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The National Institute of Standards and Technology (NIST, Gaithersburg, MD) and The Naval Research Laboratory (NRL, Washington, DC) jointly hosted a workshop entitled Pulsed Laser Deposition (PLD) Technological Barriers: Research Needs and Opportunities
The phase transformation behavior and physical properties of the technologically important PbZr 1-xTi xO 3 (PZT) solid solution series are of great interest. For example, the large piezoelectric response of PZT (x = 0.45) makes this compound suitable for
T J. Haugan, Winnie Wong-Ng, Lawrence P. Cook, L Swartzendruber, H J. Brown, D T. Shaw
Efforts to improve the magnetic flux-pinning properties of Bi 2Sr 2Ca 1Cu 20 8 +δ /Ag (2212/Ag) tape conductors utilizing (Srd1-x^Ca x)14Cu 240 41+δ (014x24) and Srd2^CaA1 20 6 (03A1 2) defects are described. Precursor powders with composition (2212 + N
The diametral compression (or Brazilian disk) test is a useful method for determining the tensile strength of ceramic materials. This test method has been utilized periodically over the past fifty years. The state of stress has been confirmed by theory of
S C. Glotzer, Y Gebremichael, N Lacevic, T B. Schroder, Francis W. Starr
We describe the application of statistical mechanical framework, originally developed to describe critical phenonema, to the problem of dynamic criticality associated with the glass transition of various materials.
Gravity can affect the physical vapor growth of mercuric iodide in two distinct ways. First, gravity will induce convection during growth, which strongly mixes residual impurities and any elementary gases resulting from imperfect stoichiometry, either of
P Pei, J Anderson, M C. Bhardwaj, Dennis B. Minor, T Thornton
Green body density measurement techniques were investigated and compared. The measurement techniques investigated include mass-volume measurement, mercury pycnometry, powderdisplacement pycnometry, and noncontact ultrasonic method. Samples studied include
D M. Saylor, B S. El-Dasher, Y Pang, H M. Miller, P Wynblatt, Anthony D. Rollett, G S. Rohrer
Three-dimensional interfacial networks in polycrystalline solids are topologically and crystallographically complex. With a few notable exceptions, most of what we know about the distribution of three-dimensional grain shapes has been derived from foams or
Roughness enhances hydrophobicity of a solid surface leading to high contact angles with water. To achieve low contact angle hysteresis along with a high contact angle, superhydrophobic surfaces should form composite interface (CI) with air pockets in the
Since the 1980s, the pace of technology innovations has accelerated exponentially. The advent of high efficiency yet environmental friendly diesel engine technology, micro-electro-mechanical devices (MEMs), better and more durable biomaterials, and ever
This paper attempts to describe the importance of standards in helping to bring new materials to the market place. Using ceramic materials as an example, the different ways that standards can be important in the materials development process are outlined
The materials community in both science and industry use crystallographic data models on a daily basis to visualize, explain, and predict the behavior of chemicals and materials. Access to reliable information on the structure of crystalline materials
Ultra-small-angle X-ray scattering data were obtained from single-crystal aluminum samples deformed in situ to strains up to 13%. The data are consistent with recent theoretical predictions, allowing quantitative microstructural parameters to be extracted
Ultra-small-angle x-ray scattering data were obtained from a single-crystal Al sample deformed in situ at strains up to 18 %. High sensitivity to the resulting dislocation structure evolution was observed. The data are consistent with theoretical
Limin Sun, Laurence C. Chow, Shozo Takagi, Elena F. Burguera, Stanislav Frukhtbeyn
This study investigated the effects of particle size on the hydrolysis reaction of DCPD at pH 7 and 37 C and on the setting properties of a TTCP/DCPD cement. The kinetics of the hydrolysis reaction was controlled by a nucleation and growth mechanism
Adhesion force has a significant effect upon the contact of rough surfaces with nanoscale asperities. The dominant component of the adhesion force is the capillary force caused by condensed water menisci. The capillary force depends upon the meniscus shape
It is generally believed that liquid phase sintering of silicon nitride invariably results in a continuous intergranular phase such that individual grains are separated by a glassy interphase, typically as thin as I nm. To the contrary, results presented
A proof-of-concept study is presented for a new force transducer and associated calibration method that provides a path for quantitative friction measurements using a Lateral Force Microscope. The transducer design is an Atomic Force Microscope (AFM)
This paper reviews lifetime prediction methodologies for high-temperature structural ceramics. The methodologies consider failure from subcritical crack growth at low temperatures, 800 C to 1000 C, and creep, or creep-rupture at high temperatures. The
Amol Jadhav, N P. Padture, Eric Jordan, Maurice Gell, Pilar Miranzo, Lin-Sien H. Lum
The solution precursor plasma spray (SPPS) process has been used to deposit ZrO2-7wt%Y2O3 (7YSZ) thermal barrier coatings (TBCs) that contain alternate layers of low and high porosities (layered-SPPS). The thermal conductivity of the layered-SPPS coating
A self-consistent, single-valued representation of the major physical, mechanical, and thermal properties of a sintered Α-SiC is presented. This comprehensive set of properties is achieved by focusing on a narrowly defined material specification in which
Brian R. Lawn, Antonia Pajares, P Miranda, Y N. Deng
A survey of recent advances in the analysis of ceramic-based layer structures for biomechanial applications is presented. Data on model layer systems, facilitating development of explicit fracture mechanics relations for predicting critical loads to
Elastic constants must be obtained by experiment methods. Materials are too complicated and theory of solids insufficiently sophisticated to obtain accurate theoretic determinations of elastic constants. Usually, simple static mechanical tests are used to
D M. Saylor, B S. El-Dasher, B L. Adams, G S. Rohrer
A stereological method is described for estimating the distribution of grain boundary types in polycrystalline materials over the five macroscopically observable parameters on the basis of observations from a single planar section. The grain boundary
Grady S. White, Lin-Sien H. Lum, Stephen W. Freiman
This chapter is intended to provide the reader with a general understanding of why brittle materials fail in a time-dependent manner in service and how to estimate the lifetimes that can be expected for such materials. In addition, we describe procedures