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On the role of experimental imperfections in constructing 1H spin diffusion NMR plots for domain size measurements

Published

Author(s)

Ryan C. Nieuwendaal

Abstract

We discuss the precision of 1D chemical-shift-based 1H spin diffusion NMR experiments as well as straightforward experimental protocols for reducing errors. The 1H spin diffusion NMR experiments described herein are useful on samples that contain components with significant spectral overlap in the 1H NMR spectrum and also with small masses (
Citation
Solid State Nuclear Magnetic Resonance

Keywords

SOLID-STATE NMR, CRAMPS, DOMAIN SIZE, POLYMER BLEND, COMPOSITE, SPIN DIFFUSION, MISCIBILITY

Citation

Nieuwendaal, R. (2016), On the role of experimental imperfections in constructing 1H spin diffusion NMR plots for domain size measurements, Solid State Nuclear Magnetic Resonance, [online], https://tsapps.nist.gov/publication/get_pdf.cfm?pub_id=919451 (Accessed June 24, 2024)

Issues

If you have any questions about this publication or are having problems accessing it, please contact reflib@nist.gov.

Created March 24, 2016, Updated February 19, 2017