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Displaying 251 - 275 of 538

Identification and Quantification of Seven Fused Aromatic Rings C26H14 Peri-Condensed Benzenoid Polycyclic Aromatic Hydrocarbons in a Complex Mixture of Polycyclic Aromatic Hydrocarbons from Coal Tar

March 2, 2016
Author(s)
Jorge O. Ona Ruales, Ruiz-Morales Yosadara, Stephen A. Wise
A methodology for the characterization of groups of PAHs using a combination of Normal Phase Liquid Chromatography with Ultraviolet-Visible Spectroscopy (NPLC/UV-vis) and Gas Chromatography with Mass Spectrometry (GC/MS) was used for the identification and

Long-term stability of carrier-added Ge-68 standardized solutions

March 1, 2016
Author(s)
Brian E. Zimmerman, Denis E. Bergeron, Ryan P. Fitzgerald, Jeffrey T. Cessna
Tests for chemical stability were carried out on carrier-added 68Ge solutions prepared and calibrated in 2007 and 2011 to evaluate the suitability of the specific composition as a potential Standard Reference Material. Massic count rates of the stored

Method Validation and Standards in Hydrogen/Deuterium Exchange Mass Spectrometry

March 1, 2016
Author(s)
Jeffrey W. Hudgens, Richard Y. Huang, Emma D'Ambro
The chapter examines method validation and measurement standards for measuring protein dynamics by hydrogen/deuterium exchange mass spectrometry. Topics examined include the rationale for a reference measurement system for HDX-MS, attaining high accuracy

Development of a Northern Continental Air Standard Reference Material

February 18, 2016
Author(s)
George C. Rhoderick, Duane Kitzis, Michael E. Kelley, Walter R. Miller Jr., Bradley Hall, Edward Dlugokencky, Pieter Tans, Antonio M. Possolo, Jennifer Carney
The National Institute of Standards and Technology (NIST) recently began to develop standard mixtures of greenhouse gases as part of a broad program mandated by the 2009 United States Congress to support research in climate change. To this end, NIST made

Measurement Challenges and Metrology for Monitoring CO2 Emissions from Smokestacks Workshop Summary

January 20, 2016
Author(s)
Aaron N. Johnson, Rodney A. Bryant, Tamae M. Wong, James R. Whetstone, Eric Harman, Woong Kang, Keith A. Gillis, Hsin-Hung Lee, Iosif I. Shinder, Liang Zhang
On April 20-21, 2015, NIST hosted a workshop that, through measurement science, enabled the owners of stationary sources (primarily the electric power industry) and their regulatory agencies (federal and state) to better characterize greenhouse gas (GHG)

SVClassify: a method to use multiple datasets to classify candidate structural variants into true positives and false positives

January 16, 2016
Author(s)
Justin M. Zook, Hemang M. Parikh, Desu Chen, Hariharan K. Iyer, Marc L. Salit, Wolfgang Losert
The human genome contains variants ranging in size from small single nucleotide polymorphisms (SNPs) to large structural variants (SVs). While high-quality benchmark small variant calls have recently been developed by the Genome in a Bottle Consortium, no

ASTM Workshop on Standards & Measurements for Tissue Engineering Scaffolds

January 1, 2016
Author(s)
Carl G. Simon Jr., John Test, Michael Yaszemski, Reto Luginbuehl, Anthony Ratcliffe, Paul Tomlins
A “Workshop on Standards & Measurements for Tissue Engineering Scaffolds” was held on May 21, 2013 and was sponsored by the American Society of Testing and Materials International (ASTM International) in Indianapolis, IN. The purpose of the workshop was to

Potential Stable Low-Permeation Rate Standard Based on Micro-machined Silicon

December 15, 2015
Author(s)
Grady S. White, Adrian Verwolf, Chris M. Poling, Nicholas Barbosa, Nikki S. Rentz
Silicon wafers with micro-machined holes were evaluated for use as low permeation standard artifacts. Accuracy, stability, and reliability were assessed. Two experimental techniques were used: chilled mirror hygrometer and mass loss. The wafers exhibited a

Determination of high-molecular weight polycyclic aromatic hydrocarbons in high performance liquid chromatography fractions of coal tar standard reference material 1597a via solid-phase nanoextraction and laser-excited time-resolved Shpolskii spectr

November 10, 2015
Author(s)
Walter B. Wilson, Bassam Alfarhani, Cristina Bisson, Stephen A. Wise, Andres Campiglia
This article presents an alternative approach for the analysis of high molecular weight – polycyclic aromatic hydrocarbons (HMW-PAHs) with molecular mass 302 Da in complex environmental samples. This is not a trivial task due to the large number of

Double-integrating-sphere system at the National Institute of Standards and Technology in support of measurement standards for the determination of optical properties of tissue-mimicking phantoms

October 27, 2015
Author(s)
Paul Lemaillet, Jeeseong C. Hwang, David W. Allen
There is a need for a common reference point that will allow for the comparison of the optical properties of tissue mimicking phantoms. This paper provides a brief review of the methods that have been used to measure tissue mimicking phantoms. The review

NIST Micronutrients Measurement Quality Assurance Program (Summer 2014 Comparability Studies): Results for Round Robin LXXVI Fat-Soluble Vitamins and Carotenoids in Human Serum and Round Robin 41 Ascorbic Acid in Human Serum

September 29, 2015
Author(s)
Jeanice M. Brown Thomas, David L. Duewer
The National Institute of Standards and Technology coordinates the Micronutrients Measurement Quality Assurance Program (MMQAP) for laboratories that measure fat- and water-soluble vitamins and carotenoids in human serum and plasma. This report describes

NIST Micronutrients Measurement Quality Assurance Program (Winter 2014 Comparability Studies): Results for Round Robin LXXV Fat-Soluble Vitamins and Carotenoids in Human Serum and Round Robin 40 Ascorbic Acid in Human Serum

September 29, 2015
Author(s)
Jeanice M. Brown Thomas, David L. Duewer
The National Institute of Standards and Technology coordinates the Micronutrients Measurement Quality Assurance Program (MMQAP) for laboratories that measure fat- and water-soluble vitamins and carotenoids in human serum and plasma. This report describes

NIST Micronutrients Measurement Quality Assurance Program Winter, Spring, and Fall 1990 Comparability Studies: Results for Round Robins XVIII, XIX, and XX Fat-Soluble Vitamins and Carotenoids in Human Serum

September 29, 2015
Author(s)
Jeanice M. Brown Thomas, David L. Duewer, Margaret C. Kline, Willie E. May, Sam A. Margolis, Neal E. Craft, Katherine E. Sharpless
The National Institute of Standards and Technology coordinates the Micronutrients Measurement Quality Assurance Program (MMQAP) for laboratories that measure fat- and water-soluble vitamins and carotenoids in human serum and plasma. This report describes

NIST Micronutrients Measurement Quality Assurance Program Winter, Spring, and Fall 1991 Comparability Studies: Results for Round Robins XXI, XXII, and XXIII Fat-Soluble Vitamins and Carotenoids in Human Serum

September 29, 2015
Author(s)
Jeanice M. Brown Thomas, David L. Duewer, Margaret C. Kline, Katherine E. Sharpless, Willie E. May, Sam A. Margolis, Neal E. Craft
The National Institute of Standards and Technology coordinates the Micronutrients Measurement Quality Assurance Program (MMQAP) for laboratories that measure fat- and water-soluble vitamins and carotenoids in human serum and plasma. This report describes

An algorithm for compensation of short-period errors in optical encoders

September 24, 2015
Author(s)
Marcus H. Mendenhall, Donald A. Windover, Albert Henins, James P. Cline
We present a simple way to collect data from an optical position or angle encoder with a readout which interpolates values between the optical features, and to process this data set so as to determine the short-range errors which arise from an

Benchmarks for genome sequencing

September 23, 2015
Author(s)
Justin M. Zook, Marc L. Salit
In this issue, Griffith et al. present one of the most comprehensive genome-sequence data sets to date from a patient with myeloid leukemia, including sequencing of normal tissue, primary cancer, and a relapse. Their raw data from a variety of sequencing

Establishing Traceability to NIST SRM 2391c: PCR-Based DNA Profiling Standard

September 16, 2015
Author(s)
Carolyn R. Steffen, Margaret C. Kline, David L. Duewer, Peter Vallone
The NIST Standard Reference Material (SRM) 2391c: PCR-Based DNA Profiling Standard was updated in April 2015 to contain new information relevant to the forensic community. Previously, there were certified genotypes for 24 autosomal STR markers plus

Development of an Ultra-Pure, Carrier-Free 209Po Solution Standard

July 23, 2015
Author(s)
Ronald Colle, Ryan P. Fitzgerald, Lizbeth Laureano-Perez
Ultra-pure, carrier-free 209Po solution standards have been prepared and standardized for their massic alpha-particle emission rate. The standards, which will be disseminated by the National Institute of Standards and Technology (NIST) as Standard

Quantifying and Improving Clinical-grade Coverage and Accuracy using Augmented Exome Sequencing

July 16, 2015
Author(s)
Justin M. Zook, Anil Patwardhan, Marc L. Salit, Carlos Bustamante, Euan Ashley, Michael Snyder, John West, Richard Chen
Exome sequencing is increasingly used for the clinical evaluation of genetic disease, yet accuracy and coverage in medically interpretable parts of the genome remains under-characterized. We evaluate recently developed exome sequencing platforms in the
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