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T J. Haugan, Winnie K. Wong-Ng, Lawrence P. Cook, H J. Brown, L Swartzendruber, D T. Shaw
Investigations into flux pinning of Bi 2Sr 2 CaCu 2O 8+γ /Ag (Bi-2212/Ag) thick film conductors utilizing micron-sized (Sr,Ca) 14Cu 24O 41 and nanophase Al 2O 3 and Au particles are described. Addition of defect particles delayed and reduced formation of
Ultra-small-angle X-ray scattering by dislocations in single-crystal aluminum has been observed in situ as a function of plastic deformation. The scattering is observed to be strongly dependent upon sample orientation, with single dislocations, dislocation
We examine the stability of polarization switching in polyscrystalline ferroelectric/ferroelastic materials subject to continuous electromechanical loading. In case of unstable switching, a finite change of remanent polarization or strain results from an
D W. Schaefer, T Rieker, M M. Agamalian, J S. Lin, Daniel A. Fischer, S Sukumaran, C I. Chen, G Beaucage, C Herd, J Ivie
We study the structure of colloidal silica and carbon on length scales from 0.25 -1 7 using x-ray, neutron and light scattering. These materials consist of primary particles of the order of 100 , aggregated into micrometer-sized aggregates that in turn are
The electric fatigue behavior of a commercial lead zirconate titanate (PZT) was investigated by optical microscopy and instrumented Hertzian microindentation. Macroscopic delamination cracks were found near the electrodes after large numbers of electrical
E J. Nelson, Joseph C. Woicik, M Hong, JP Mannaerts
Extended x-ray absorption fine structure (EXAFS) has been used to measure the bond length in a 23 epitaxial Gd 2O 3 film grown on GaAs(001). The Gd-O bond length is determined to be 2.390 0.013 or a bond-length strain of +2.7 0.6 % relative to the bond
Total energy calculations were performed for three perovskite related ordered supercells in several stoichiometries of A(B,B')O 3; where A = Pb 2+, Ba 2+ and B = Mg 2+ Zn 2+, Sc 3+, In 3+ and B' = Nb 5+, Ta 5+, W 6+. A striking difference between the Pb-
Andrew J. Allen, J Ilavsky, Gabrielle G. Long, Jay S. Wallace, C C. Berndt, H Herman
Density, electron microscopy, elastic modulus, and small-angle neutron scattering studies are used to characterize the microstructures of yttria-stabilized zirconis plasma-sprayed deposits as a function fo both feedstock morphology and annealing. In
Melting information for the Pb-doped 2223 high T c phase in the Bi(Pb)-Sr-Ca-Cu-O system is important for the superconducting wire and tape industry. This paper examines the melting equilibria of a composition Bi 1.8Pb 0.4Sr 2Ca 2.2Cu 3O x under oxygen
The effects of the thickness of the thermally grown oxide on residual thermal stresses in a plasma-sprayed thermal barrier coating were numerically simulated in Part I. In the tip region of a convex asperity, the residual stress normal to the interface,
The perovskite phase SrPbO 3 is important as a buffer and indicator of PbO chemical potential (at fixed p O2 ) according to the reaction: 2 SrPbO 3 --> Sr 2PbO 4 + PbO(g) + 1/2 O2 (g), where the term PbO(g) includes several Pb-containing gaseous species
The thermal conductivity of porous α-Al 2O 3 specimens prepared using nanosize γ-Al 2O 3 powder or conventional sub-micro a}-alumina powders was studied. Plots of thermal conductivity versus volume fraction porosity showed that both sets of samples
B D. Viers, Barry J. Bauer, Y A. Akpalu, F Groehn, Da-Wei Liu, G Kim
Hydrogels were formed by endlinking telechelic vinyl sulfone end-functionalized poly(ethylene glycol) with the terminal amines on dendrimers of different generation. These structures are unique in that the dendrimer crosslink sites were very large, and
Jan Genzer, E Sivaniah, E K. Kramer, J G. Wang, H Kerner, M Xiang, K Char, Christopher K. Ober, B M. DeKoven, Robert A. Bubeck, M K. Chaudhury, S Sambasivan, Daniel A. Fischer
The surface molecular orientation of a liquid crystalline (LC) layer made up a semi-fluorinated (SF) single side-groups [-CO-(CH 2) x-1-(CF 2) yF] (single SF groups) attached to polyisoprene homopolymer or the isoprene block of a styrene-isoprene diblock
E J. Gonzalez, John E. Bonevich, Gery R. Stafford, Grady S. White, Daniel Josell
Thermal transport properties of multilayer thin films both normal and parallel to the layers were measured. Al/Ti multilayer films 3 m thick, with individual layers systematically varied from 2.5 to 40 nm, were studied on Si substrates. Layers ofAl and Ti
T M. Regan, D C. Harris, D W. Blodgett, K C. Baldwin, J A. Miragliotta, M E. Thomas, M J. Linevsky, J W. Giles, R M. Stroud, T A. Kennedy, M Fatemi, David R. Black
Neutron irradiation of sapphire with 1 x 10 18 neutrons (≥ 1 MeV)/cm 2 increases the c-axis compressive strength by a factor of 3 at 600 C. The mechanism of strength enhancement is the retardation of r-plane twin propagation by radiation-induced defects
A brief survey is given of mechanisms of subcritical crack growth in ceramics, for a solicited article in Encyclopedia of Materials: Science and Technology.
The Ceramic Coatings Metrology Workshop was held at NIST to identify the measurement needs of the various industries that manufacture and use ceramic coatings. The industrial perspectives were complemented by reviews of the scientific issues that require
Winnie K. Wong-Ng, Lawrence P. Cook, W Greenwood, Anthony J. Kearsley
The subsolidus equilibria and the primary phase field (crystallization field) of the 110K high T c (Bi,Pb)-2223 ([Bi,Pb]:Sr:Ca:Cu) superconductor in the presence of Ag have been determined under 7.5 volume % O 2 (92.5 % Ar). A total of 29 six-phase volumes
Elastic Modulus is commonly measured by vibrating prismatic specimens at their natural frequency. The elastic modulus is calculated from the frequency, mass and physical dimension of the beam. The calculations assume that the bar is perfectly rectangular
It is generally agreed that measurements and standards play an integral role in the manufacture of ceramic materials. They enhance reliability by providing a basis for quantifying and comparing material properties during each phase of the manufacturing
A R. Moodenbaugh, B Nielson, S Sambasivan, Daniel A. Fischer, T Friessnegg, S Aggarwal, R Ramesh, B Pfeffer
The oxygen K near edge x-ray absorption fine structure (NEXAFS) of polycrystalline and film La1-xSrxCoO3-d at room temperature was studied using fluorescence yield techniques. The bulk sensitive nature of fluorescence yield (relative to electron yield)
Yeon-Gil G. Jung, I M. Peterson, D H. Kim, Brian R. Lawn
Indentation damage and associated strength degradation from multi-cycle contacts with spherical indenters in water are evaluated in four dental ceramics, to examine the hypothesis that the lifetimes of dental restorations are limited by the accumulation of
A powder x-ray diffraction method has been developed to measure the volume fraction of (111), (100), and randomly oriented PZT in 200 nm thick films used for FRAM applications. The integrated and peak intensities of 100, 110, 200 and 222 Bragg peaks from
New calcium tantalate polytypes, with weberite related structures have been prepared by doping Ca 2Ta 2O 7 with Sm 2Ti 2O 7. Trigonal 6-layer (6T) and monoclinic 5-layer (5M) polytypes containing approximately equal to} 6 mol % and 10 mol % respectively of