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Materials

Projects/Programs

Keyword

Organizational Unit

Metrology for Integration of New Magnetic Materials

Ongoing

Integration of magnetic materials remains a key challenge facing advanced packaging technologies. High power applications require voltage conversion at or near the die, and most practical power converters rely on inductors. Beyond power electronics, integration of magnetic components such as...

Photo of the magnetic moment and susceptibility SRMs - platinum cylinder, YIG sphere, Ni sphere, and Ni disk.

Metrology of Magnetic Materials

Ongoing

Currently, the bulk of this project is focused on three main pieces: Thermal MagIC: An SI-Traceable Method for 3D Thermal Magnetic Imaging and Control Magnetic Refrigeration Magnetic Standard Reference Materials (SRMs) Thermal MagIC (MAGnetic Imaging and Control) is focused on developing new...

Metrology for Nanoimprint Lithography

Completed

Nanoimprint Lithography (NIL) was originally perceived as a versatile, low-cost, and high-resolution patterning alternative for optical lithography in CMOS fabrication. However, it is becoming apparent that NIL has great potential for nanotechnology in general. It is capable of patterning sub-10 nm...

Metrology for Nanolithography

Ongoing

Small Angle Scattering techniques are employed to measure, with sub-nm precision, pattern shape, dimensions, and orientation for structures created in periodic arrays. Critical-Dimension Small Angle X-ray Scattering (CD-SAXS) utilizes the variable-angle transmission scattering from a small beam size...

Microplastic and Nanoplastic Metrology

Ongoing

The Micro and Nanoplastic (MNP) Metrology Project aims to develop a toolbox of methods for size-based separations from complex matrices, chemical characterization protocols, and test materials necessary to enable quantification of micro- and nano-sized plastic particles, a need articulated by our...

Micro-rheometry

Completed

One way to develop small-volume rheology methods that we have used successfully is to start with existing concepts and geometries of rheometry and to then "think small." This approach ensures that we are measuring fundamental materials properties rather than quantities that are experiment and...

Microscopy Methods

Completed

Due to projection effects, analytical transmission electron microscopy (AEM) of thinned or sectioned samples has traditionally been limited to essentially two-dimensional imaging and analysis. Current nanometer scale devices are too small and complex for current sectioning capabilities and two...

A stainless steel micro tensile specimen in a silicon frame.

Microsystems for Harsh Environment Testing

Completed

Classically, measurement of the mechanical properties and reliability of bulk-scale materials is performed with macroscopic specimens and methods. Specimen preparation limitations, miniaturized load-frame tooling problems, and inadequate understanding of the roles of specimen size and constraint on...

Modeling Dispersion Rheology for Non-Spherical Particles

Completed

The goal of this MGI project is to establish an interactive database, generated by sophisticated modeling, such as dissipative particle dynamics and smooth particle hydrodynamics, to compute the rheological properties of polymer composites, where interaction among inclusions, inclusion particle...

Schematic of low-melting point alloy particles (top-left) mixed with a thermoplastic elastomer (top-right) and processed into printable material for fused filament fabrication and pellet extrusion. A filament-based 3D printing setup (lower-left) feeds material through rollers into a heated nozzle, depositing material onto a print bed. A pellet-extrusion setup (lower-right) feeds pellets into a hopper, moves them through a heated barrel, and extrudes through a nozzle onto a bed.

Multifunctional 3D Printable Polymer-Metal Composites

Ongoing

1. Phase-Change Polymer–Metal Composites with Tunable Thermal Conductivity Recent advances in additive manufacturing (AM) have positioned metals and polymers as two key materials. Typically, AM of these two materials involves incompatible methods and conditions. This project addresses that challenge...

Multiparametric Analysis of Network Growth Process via Combined Experimental and Computational Approaches

Ongoing

We have developed techniques that use simultaneous measurements of evolution of multiple polymerization properties combined with computational approaches. In-situ measurements including stress evolution, chemical evolution, and temperature changes during polymerization and computation approaches can...

Multiscale MD-FEM Methodology

Completed

MSED, as a part of the MGI effort within NIST, is developing a multiscale modeling schema, statically coupling finite element modeling (FEM) to atomistic Molecular Dynamics (MD) 1. This methodology allows a far more realistic representation of physical phenomena than that obtained by applying each...

Multiscale structure and dynamics in advanced technological materials

Ongoing

New technologies increasingly harness materials phenomena that operate across many length-scales: e.g., in selective gas adsorption, additive manufacturing, new alloy designs, or advanced concretes. To overcome technology barriers, it is no longer sufficient just to characterize the materials...

Nanocalorimetry Measurements

Ongoing

Accurate thermodynamic measurements are essential to understand fundamental properties of materials, providing direct and quantifiable insight into the thermodynamics of thin film reactions and phase transitions. Going forward, new classes of materials may only be synthesized as thin films, a scale...

Nanometer Scale Measurements of Crack Tips in Glass

Ongoing

Our approach is to fracture glass samples under controlled conditions in order to elucidate fracture mechanisms. Specimen geometries with well-defined fracture mechanics behavior are used to propagate cracks at controlled velocities ranging from 10-11 m s-1 to 102 m s-1. Fracture surfaces are then...

Nanoparticle Assembly in Complex Fluids

Completed

Engineered nanomaterials are promising for technological and medical purposes. However, molecular mechanisms of toxicology are less known. This presents a problem and barrier for future innovation and applications as new nanomaterials are developed for healthcare where particles are intentionally...

Nanoscale Property Measurements by Atomic Force Microscopy

Ongoing

Over the past several decades, Atomic Force Microscopy (AFM) has advanced from a technique used primarily for surface topography imaging to one capable of characterizing a range of chemical, mechanical, electrical, and magnetic material properties with nanometer resolution. Such characterizations...

Nanoscale Spectroscopy for Advanced Electronics, Quantum Materials and Devices

Ongoing

Semiconductor technologies are critical to U.S. economic and national security as they are essential to modern life in communications, healthcare, energy, etc. and also underpin many emerging technologies like quantum, artificial intelligence, high power electronics and advanced wireless (6G+). The...

Nanotube Metrology

Completed

Single-wall carbon nanotubes (SWCNTs) are a tubular form of carbon consisting of a single shell of sp2 bonded carbon with a nanometer scale diameter that have many predicted properties superior to other available materials. However, every production technique for SWCNTs produces many different...

Carbon Nanotubes imaged via Focused Ion Beam Scanning Electron Microscope.

Nanotube Quality Control

Completed

Thermogravimetric analysis (TGA) is widely used to gather data on nanotube chemistry. By monitoring weight loss as a function of temperature, one can determine decomposition kinetics and use this data to closely approximate the distribution of impurities present in a few milligrams of material...

NCAL: Data Management

Ongoing

In the mechanical testing and materials science communities there is not a widely accepted solution for data management of test data. As part of NIST efforts on data archiving, provenance, and availability, we have worked to improve our data practices. We have extended our system beyond many out-of...

NCAL: Diffraction Stress Measurement Under Applied Load

Ongoing

Using X-ray diffraction (XRD) techniques one can measure the full stress tensor just inside the surface of a sheet metal specimen under applied loading. This permits the measurement of biaxial stress states resulting from directly applied deformation (see NCAL: Multiaxial Material Performance) or...

NCAL: Intermediate Strain Rate Testing

Ongoing

This project seeks to improve servohydraulic testing methods at intermediate strain rates by addressing the well-known problems associated with excessive stress oscillations (ringing) that currently limit our understanding of the mechanical behavior of engineering materials for loading conditions...

NCAL: International Documentary Standards Activities

Ongoing

NIST Center for Automotive Lightweighting (NCAL) staff participate in many different international standards committees (e.g. ISO TC 164, ASTM E28 and D30); however, our main focus has been in the mechanical testing of metals and, to a lesser extent, composites. We work on the calibration and...

NCAL: Materials Testing 2.0

Ongoing

The traditional approach to calibrating material models, known as Materials Testing 1.0, is a time-consuming and costly process that requires multiple experiments to be performed on different types of testing equipment. This not only results in high capital costs for testing machines but also leads...

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