

A thorough understanding of the analytical benefits and characteristics of the implementation of exact matching with HP-ICP-OES will enable HP-ICP-OES to be applied more effectively to a variety of NIST measurements. Such measurements include, but are not limited to, value assignment measurements...

Infrared Imaging of Live Cells: Absolute Quantity Measurement of Biomolecules

Ongoing

The NIST Biomaterials Group introduced benchtop infrared (IR) microscopy based on a quantum cascade laser (QCL) as a quantitative chemical imaging modality of live cells. The strong IR absorption by water was mitigated by a solvent absorption compensation (SAC) technique, which pre-compensates for...

Photograph of a weathered metal surface labeled Danger Toxic Fumes

Instrument Standards for Detection of Hazardous Chemical Vapors

Ongoing

Chemical threat detection is a challenging problem. Contaminants must be accurately identified and quantified often in complex mixtures where non-toxic components can often obscure the measurement. Furthermore, highly toxic chemicals are problematic at low concentrations, requiring ultra-sensitive...

International Comparisons for Chemical Measurements

Ongoing

International agreements and decisions concerning trade and our social well-being increasingly require mutual recognition of measurements and tests among nations. The Mutual Recognition Arrangement (MRA) on national measurement standards and calibration and measurement certificates issued by NMIs...

Ion Mobility Spectrometry

Ongoing

IMS employs a drift tube with an applied electric field to separate ionized molecules based on their mobility. The technique is robust and capable of differentiating a wide range of drug and explosive molecules. Recent work has sought to investigate the utility of IMS for screening of illicit...

Photograph of a seabird with a spotted turquoise egg.

Isotopes as Environmental Tracers in Biological Specimens

Ongoing

Multicollector inductively coupled plasma mass spectrometry (MC-ICP-MS) provides sensitive and precise measurements of stable isotope ratios and can be coupled to a variety sample introduction systems such as laser ablation and gas or liquid chromatography. The versatility and performance of MC-ICP...

Macromolecular Architectures

Ongoing

This project’s purpose is to synthesize and characterize model thermoplastics, thermoplastic elastomers (TPE), and mixed resins with systematic variation of polymer sequence, chemistry, and architectures to generate libraries of quantitative structure-property relationships validated by multiple...

Magnetic Sector Secondary Ion Mass Spectrometry

Ongoing

Magnetic sector SIMS uses high energy “primary” ions to bombard the surface and liberate “secondary” ions much like in ToF-SIMS, but the ion beam is operated continuously to maximize duty cycle. The high ion dose is preferred for depth profiling, where the concentration of elements and isotopes are...

Measurement Quality in Hydrogen Storage R&D

Ongoing

The hydrogen storage project targets metrologies that assess kinetics and energetics of hydrogen charging and discharging in combinatorial structures as well as the degradation mechanisms that limit life of use. New capabilities are being developed and several existing measurement capabilities are...

Measurement and Sampling Standards

Ongoing

A foundational activity that crosscuts our research goals is the development of a variety of standards and test materials to support the effective operation of trace explosive and narcotic detection devices. Trace sampling issues are addressed through fundamental studies on the adhesion and...

Measurements and Standards for Botanical Dietary Supplements

Ongoing

Many consumers believe that botanical dietary supplements will improve their health and that these "natural" remedies are both effective and free from the side effects that may occur with other medications. There are occasional reports of inaccurate labeling, adulteration, contamination (with...

Measurements and Standards for Contaminants in Biological (Human) Materials

Ongoing

The development of SRMs to support measurements for contaminants in biological fluids and tissues will expand quality assurance capabilities to important species critical to human health. We will provide SRMs that are representative of the analytical challenges that may be encountered by analysts in...

Measurements and Standards to Support Nutrition Labeling

Ongoing

Well-characterized certified reference materials are needed by laboratories in the food testing and nutrition communities to facilitate compliance with labeling laws and improve the accuracy of information provided on product labels so that consumers can make good choices. As a result of the...

Wordcloud figure with about 25 words including NIST, metabolomics, quality assurance, and measurements.

Metabolomics Quality Assurance and Quality Control Materials (MetQual) Program

Ongoing

Metabolomics, a rapidly growing field of systems biology, is expanding beyond human health and precision medicine to encompass areas such as food science, biomanufacturing, and forensic investigation. Analytical techniques include both targeted identification and quantification of metabolites and...

Method Assessment for Non-Targeted Analyses (MANTA) Program

Ongoing

Typical targeted analysis aims to detect and/or quantify a set of known chemical compounds using specific instrumental techniques (such as liquid chromatography with triple quadrupole mass spectrometry). In contrast, non-targeted analysis is an analytical technique that detects, identifies, and/or...

Direct Analysis in Real Time Mass Spectrometry infogram

Methods, Software Tools, and Resources for Forensics Laboratories with DART-MS or other AI-MS Techniques

Ongoing

The development of methods, software tools, and resources for forensic laboratories using DART-MS or other AI-MS techniques is a collaborative effort between the Surface and Trace Chemical Analysis Group (STCAG), the Mass Spectrometry Data Center (MSDC), and practicing forensic laboratories across...

pH Metrology

Ongoing

The suite of NIST pH SRMs forms the basis for pH measurements in the United States, and pH is the most-often-measured chemical quantity. Hence this NIST work directly or indirectly impacts a large number of users in industry, government, and academia. One of the most critical set of users is in...

Metrology and Standards for Canine Olfactory Detection of Explosives

Completed

Effective and accepted by the public, trained dogs are the most frequently deployed detection systems for identification of explosives threats in mobile applications. In addition to being highly sensitive, dogs can rapidly discriminate the unique profile of an explosive in a presence of a large...

A micromechanical bulk acoustic resonator that uses phononic crystal tethers to achieve a quality factor approaching the fundamental dissipation limit (fxQ can be as large as 1.2 x 1013 Hz)

Micro- and Nanoelectromechanical Systems

Completed

MEMS/NEMS are enabling technologies that bring new functionalities with the potential to radically transform markets ranging from consumer products to national defense. The meteoric rise of the smartphone is an excellent example, in which MEMS accelerometers, gyroscopes, microphones, displays, and...

Figure showing four components of metabolomics with samples and processing

Microbial Metabolomics

Ongoing

Mass spectrometry (MS) and nuclear magnetic resonance (NMR) spectroscopy are widely used and complementary analytical platforms for the characterization, identification, and quantification of a metabolome. MS techniques, typically coupled to chromatography, provide a chemical fingerprint of complex...

Micronutrients Measurement Quality Assurance Program (MMQAP)

Completed

The MMQAP supported the long-term (months to years) reliability of selected fat- or water-soluble vitamin measurements in human serum and plasma. Results from the comparison studies helped participants to make accurate clinical and health-care decisions as well as to maintain and improve their...

Graphic of a erlenmeyer flask containing tilled soil, a green leaf, and yellow wheat.

Molecular Innovation in Agriculture

Ongoing

Plant science and breeding aim to develop new plant phenotypes with desired qualities, increased production, disease resistance, and traits that reduce water usage. At the federal level, plant research is conducted by the USDA's Animal and Plant Health Inspection Service (APHIS) and Agricultural...

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