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We discuss the precision of 1D chemical-shift-based 1H spin diffusion NMR experiments as well as straightforward experimental protocols for reducing errors. The 1H spin diffusion NMR experiments described herein are useful on samples that contain
The importance of particle shape in affecting the behaviour of powders and other particulate systems has long been recognised, but until fairly recently particle shape information has been rather difficult to obtain and use compared to its more well-known
Stephanie L. Miller, Erik A. Pfeif, Andrei F. Kazakov, Esther Baumann, Marla L. Dowell
Laser welding has many advantages over traditional joining methods, but remains underutilized. NIST has undertaken an initiative to improve predictions of weldability, reliability, and performance of laser welds. This study investigates butt welding of
Nicholas Clore, Dennis D. Fritz, Wei-Hsun Chen, Maureen E. Williams, John E. Blendell, Carol A. Handwerker
This chapter focuses on a study to develop & validate a surface defect counting procedure to be applied in research on the specific mechanisms responsible for stress relaxation & tin whisker formation in tin films. The current JEDEC standards [1,2] for the
Jan Obrzut, Caglar Dogu Emiroglu, Oleg A. Kirillov, Yanfei Yang, Randolph E. Elmquist
A method is established to reliably determine surface conductance of single-layer or multi-layer atomically thin nano-carbon graphene structures. These can be synthesized by chemical vapor deposition (CVD), epitaxial growth on silicon carbide (SiC)
Increases in computational capability enabled sophisticated materials design to evolve from trial-and-error approaches towards more informed methodologies that require large amounts of data. Expert designed tools and their underlying databases facilitate
Zeeshan Ahmed, Matthew Skorski, Jake Esenther, Abigail E. Miller, Hartings Mathew
3-D printing has captured the imagination of many and has enabled a culture of makers. The ability of this process to generate intricate structures from polymer filaments has led to interest from home enthusiasts as well as laboratory scientists. From a
Sebastian Engmann, Felicia A. Bokel, Hyun W. Ro, Dean M. DeLongchamp, Lee J. Richter
We present a method to study the structural evolution of organic bulk-heterojunctions via real-time, in-situ, steady state photoluminescence (PL). In-situ PL, in combination with real-time transmission and reflection measurements, allowed us to
Lee J. Richter, Hyunbok Lee, Christopher McNeil, Eliot Gann, Lars Thomsen, S. Park, J. Jeong, Z. A. Page, Egle Puodziukynaite, Todd Emrick, Alejandro Briseno, John C. Stephenson, Dean M. DeLongchamp
Market demand for ubiquitous, increased functionality products at low cost (the internet of things) is spurring development in additive, solution processing of electronic devices. Performance in thin-film functional devices, be they transistors, diodes, or
Jae Hyun Kim, Christopher M. Stafford, Yadong Lyu, Li C. Yu, Chiao-Chi Lin, Tinh Nguyen, Xiaohong Gu
EVA as an encapsulant material is exposed to various UV irradiation, thermal cycles, and humidity conditions. Degradation of EVA can reduce not only power generation due to yellowing, but also a structural integrity of a PV module. In order to investigate
Dmitry A. Ruzmetov, Kehao Zhang, Gheorghe Stan, Berc Kalanyan, Ganesh R. Bhimanapati, Sarah M. Eichfeld, R A. Burke, Pankaj B. Shah, Terrance P. O'Regan, Frank J. Crowne, A. Glen Birdwell, Joshua A. Robinson, Albert Davydov, Tony G. Ivanov
When designing semiconductor heterostructures, it is expected that epitaxial alignment will facilitate low-defect interfaces and efficient vertical transport. Here, we report lattice-matched epitaxial growth of molybdenum disulfide (MoSub2) directly on
Lawrence Henry Friedman, Mark D. Vaudin, Stephan J. Stranick, Gheorghe Stan, Yvonne B. Gerbig, William Alexander Osborn, Robert F. Cook
The accuracy of electron backscattered diffraction (EBSD) and confocal Raman microscopy (CRM) for small-scale strain mapping are assessed using the multi-axial strain field surrounding a wedge indentation in Si as a test vehicle. The strain field is
Wojtek J. Tutak, Carl Simon Jr., Jyotsnendu J. Giri, Peter Bajcsy
Recent work has shown that osteoprogenitor cell culture on nanofiber scaffolds can promote differentiation. This response may be driven by changes in cell morphology caused by the 3D structure of nanofibers. Herein, we hypothesized that nanofiber effects
Semiconducting single-wall carbon nanotubes (SWCNTs) with long lengths are highly desirable for many applications such as thin film transistors and circuits. Previous reported length sorting techniques usually require sophisticated instrumentations and are
Fangming Xiang, Dorsa Parviz, Tara M. Givens, Ping Tzeng, Eric Davis, Christopher Stafford, Micah J. Green, Jaime C. Grunlan
Since its discovery in 2004, graphene has been intensely studied due to its high elastic modulus, thermal conductivity, electrical conductivity, and gas impermeability. Although it is possible to use small quantities of graphene sheets for fundamental
Various topics taken from the author's research portfolio that involve multicomponent alloy solidification will be reviewed. Topics include: ternary eutectic solidification and Scheil-Gulliver paths in ternary systems. A case study of the solidification of
We explore the coupling between configurational shape of flexible highly-charged polyelectrolytes of variable topology (linear chain, star, unknotted and trefoil ring) and the counter-ion distribution by molecular dy-namics simulations that include an
This guideline presents methods for the preparation and investigation of samples of multiwall carbon nanotube-polymer composites by scanning electron microscopy. It is focused on multiwall carbon nanotube epoxy composite, but the strategy should be
We explore the nature of glass-formation in variable spatial dimensionality (d) based on the generalized entropy theory, a synthesis of the Adam-Gibbs model with direct computation of the configurational entropy of polymer fluids using an established
Guangjun Cheng, Christina A. Hacker, Curt A. Richter, Angela R. Hight Walker
We present an investigation on the etching of graphite catalyzed by the particles produced by dewetting Fe thin films on graphite in forming gas. Raman mapping of the etched graphite shows the thickness variation in the etched channels and reveals that the
Yaakov S. Idell, Lyle E. Levine, Andrew J. Allen, Fan Zhang, Carelyn E. Campbell, Greg Olson, Jiadong Gong, David Snyder
An as-built and solutionized Ni-based super alloy built by additive manufacturing through a direct metal laser sintering technique is characterized to understand the microstructural differences as compared to the as-wrought alloy. The rapid solidification
Eric J. Cockayne, Marek Mihalkovic, Christopher L. Henley
We model the remarkable thin-film Ba-Ti-O structures formed by heat treatment of an initial perovskite BaTiO$_3$ thin film on a Pt(111) surface. All structures contain a rumpled Ti-O network with all Ti threefold coordinated with O, and with Ba occupying
Carl G. Simon Jr., John Test, Michael Yaszemski, Reto Luginbuehl, Anthony Ratcliffe, Paul Tomlins
A Workshop on Standards & Measurements for Tissue Engineering Scaffolds was held on May 21, 2013 and was sponsored by the American Society of Testing and Materials International (ASTM International) in Indianapolis, IN. The purpose of the workshop was to