NOTICE: Due to a lapse in annual appropriations, most of this website is not being updated. Learn more.
Form submissions will still be accepted but will not receive responses at this time. Sections of this site for programs using non-appropriated funds (such as NVLAP) or those that are excepted from the shutdown (such as CHIPS and NVD) will continue to be updated.
An official website of the United States government
Here’s how you know
Official websites use .gov
A .gov website belongs to an official government organization in the United States.
Secure .gov websites use HTTPS
A lock (
) or https:// means you’ve safely connected to the .gov website. Share sensitive information only on official, secure websites.
Joy P. Dunkers, Jospeh L. Lenahrt, J Van Zanten, Richard~undefined~undefined~undefined~undefined~undefined Parnas
The properties of an epoxy/glass interfacial region are studied by covalently grafting a fluorescent probe to the glass surface. A dimethylaminonitrostilbene fluorophore is tethered to a triethoxysilane-coupling agent, generating a fluorescently labeled
The effects of the thickness of the thermally grown oxide on residual thermal stresses in a plasma-sprayed thermal barrier coating were numerically simulated in Part I. In the tip region of a convex asperity, the residual stress normal to the interface,
Rafael L. Bowen, M Farahani, Sabine H. Dickens, Charles M. Guttman
Polymerizable cyclodextrin derivatives (PCDs) have been proposed as candidates for use in dental therapeutics (Bowen, 1996 and Bowen and Reed, 1997). Here PCD libraries were synthosized by quasi-random reactions of 6 moles of methacrylic anhydride plus 7
The viscoelastic and physical aging responses have been analyzed for an amorphous poly(ethylene naphthalate) (PEN) using uniaxial tension stress relaxation experiments. It is known that PEN exhibits a strong β relaxation that overlaps the α relaxation in
Technical activities of the Polymers Division, 854, for the 1999 fiscal year are described. The report is organized by programs: Electronic Packaging, Interconnection and Assembly; Polymer Blends and Processing; Polymer Composites; Polymer Characterization
The perovskite phase SrPbO 3 is important as a buffer and indicator of PbO chemical potential (at fixed p O2 ) according to the reaction: 2 SrPbO 3 --> Sr 2PbO 4 + PbO(g) + 1/2 O2 (g), where the term PbO(g) includes several Pb-containing gaseous species
S D. Kim, E M. Boczar, Barry J. Bauer, A Klein, L H. Sperling
Polystyrene latex film is a model system for the study of interdiffusion in polymers. Small-angle neutron scattering (SANS) and a direct nonradiative energy transfer technique (DET) are widely used to study the interdiffusion of polymers in latex film
The certification of a polyethylene standard reference material, SRM 2886, is described. The Mw of SRM 2886 by light scattering was determined to be 87.0x10+3 g/mol with a sample standard deviation of 2.4 x10+3 g/mol. A combined expanded uncertainty for
Kathleen M. Flynn, S Wetzel, William E. Wallace, William R. Blair, R J. Goldschmidt, David L. VanderHart, B M. Fanconi
NIST has sponsored a matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOF-MS) interlaboratory comparison using a well-characterized polystyrene to determine the reproducibility in determining the molecular mass
The thermal conductivity of porous α-Al 2O 3 specimens prepared using nanosize γ-Al 2O 3 powder or conventional sub-micro a}-alumina powders was studied. Plots of thermal conductivity versus volume fraction porosity showed that both sets of samples
An optical sensor containing polarizing optical components has been constructed for the purpose of monitoring fluorescence anisotropy during polymer processing and for carrying out remote sensing of polymer products doped with fluorescent dyes. The sensor
B D. Viers, Barry J. Bauer, Y A. Akpalu, F Groehn, Da-Wei Liu, G Kim
Hydrogels were formed by endlinking telechelic vinyl sulfone end-functionalized poly(ethylene glycol) with the terminal amines on dendrimers of different generation. These structures are unique in that the dendrimer crosslink sites were very large, and
William E. Wallace, Charles M. Guttman, Joseph M. Antonucci
Matrix-assisted laser desorption ionization time-of-flight mass spectrometry has been shown to be an effective method to determine the degree-of-intramolecular-condensation of polymeric silsesquioxanes. The nature of the organic R' leaving group was found
William E. Wallace, Charles M. Guttman, Joseph M. Antonucci
The degree-of-condensation, defined as the number of residual silanol (SiOH) groups per oligomer, for a variety of silsesquioxane polymers was measured by matrix-assisted laser desorption/ionization time-of-flight mass spectrometry. Condensation of SiOH
Eric J. Amis, Barry J. Bauer, A Topp, F Groehn, T J. Prosa, B D. Viers, Da-Wei Liu, K A. Barnes, C L. Jackson, G Nisato, Alamgir Karim, Jack F. Douglas
This report is a summary of the results of measurement and characterization on dendritically branched polymers that was done under Army Research Office Grant contract 35109-CH. This summary encompasses 3 previous NISTIR's for consecutive 12 month periods
Jan Genzer, E Sivaniah, E K. Kramer, J G. Wang, H Kerner, M Xiang, K Char, Christopher K. Ober, B M. DeKoven, Robert A. Bubeck, M K. Chaudhury, S Sambasivan, Daniel A. Fischer
The surface molecular orientation of a liquid crystalline (LC) layer made up a semi-fluorinated (SF) single side-groups [-CO-(CH 2) x-1-(CF 2) yF] (single SF groups) attached to polyisoprene homopolymer or the isoprene block of a styrene-isoprene diblock
E J. Gonzalez, John E. Bonevich, Gery R. Stafford, Grady S. White, Daniel Josell
Thermal transport properties of multilayer thin films both normal and parallel to the layers were measured. Al/Ti multilayer films 3 m thick, with individual layers systematically varied from 2.5 to 40 nm, were studied on Si substrates. Layers ofAl and Ti
T M. Regan, D C. Harris, D W. Blodgett, K C. Baldwin, J A. Miragliotta, M E. Thomas, M J. Linevsky, J W. Giles, R M. Stroud, T A. Kennedy, M Fatemi, David R. Black
Neutron irradiation of sapphire with 1 x 10 18 neutrons (≥ 1 MeV)/cm 2 increases the c-axis compressive strength by a factor of 3 at 600 C. The mechanism of strength enhancement is the retardation of r-plane twin propagation by radiation-induced defects
A brief survey is given of mechanisms of subcritical crack growth in ceramics, for a solicited article in Encyclopedia of Materials: Science and Technology.
The Ceramic Coatings Metrology Workshop was held at NIST to identify the measurement needs of the various industries that manufacture and use ceramic coatings. The industrial perspectives were complemented by reviews of the scientific issues that require
Winnie K. Wong-Ng, Lawrence P. Cook, W Greenwood, Anthony J. Kearsley
The subsolidus equilibria and the primary phase field (crystallization field) of the 110K high T c (Bi,Pb)-2223 ([Bi,Pb]:Sr:Ca:Cu) superconductor in the presence of Ag have been determined under 7.5 volume % O 2 (92.5 % Ar). A total of 29 six-phase volumes
Elastic Modulus is commonly measured by vibrating prismatic specimens at their natural frequency. The elastic modulus is calculated from the frequency, mass and physical dimension of the beam. The calculations assume that the bar is perfectly rectangular
It is generally agreed that measurements and standards play an integral role in the manufacture of ceramic materials. They enhance reliability by providing a basis for quantifying and comparing material properties during each phase of the manufacturing
A R. Moodenbaugh, B Nielson, S Sambasivan, Daniel A. Fischer, T Friessnegg, S Aggarwal, R Ramesh, B Pfeffer
The oxygen K near edge x-ray absorption fine structure (NEXAFS) of polycrystalline and film La1-xSrxCoO3-d at room temperature was studied using fluorescence yield techniques. The bulk sensitive nature of fluorescence yield (relative to electron yield)
Yeon-Gil G. Jung, I M. Peterson, D H. Kim, Brian R. Lawn
Indentation damage and associated strength degradation from multi-cycle contacts with spherical indenters in water are evaluated in four dental ceramics, to examine the hypothesis that the lifetimes of dental restorations are limited by the accumulation of