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Chemistry

Analytical chemistry

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Displaying 576 - 600 of 4041

Accelerated Weathering Parameters for Some Aromatic Engineering Thermoplastics

May 24, 2019
Author(s)
Li Piin Sung, James E. Pickett, Olga Kuvshinnikova, Brett Ermi
Samples of polycarbonate (PC), poly(butylene terephthalate) (PBT), a PC/PBT blend, and poly(styrene-co-acrylonitrile) (SAN), all containing 3 % TiO2 (by mass), were exposed in the NIST (National Institutes of Standards and Technology) SPHERE (Simulated

Health Assessment Measurements Quality Assurance Program: Exercise 2 Final Report

May 21, 2019
Author(s)
Charles A. Barber, Jeanice M. Brown Thomas, Carolyn Q. Burdette, Johanna Camara, Stephen E. Long, Melissa M. Phillips, Benjamin J. Place, Catherine A. Rimmer, Laura J. Wood, Lee L. Yu
The NIST Health Assessment Measurements Quality Assurance Program (HAMQAP) was launched in collaboration with the National Institutes of Health (NIH) Office of Dietary Supplements (ODS) in 2017. HAMQAP was established to enable laboratories to improve the

Practical Guides for X-Ray Photoelectron Spectroscopy: First Steps in Planning, Conducting, and Reporting XPS Measurements

May 15, 2019
Author(s)
Cedric J. Powell, Donald R. Baer, Kateryna Artyushkova, Christopher R. Brundle, James E. Castle, Mark Engelhard, Karen Gaskell, John Grant, Richard Haasch, Matthew Linford, Peter Sherwood, Vincent Smentkowski, Alexander Shard
Over the past three decades, the use of x-ray photoelectron spectroscopy (XPS) in research and applications has grown to make XPS the most popular method of surface analysis. There has also been an increase in the number of new or inexperienced users along

Certification of Standard Reference Material 3389 Ginsenoside Calibration Solution

May 10, 2019
Author(s)
Walter B. Wilson, Lane C. Sander, Benjamin J. Place, James H. Yen
Standard Reference Material (SRM) 3389 is intended as a calibration solution for use for the determination of ginsenosides in natural matrix samples. A unit of SRM 3389 consists of two different ampule solutions: (1) four ampules of a six-component mixture

Interlaboratory Comparison of Hydrogen-Deuterium Exchange Mass Spectrometry (HDX-MS) MMeasurements of the Fab fragment of NISTmAb

May 2, 2019
Author(s)
Jeffrey W. Hudgens, Ioannis L. Karageorgos, Elyssia S. Gallagher, Kyle W. Anderson, James J. Filliben, Richard Y. Huang, Guodong Chen, Michael J. Chalmers, Benjamin T. Walters, Jennifer Zhang, John Venable, Caitlin Steckler, In Hee Park, Ansgar Brock, Xiaojun Lu, Ratnesh Pandey, Arun Chandramohan, Ganesh Srinivasan Anand, Sasidhar N. Nirudodhi, Justin Sperry, Jason C. Rouse, James A. Carroll, Kasper D. Rand, Ulrike Leurs, David D. Weis, Mohammed A. Al-Naqshabandi, Tyler S. Hageman, Patrick Wintrode, John D. Lambris, Sarah Urata, George M. Bou-Assaf, Alfonso Espada
Hydrogen-deuterium exchange mass spectrometry (HDX-MS) is an established, powerful tool for investigating protein-ligand interactions, protein folding, and protein dynamics. However, HDX-MS is still an emergent tool for quality control of

A Synchrotron X-ray Micro-Spectroscopy Study of the Explosive Melt Glass Derived From the Trinity Nuclear Test

April 28, 2019
Author(s)
Bruce D. Ravel, Daniel E. Crean, Daniel J. Bailey, M. C. Stennett, Claire L. Corkhill, Ryan Tappero, N. C. Hyatt
Trinitite, the explosive melt glass derived from the Trinity nuclear test, is of interest as a model material for nuclear forensics investigation. However, there remains uncertainty as to the mechanism of trinitite formation. In this study, new insight is

Review of the National Institute of Standards and Technology Research Program in Trace Contraband Detection

April 14, 2019
Author(s)
J Greg Gillen, Jennifer R. Verkouteren, R. Michael Verkouteren, Marcela Najarro, Edward Sisco, Matthew Staymates, Jessica L. Staymates, Robert A. Fletcher, Jeffrey Lawrence, Elizabeth Robinson, Alexander T. Bulk, Joe Bennett, Shin Muramoto, Thomas Forbes
Current national priorities in homeland security have led to an unprecedented level of utilization of explosives trace detection (ETD) systems for counterterrorism and law enforcement. Despite the widespread deployment of ETD instruments at airports

Examining the Relationships Between Blubber Steroid Hormone and Persistent Organic Pollutant Measurements in Common Bottlenose Dolphins

March 24, 2019
Author(s)
Thomas M. Galligan, Brian C. Balmer, Lori Schwacke, Jennie L. Bolton, Brian M. Quigley, Patricia Rosel, Gina M. Ylitalo, Ashley Russell
In this study, we use remotely collected blubber samples from common bottlenose dolphins (Tursiops truncatus) inhabiting the waters near a U.S. Environmental Protection Agency Superfund site with high local DDx concentrations, to study the impacts of DDx
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