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Materials

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Displaying 1676 - 1700 of 2329

Structure and Dynamics Studies of Concentrated Micrometer-Sized Colloidal Suspensions

January 7, 2013
Author(s)
Fan Zhang, Andrew J. Allen, Lyle E. Levine, Jan Ilavsky, Gabrielle G. Long
We present an experimental study of the structural and dynamical properties of concentrated suspensions of a series of different sized polystyrene microspheres dispersed in glycerol for volume fraction concentrations between 10 % and 20 %. The static

Design and Implementation of Two-Dimensional Polymer Adsorption Models: Evaluating the Stability of Candida Antartica Lipase B at Solid-Support Interfaces by QCM-D

January 4, 2013
Author(s)
Sara V. Orski, Santanu Kundu, Richard Gross, Kathryn L. Beers
A two-dimensional model of a solid-supported enzyme catalyst bead is fabricated on a quartz crystal microbalance sensor to measure in situ stability and mechanical properties of Candida Antartica Lipase B (CAL B) layers under varied conditions relating to

Swelling of ultrathin crosslinked polyamide water desalination membranes

December 27, 2012
Author(s)
Edwin P. Chan, Allison P. Young, Jung-Hyun Lee, Jun-Young Chung, Christopher M. Stafford
We study the water swelling behavior of semi-aromatic crosslinked polyamide ultrathin films in order to characterize the materials properties of the polymer network. Specifically, we utilize X-ray reflectivity and quartz crystal microbalance to measure

Direct Measurement of Intrinsic Dirac Point and Fermi level at Graphene/Oxide interface and Its Band Alignment by Cavity Enhanced Internal Photoemission

December 17, 2012
Author(s)
Kun Xu, Caifu Zeng, Qin Zhang, Rusen Yan, Peide Ye, Kang Wang, Alan C. Seabaugh, Huili G. Xing, John S. Suehle, Curt A. Richter, David J. Gundlach, Nhan V. Nguyen
We report the first direct measurement of the Dirac point, the Fermi level, and the work function of graphene by performing internal photoemission measurements on a graphene/SiO2/Si structure with a unique optical-cavity enhanced test structure. A complete

Atom-Probe Tomographic Study of ?/?' Interfaces and Compositions in an Aged Co-Al-W Superalloy

December 12, 2012
Author(s)
Eric Lass, Kil-Won Moon, Maureen E. Williams, Carelyn E. Campbell, Ursula R. Kattner, David C. Dunand, Peter J. Bocchini, David N. Seidman
Atom-probe tomography (APT) is utilized to investigate, in a Co-9.7Al-10.8W at.% alloy aged at 900 °C for 1000 h, the phase composition and partitioning behavior of the two-phase ɣ(f.c.c.)/ɣ'(L12) microstructure. The APT composition of the ɣ-matrix (Co-8

Standard Operating Procedures for Smolder Ignition Testing of Upholstery Fabrics

December 11, 2012
Author(s)
Rick D. Davis, Mauro Zammarano, Szabolcs Matko, Roland H. Kraemer
This manuscript describes a methodology to measure the influence of an upholstery cover fabric to promote smoldering mass loss of a small-scale mock-up. The primary test metric is total mock-up mass loss after 45 min exposure to the smoldering ignition

Capturing nanoscale in network gels by microemulsion polymerization

December 3, 2012
Author(s)
Kirt A. Page, John Texter, Dustin England
Difficulties in capturing nanoscale structure by polymerizing microemulsions have persisted with the use of thermal initiation. Bicontinuous microemulsion polymerization with reactive surfactant monomer and cross-linker was done with only a 20% increase in

High-energy Ultra-Small Angle X-ray Scattering Instrument at the Advanced Photon Source

December 1, 2012
Author(s)
Andrew J. Allen, Lyle E. Levine, Fan Zhang, Gabrielle G. Long, Jan Ilavsky, Pete R. Jemian
This paper reports recent tests performed on the Bonse-Hart-type ultra-small angle X-ray scattering (USAXS) instrument at the Advanced Photon Source with higher-order reflection optics — Si (440) instead of Si (220) — and with X-ray energies greater than

Molecular beam growth of graphene nanocrystals on dielectric substrates

November 27, 2012
Author(s)
Daniel Fischer, Ulrich Wurstbauer, Theanne Schiros, Cherno Jaye, A. S. Plaut, R. He, Albert Rigosi, Liuyan Zhao, Christopher Gutierrez, P. Kim, L. N. Pfeiffer, A. Pasupathy, A. Pinczuk, J. M. Garcia
A variety of methods have been reported to create graphene. These include the pervasive mechanical exfoliation of graphite1, as well as methods that obtain large area graphene such as thermal decomposition of SiC2,3, chemical vapor deposition on transition

Formation of Extended Ionomeric Network by Bulk Polymerization of L,D-lactide with Layered Double Hydroxide

November 22, 2012
Author(s)
Edward D. McCarthy, Mauro Zammarano, Douglas M. Fox, Ryan Nieuwendaal, Yeon S. Kim, P H. Maupin, Paul C. Trulove, Jeffrey W. Gilman
We report the formation of an ionomeric network in a poly(L,D-lactide) hybrid nanocomposite, (PLDLA-HYB) during in-situ melt polymerization of L,D lactide in the presence of magnesium/aluminium layered-double-hydroxide (LDH) without added catalyst. The

Capillary Wave Dynamics of Thin Polymer films over Submerged Nanostructures

November 16, 2012
Author(s)
Christopher L. Soles, Hyun W. Ro, K. J. Alvine, Oleg Shpyrko, Yenling Dai, Alec Sandy, Suresh Narayanan
The surface dynamics of thin molten polystyrene films supported by nanoscale periodic silicon line-space gratings were investigated with X-ray photon correlation spectroscopy. Surface dynamics over these nanostructures exhibit high directional anisotropy

Giant piezoelectricity in PMN-PT thin films: Beyond PZT

November 1, 2012
Author(s)
S. H. Baek, M. S. Rzchowski, Vladimir Aksyuk
Micro-electromechanical systems (MEMS) incorporating piezoelectric layers provide active transduction between electrical and mechanical energy, which enables highly sensitive sensors and low-voltage driven actuators surpassing the passive operation of

High temperature thermoelectric properties of p-type skutterudites BaxYbyCo4-zFezSb12

October 23, 2012
Author(s)
Yongkwan Dong, Pooja Puneet, Terry M. Tritt, Joshua Martin, George S. Nolas
Several polycrystalline p-type skutterudites with compositions BaxYbyCo4-zFezSb12, with varied filler concentrations x and y, and z = 1 to 2, have been synthesized by first reacting the constituents and subsequent solid state annealing, followed by
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