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The availability of certified or reference particle size distributions has become increasingly important for the testing and certification of equipment used in size analysis. We describe here the currently available NIST Standard Reference Materials (SRMs)
A H. Gomoll, A Bellare, W Fitz, T S. Thornhill, R D. Scott, P R. Jemian, Gabrielle G. Long
Poly(methyl methacrylate) (PMMA) based orthopaedic bone cements contain 1-3 micro υ size radiopacifier particles. Incomplete dispersion of these particles leads to the presence of 50-200 micro υ size agglomerates. These large defects are sites of high
Machinable glass ceramics are used to prepare dental restorations with modern dental CAD/CAM systems. Unfortunately, little is understood about the influence of mahining parameters on material removal rates and any damage which could be introduced into the
Wear studies on a glass-ceramic dental restorative material were performed under two types of lubrication conditions with distilled water. In one set of experiments, the contact interface was continuously flushed with fresh water to remove the wear debris
The effect of polydispersity on structure development in linear polyethylenes is studied by simultaneous real time small-angle x-ray scattering (SAXS) and wide-angle x-ray scattering (WAXS). Our measurements show that below 128 degrees C, changes in the
Not only because of its historic and widespread use in applications where its strength and brittle nature are significant factors, but also because it is homogeneous in composition and structure, and isotropic in its properties, glass is an ideal medium in
High resolution monochomatic diffraction imaging is playing a central role in the optimization of novel high energy radiation detectors for superior energy resolution at room temperature. In the early days of the space program, the electronic transport
Fiber-matrix interface strength is known to be a critical factor in controlling the long-term performance of structural composites. This parameter is often obtained by using the average fragment length data generated from the single-fiber fragmentation
The microstructure and chemistry of (Ba,Sr)TiO 3 thin films deposited on Pt/SiO 2/Si substrates by metalorganic chemical vapor deposition were studied using high-resolution transmission electron microscopy and quantitative spectrum imaging in electron
The boundary lubrication characteristics of sulfonates, phenates, and salicylates in a silicon nitride on silicon nitride contact were investigated. The additives were blended at one percent by weight solution in a purified paraffinic base oil and tested
A Lattice Metric Singularity occurs when unit cells defining two (or more) lattices yield the identical set of calculated d-spacings. The existence of such singularities, therefore, has a practical impact on the indexing of powder patterns. For example
J A. Rodriguez, T Jirsak, S Sambasivan, Daniel A. Fischer, A Maiti
In environmental catalysis the destruction or removal of nitrogen oxides (DeNOx process) is receiving a lot of attention. Synchrotron-based x-ray absorption near-edge spectroscopy, high-resolution photoemission, and first-principles density-functional
On June 14, 2000, the New Jersey Center for Biomaterials and the Polymers Division of the National Institute of Standards and Technology (NIST) co-sponsored a one-day workshop on Critical Issues in the Characterization of Polymers for Medical Applications
Gale A. Holmes, Walter G. McDonough, R C. Peterson, Donald L. Hunston
In this paper the nonlinear viscoelastic response of the diglycidyl ether of bisphenol-A (DGEBA)/meta-phenylenediamine (m-PDA) matrix was correlated with changes in the final fragment distribution. The changes in the final fragment distribution were
T J. Haugan, Winnie K. Wong-Ng, Lawrence P. Cook, H J. Brown, L Swartzendruber, D T. Shaw
Investigations into flux pinning of Bi 2Sr 2 CaCu 2O 8+γ /Ag (Bi-2212/Ag) thick film conductors utilizing micron-sized (Sr,Ca) 14Cu 24O 41 and nanophase Al 2O 3 and Au particles are described. Addition of defect particles delayed and reduced formation of
Ultra-small-angle X-ray scattering by dislocations in single-crystal aluminum has been observed in situ as a function of plastic deformation. The scattering is observed to be strongly dependent upon sample orientation, with single dislocations, dislocation
J D. Barnes, R Kolb, K A. Barnes, A Nakatani, Boualem Hammouda
We propose to introduce Temperature-Induced Contrast Variation (TICV) as a technique for improving the specificity of microstructure analyses obtained using small-angle scattering methods. TICV exploits the fact that, at temperatures well below the melting
We examine the stability of polarization switching in polyscrystalline ferroelectric/ferroelastic materials subject to continuous electromechanical loading. In case of unstable switching, a finite change of remanent polarization or strain results from an
D W. Schaefer, T Rieker, M M. Agamalian, J S. Lin, Daniel A. Fischer, S Sukumaran, C I. Chen, G Beaucage, C Herd, J Ivie
We study the structure of colloidal silica and carbon on length scales from 0.25 -1 7 using x-ray, neutron and light scattering. These materials consist of primary particles of the order of 100 , aggregated into micrometer-sized aggregates that in turn are
William R. Blair, Charles M. Guttman, A A. Guiseppetti
Continuing interest at NIST (National Institute of Standards and Technology) in producing MALDI (Matrix Assisted Laser Desorption/Ionization) analyses with a mimimum of sample to sample signal variation has led to the comparison of hand spotting, spin
Gale A. Holmes, Donald L. Hunston, Walter G. McDonough, R C. Peterson
Two of the critical factors controlling the long-term performance and durability of composites in structural applications is the fiber-matrix interfacial shear strength (IFSS) and the durability of the fiber-matrix interface. The single fiber fragmentation
The effect of cyclic hygrothermal aging on a particle-filled, epoxy-based adhesive was studied using a sequence of water absorption, desorption and reabsorption at different temperatures. Moisture sorption characteristics were explored by measuring the
E J. Nelson, Joseph C. Woicik, M Hong, JP Mannaerts
Extended x-ray absorption fine structure (EXAFS) has been used to measure the bond length in a 23 epitaxial Gd 2O 3 film grown on GaAs(001). The Gd-O bond length is determined to be 2.390 0.013 or a bond-length strain of +2.7 0.6 % relative to the bond
Total energy calculations were performed for three perovskite related ordered supercells in several stoichiometries of A(B,B')O 3; where A = Pb 2+, Ba 2+ and B = Mg 2+ Zn 2+, Sc 3+, In 3+ and B' = Nb 5+, Ta 5+, W 6+. A striking difference between the Pb-
Andrew J. Allen, J Ilavsky, Gabrielle G. Long, Jay S. Wallace, C C. Berndt, H Herman
Density, electron microscopy, elastic modulus, and small-angle neutron scattering studies are used to characterize the microstructures of yttria-stabilized zirconis plasma-sprayed deposits as a function fo both feedstock morphology and annealing. In