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Vivek M. Prabhu, Vytautas Reipa, Adam Rondinone, Peter V. Bonnesen, Eric Formo
An in situ electrochemical small-angle neutron scattering (eSANS) method was developed to measure simultaneously the redox properties and size, shape and interactions of solution-dispersed nanomaterials. By combining multi-step potentials and
Jochen I. Campo, Yanmei Piao, Stephanie Lam, Christopher Stafford, Jason K. Streit, Jeffrey R. Simpson, Angela R. Hight Walker, Jeffrey Fagan
Chemical control of the endohedral volume of single-wall carbon nanotubes (SWCNTs) via liquid-phase filling is demonstrated to be a facile strategy to controllably modify properties of the nanotubes in manners significant for processing and proposed
This work demonstrates controlled bottom-up nickel filling of Through Silicon Vias based on the coupling of suppression breakdown and surface topography. Deposition was performed in a NiSO4 + NiCl2 + H3BO3 electrolyte with a branched polyethyleneimine
Nathan Mahynski, Lorenzo Rovigatti, Christos Likos, Athanassios Panagiotopoulos
Globally ordered colloidal crystal lattices have broad utility in a wide range of optical and catalytic devices, for example, as photonic bandgap materials. However, the self-assembly of stereospecific structures is often confounded by polymorphism. Small
Thien Q. Phan, Lyle E. Levine, I-Fang Lee, Jonathan Z. Tischler, Ruqing Xu, Yi Huang, Terrance G. Langdon, Michael E. Kassner
Synchrotron X-ray microbeam diffraction was used to measure the full elastic long range internal strain and stress tensors of low dislocation density regions within the submicrometer grain/subgrain structure of equal-channel angular pressed (ECAP) AA1050
Yvonne B. Gerbig, Chris A. Michaels, Robert F. Cook
The pressure induced phase transitions of crystalline Si films was studied in situ under a Berkovich probe using the Raman spectroscopy-enhanced instrumented indentation technique. The observations suggested strain and time as important parameters in the
Youngung Jeong, Mark A. Iadicola, Thomas H. Gnaeupel-Herold, Adam A. Creuziger
Constitutive behaviors of an interstitial-free steel sample were measured using an augmented Marciniak experiment. In these tests, multiaxial strain field data of the flat specimens were measured on the basis of the digital image correlation technique. In
Gery R. Stafford, Matthew R. Fayette, Ugo Bertocci
Cantilever curvature was used to examine stress generation during the electrodeposition of Co from 0.1 M NaClO4 + 0.001 M Co(ClO4)2 (pH = 4.8) in films measuring less than 100 nm in thickness. The stress-thickness product showed a -0.2 N/m compression in
Nanoparticle stabilizer type, casting solution additives, and nanoparticle processing by centrifugal or magnetic separation were varied, and specific membrane characteristics were evaluated. Specifically, membrane casting solution viscosity, cast membrane
Li Piin Sung, Justin Gorham, Deborah Jacobs, Savelas A. Rabb, Lee L. Yu, Tinh Nguyen
Temperature effect on the kinetics of photodegradation, surface accumulation of nanoparticles, and nanoparticle release in an epoxy nanocoating exposed to ultraviolet light (UV) was investigated. A model epoxy coating containing 5 % untreated nanosilica
We discuss the precision of 1D chemical-shift-based 1H spin diffusion NMR experiments as well as straightforward experimental protocols for reducing errors. The 1H spin diffusion NMR experiments described herein are useful on samples that contain
The importance of particle shape in affecting the behaviour of powders and other particulate systems has long been recognised, but until fairly recently particle shape information has been rather difficult to obtain and use compared to its more well-known
Stephanie L. Miller, Erik A. Pfeif, Andrei F. Kazakov, Esther Baumann, Marla L. Dowell
Laser welding has many advantages over traditional joining methods, but remains underutilized. NIST has undertaken an initiative to improve predictions of weldability, reliability, and performance of laser welds. This study investigates butt welding of
Nicholas Clore, Dennis D. Fritz, Wei-Hsun Chen, Maureen E. Williams, John E. Blendell, Carol A. Handwerker
This chapter focuses on a study to develop & validate a surface defect counting procedure to be applied in research on the specific mechanisms responsible for stress relaxation & tin whisker formation in tin films. The current JEDEC standards [1,2] for the
Jan Obrzut, Caglar Dogu Emiroglu, Oleg A. Kirillov, Yanfei Yang, Randolph E. Elmquist
A method is established to reliably determine surface conductance of single-layer or multi-layer atomically thin nano-carbon graphene structures. These can be synthesized by chemical vapor deposition (CVD), epitaxial growth on silicon carbide (SiC)
Increases in computational capability enabled sophisticated materials design to evolve from trial-and-error approaches towards more informed methodologies that require large amounts of data. Expert designed tools and their underlying databases facilitate
Zeeshan Ahmed, Matthew Skorski, Jake Esenther, Abigail E. Miller, Hartings Mathew
3-D printing has captured the imagination of many and has enabled a culture of makers. The ability of this process to generate intricate structures from polymer filaments has led to interest from home enthusiasts as well as laboratory scientists. From a
Sebastian Engmann, Felicia A. Bokel, Hyun W. Ro, Dean M. DeLongchamp, Lee J. Richter
We present a method to study the structural evolution of organic bulk-heterojunctions via real-time, in-situ, steady state photoluminescence (PL). In-situ PL, in combination with real-time transmission and reflection measurements, allowed us to
Lee J. Richter, Hyunbok Lee, Christopher McNeil, Eliot Gann, Lars Thomsen, S. Park, J. Jeong, Z. A. Page, Egle Puodziukynaite, Todd Emrick, Alejandro Briseno, John C. Stephenson, Dean M. DeLongchamp
Market demand for ubiquitous, increased functionality products at low cost (the internet of things) is spurring development in additive, solution processing of electronic devices. Performance in thin-film functional devices, be they transistors, diodes, or
Jae Hyun Kim, Christopher M. Stafford, Yadong Lyu, Li C. Yu, Chiao-Chi Lin, Tinh Nguyen, Xiaohong Gu
EVA as an encapsulant material is exposed to various UV irradiation, thermal cycles, and humidity conditions. Degradation of EVA can reduce not only power generation due to yellowing, but also a structural integrity of a PV module. In order to investigate
Dmitry A. Ruzmetov, Kehao Zhang, Gheorghe Stan, Berc Kalanyan, Ganesh R. Bhimanapati, Sarah M. Eichfeld, R A. Burke, Pankaj B. Shah, Terrance P. O'Regan, Frank J. Crowne, A. Glen Birdwell, Joshua A. Robinson, Albert Davydov, Tony G. Ivanov
When designing semiconductor heterostructures, it is expected that epitaxial alignment will facilitate low-defect interfaces and efficient vertical transport. Here, we report lattice-matched epitaxial growth of molybdenum disulfide (MoSub2) directly on
Lawrence Henry Friedman, Mark D. Vaudin, Stephan J. Stranick, Gheorghe Stan, Yvonne B. Gerbig, William Alexander Osborn, Robert F. Cook
The accuracy of electron backscattered diffraction (EBSD) and confocal Raman microscopy (CRM) for small-scale strain mapping are assessed using the multi-axial strain field surrounding a wedge indentation in Si as a test vehicle. The strain field is
Wojtek J. Tutak, Carl Simon Jr., Jyotsnendu J. Giri, Peter Bajcsy
Recent work has shown that osteoprogenitor cell culture on nanofiber scaffolds can promote differentiation. This response may be driven by changes in cell morphology caused by the 3D structure of nanofibers. Herein, we hypothesized that nanofiber effects