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Search Publications by: Rick L. Paul (Fed)

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Displaying 1 - 25 of 78

Certification of Standard Reference Material(R) 2693a Bituminous Coal (Nominal Mass Fraction 0.5 % Sulfur)

January 25, 2024
Author(s)
Thomas W. Vetter, Colleen E. Bryan Sallee, Brian Lang, Anthony F. Marlow, Jennifer Ness, Rick L. Paul, Adam L. Pintar, Bruce Scruggs, Nicholas Sharp, Maria Isabel Vega Martinez, John Sieber
Standard Reference Material (SRM) 2693a Bituminous Coal (Nominal Mass Fraction 0.5 % Sulfur) is intended for use in the evaluation of techniques employed in the determination of sulfur, mercury, chlorine, and ash in coal and materials of a similar matrix

Certification of Standard Reference Material(R) 2386 Avocado Powder

October 18, 2023
Author(s)
Melissa M. Phillips, Laura Wood, Joseph Browning, George Caceres, Grace Hahm, Mahboubeh Hanaee, Abigail Lee, Karen Murphy, Rabia Oflaz, Rick L. Paul, Benjamin Place, Jeanice "Brown Thomas ", James H. Yen
The National Institute of Standards and Technology (NIST) recently released SRM 2386 Avocado Powder which has value assignment for over 70 analytes. This material is intended to be used for the evaluation of methods for the determination of elements

Classification and Authentication of Materials using Prompt Gamma Ray Activation Analysis

July 12, 2023
Author(s)
Nathan Mahynski, Jacob Monroe, David Sheen, Rick L. Paul, Heather H. Chen-Mayer, Vincent K. Shen
Prompt gamma ray activation analysis (PGAA) is a non-destructive nuclear measurement technique that quantifies isotopes present in a sample. Here, we use PGAA spectra to train different types of models to elucidate how discriminating these spectra are for

Certification of Standard Reference Material(R) 1568c Rice Flour

July 29, 2022
Author(s)
Chuck Barber, Colleen E. Bryan Sallee, Monique Johnson, Shaun Kotoski, Rick L. Paul, Nicholas Sharp, Maria Isabel Vega Martinez, James H. Yen, Lee L. Yu, Laura Wood, John Sieber, Stephen Long
The National Institute of Standards and Technology (NIST) recently released SRM 1568c Rice Flour which has value assignments for over 30 analytes, including arsenic species. This material is intended to be used for the evaluation of methods for the

Quantifying and Suppressing Proton Intercalation to Enable High-Voltage Zn-Ion Batteries

November 4, 2021
Author(s)
Fei Wang, Lauren E. Blanc, Qin Li, Antonio Faraone, Xiao Ji, Huaiyu H. Chen-Mayer, Rick L. Paul, Joseph Dura, Enyuan Hu, Kang Xu, Linda F. Nazar, Chunsheng Wang
We explore the Zn-ion intercalation mechanisms/interfacial dynamics of VPO 4F and quantify the water dynamics in water-in-salt (WISE) and hybrid aqueous-non aqueous electrolytes (HANEs). We demonstrate that H + intercalation dominates electrochemical

Certification of Standard Reference Material(R) 2386 Avocado Powder

October 20, 2021
Author(s)
Melissa M. Phillips, Laura J. Wood, George Caceres, Grace Hahm, Karen E. Murphy, Rick L. Paul, Benjamin Place, James H. Yen
The National Institute of Standards and Technology (NIST) recently released SRM 2386 Avocado Powder which has value assignment for over 70 analytes. This material has certified values assigned for 22 analytes and non-certified values assigned for 53

Hidden Complexity in the Chemistry of Ammonolysis-Derived "gamma-Mo2N": An Overlooked Oxynitride Hydride

September 14, 2021
Author(s)
Rick L. Paul, Shobhit A. Pandey, Chi Zhang, Daniah H. Ibrahim, Elise A. Goldfine, Jill K. Wenderott, Roberto dos Reis, Ionnis Spanopoulos, Mercouri Kanatzidis, Michael J. Bedzyk, Vinayak P. Dravid, Gabriela B. Gonzalez, Sossina M. Haile
Molybdenum nitrides have been employed in a variety of catalysis and electronic applications. For use in catalysis, the cubic  phase with nominal stoichiometry Mo2N and space group Fm3 ̅m is typically prepared by high temperature reaction of MoO3 with NH3

Quantitative Analysis of Zirconium Alloys Using Borate Fusion and Wavelength Dispersive X-Ray Fluorescence Spectrometry

January 26, 2021
Author(s)
John R. Sieber, Anthony F. Marlow, Rick L. Paul, Charles A. Barber, Laura J. Wood, Lee L. Yu, Alaina Rieke, Amy Kutnerian, Jessica McCandless, Candace Wallace
The National Institute of Standards and Technology (NIST) uses borate fusion, wavelength dispersive X-ray fluorescence (WDXRF) spectrometry and synthetic calibration standards for high performance, quantitative analyses of a wide range of materials

Niche partitioning of microbial communities at an ancient vitrified hillfort: implications for vitrified radioactive waste disposal

August 30, 2020
Author(s)
Andrew Plymale, Jacqueline Wells, Carolyn Pearce, Colin Brislawn, Emily Graham, Tanya Cheeke, Jessica Allen, Sarah Fansler, Bruce Arey, Mark Bowden, Danielle Saunders, Vincent Danna, Kimberly Tyrrell, Jamie Weaver, Rolf Sjoblom, Rick L. Paul, John McCloy, Eva Hjarthner-Holdar, Mia Englund, Erik Ogenhall, David Peeler, Albert Kruger
A pre-Viking era vitrified hillfort, Broborg, provides a habitat analogue for disposed radioactive waste glass and shows strong niche partitioning among the organisms involved in glass alteration. Microbes cannot be eliminated from radioactive waste

Development of a kelp powder (Thallus laminariae) Standard Reference Material

December 9, 2017
Author(s)
Lee L. Yu, Joseph Browning, Carolyn Q. Burdette, George C. Caceres, Kaitlyn Chieh, William C. Davis, MIchael Ellisor, Brittany Kassim, Stephen E. Long, Karen E. Murphy, Rabia Oflaz, Rick L. Paul, Katherine E. Sharpless, Laura J. Wood, James H. Yen, Rolf L. Zeisler
A Standard Reference Material (SRM) of seaweed, SRM 3232 Kelp Powder (Thallus laminariae) has been developed to support food and dietary supplement measurements in compliance with the Food Safety Modernization Act (FSMA) and the Dietary Supplement Health

Assessment of PGAA capability for low-level measurements of H in Ti alloy

December 1, 2017
Author(s)
Danyal J. Turkoglu, Huaiyu H. Chen-Mayer, Rick L. Paul, Rolf L. Zeisler
The accuracy of low-level hydrogen measurements with prompt gamma-ray activation analysis (PGAA) depends on identifying and accounting for all background H signal, including interfering signals. At the cold-neutron (CN)PGAA facility at the NIST Center for

Multiferroicity in Doped Hexagonal LuFeO 3

August 27, 2015
Author(s)
Steven M. Disseler, Xuan Luo, Bin Gao, Yoon Seok Oh, Rongwei Hu, Yazhong Wang, Dylan Quintana, Alexander Zhang, Qingzhen Huang, June W. Lau, Rick L. Paul, Jeffrey W. Lynn, Sang-Wook Cheong, William D. Ratcliff
The hexagonal phase of LuFeO 3 is a rare example of a multiferroic material possessing a weak ferromagnetic moment, which is predicted to be switchable by an electric field. We stabilize this structure in bulk form through Mn and Sc doping, and determine

Elemental characterization of Single-Wall Carbon Nanotube (SWCNT-1) reference material by neutron and prompt gamma activation analysis

April 7, 2015
Author(s)
Rick L. Paul, Rabia Oflaz, Jan Kucera, J W Bennett, E. A. De Nadai Fernandes, M. Kubesova, M. A. Bacchi, A. J. Stopic, R. E. Sturgeon, P. Grinberg
Instrumental neutron activation analysis with both relative and k0 standardization was used in four experienced laboratories to determine element mass fractions in single-wall carbon nanotube certified reference material (CRM) SWCNT-1. Results obtained

NGD Cold Neutron Prompt Gamma-ray Activation Analysis Spectrometer at NIST

April 1, 2015
Author(s)
Rick L. Paul, Dagistan NMN Sahin, Jeremy C. Cook, Christoph W. Brocker, Richard M. Lindstrom, Donna J. O'Kelly
A new instrument for cold neutron prompt gamma-ray activation analysis (CNPGAA) has been designed and constructed as part of the recent expansion of the cold neutron guide hall at the NIST Center for Neutron Research (NCNR). Located on neutron guide NGD

Physical Properties of LiMn 2-x MxO 4 (M = Ni, Fe) Sol-Gel Nanopowders

December 15, 2014
Author(s)
E. Talik, L. Lipinska, A. Guzik, Pawel Zajdel, M. Michalska, M. Szubka, M. Kadziolka-Gawel, Rick L. Paul
The Pechini sol-gel method was applied to obtain LiMn 2-xT xO 4 (T=Ni, Fe; x = 0.1 to 0.5) nanopowders. Crystal and electronic structures, chemical composition and magnetic properties of the materials were characterized by X-ray diffraction, XPS, SEM/EDX

Incoherent Quasielastic Neutron Scattering Study of the Relaxation Dynamics in Molybdenum-Oxide Based Keplerate Type Nanocages

June 19, 2014
Author(s)
Antonio Faraone, Emiliano Fratini, Somenath Garai, Achim Muller, Madhu Sudan Tyagi, Timothy Jenkins, Eugene Mamontov, Rick L. Paul, John R. Copley, Piero Baglioni
The single particle relaxation dynamics of hydrogen atoms in different oxomolybdate Keplerate type nanocages characterized by a (metal) 30 icosidodecahedron and a size of {approximately equal}25 A were studied using Incoherent Quasielastic Neutron

Dietary Supplement Laboratory Quality Assurance Program: Exercise J Final Report

April 16, 2014
Author(s)
Laura J. Wood, Melissa M. Phillips, Catherine A. Rimmer, Mary Bedner, Kaitlyn Chieh, Rick L. Paul
The NIST Dietary Supplement Laboratory Quality Assurance Program (DSQAP) was established in collaboration with the National Institutes of Health (NIH) Office of Dietary Supplements (ODS) in 2007 to enable members of the dietary supplements community to

Certification of Total Arsenic in Blood and Urine Standard Reference Materials by Radiochemical Neutron Activation Analysis and Inductively Coupled Plasma Mass Spectrometry

March 1, 2014
Author(s)
Rick L. Paul, William C. Davis, Karen E. Murphy, Colleen E. Bryan Sallee, Lee L. Yu, William F. Guthrie, Dennis D. Leber, Thomas W. Vetter
A newly developed procedure for determination of arsenic by radiochemical neutron activation analysis was used to measure arsenic in SRM 955c Toxic Elements in Caprine Blood and SRM 2668 Toxic Elements in Frozen Human Urine for the purpose of providing