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Materials

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Displaying 476 - 500 of 2343

Major to Trace Element Imaging and Analysis of Iron Age Glasses Using Stage Scanning in The Analytical Dual Beam Microscope (Tandem)

June 16, 2022
Author(s)
Edward P. Vicenzi, Thomas Lam, Jamie Weaver, Andrew Herzing, John McCloy, Rolf Sjoblom, Carolyn Pearce
Dark and clear silicate glasses formed during an iron age vitrification event ≈ 1500 years ago at the Broborg hillfort near Uppsala, Sweden have been analyzed using a scanning electron microscope equipped with a micro-X-ray fluorescence (μXRF) spectrometer

Engineering 3D Printed Scaffolds with Tunable Hydroxyapatite

June 15, 2022
Author(s)
Yoontae Kim, Eun Jin Lee, Anthony Kotula, Shozo Takagi, Laurence C. Chow, Styliani Alimperti
Bone grafting is a surgical procedure to bone repair due to trauma or diseases in the craniofacial and dental area. Current limitations of autogenous and allogeneic grafts are often associated with reduced host-graft integration due to geometrical confor

Turning Molecular Springs into Nano-Shock Absorbers: The Effect of Macroscopic Morphology and Crystal Size on the Dynamic Hysteresis of Water Intrusion-Extrusion into-from Hydrophobic Nanopores

June 15, 2022
Author(s)
Pawel Zajdel, David Madden, Robin Babu, Diego Mirani, Nikolay Tsyrin, Luis Bartolome, Eder Amayuelas, David Fairen-Jimenez, Alexander Lowe, Miroslaw Chorazewski, Juscelino Leao, Craig Brown, Markus Bleuel, Victor Stoudenets, Maria Echeverria, Francisco Bonilla, Giulia Grancini, Simone Meloni, Yaroslav Grosu
Controlling the pressure at which liquids intrude (wet) and extrude (dry) into/from nanopore is of paramount importance for a broad range of applications, such as energy conversion, catalysis, chromatography, separation, ionic channels, and many more. To

Evidence that gecko setae are coated with an ordered nanometer-thin lipid film

June 9, 2022
Author(s)
Cherno Jaye, Daniel A. Fischer, Mette Rasmussen, Katinka Holler, Joe Baio, Stanislav Gorb, Tobias Weidner
Motivated by the fascination of gecko adhesion based on the fibrous setae at the tips of their toe pads and their potential for biomimetic applications, the adhesion mechanism has been studied in detail. While the mechanism has been shown to be based on

High Energy X-Ray Diffraction and Small-Angle Scattering Measurements of Hydrogen Fatigue Damage in AISI 4130 Steel

June 4, 2022
Author(s)
Matthew Connolly, May Ling Martin, Peter Bradley, Damian Lauria, Andrew Slifka, Jun-Sang Park, Robert Amaro, Jonathan Almer
Accurate lifetime predictions are critical for repurposing existing pipelines for hydrogen transmission as well as for developing novel steels which are minimally susceptible to lifetime degradation by hydrogen. Ultimately, lifetime prediction models

Assessment of intra-build variations in tensile strength in electron beam powder-bed fusion Ti-6Al-4V part 1: Effects of build height

June 2, 2022
Author(s)
Nicholas Derimow, Alejandro Romero, Aldo Rubio, Cesar Terrazas, Newell Moser, Orion Kafka, Jake Benzing, Francisco Medina, Ryan Wicker, Nik Hrabe
In this work, rectangular blocks of electron beam powder-bed fusion (PBF-EB) additively manufactured (AM) Ti-6Al-4V were built, such that a total of 68 mini-tensile test coupons could be extracted for mechanical testing over a range of build height and

On-the-Fly Autonomous Control of Neutron Diffraction via Physics-Informed Bayesian Active Learning

June 1, 2022
Author(s)
Austin McDannald, Matthias Frontzek, Andrew Savici, Mathieu Doucet, Efrain Rodriguez, Kate Meuse, Jessica Opsahl-Ong, Daniel Samarov, Ichiro Takeuchi, William Ratcliff, A. Gilad Kusne
We demonstrate the first live, autonomous control over neutron diffraction experiments by developing and deploying ANDiE: the autonomous neutron diffraction explorer. Neutron scattering is a unique and versatile characterization technique for probing the

STEM-in-SEM: A Re-Emerging Material Measurement Approach

June 1, 2022
Author(s)
Bob R. Keller, Benjamin Caplins, Jason Holm
Scanning transmission electron microscopy performed in a scanning electron microscope (STEM-in-SEM) is undergoing a striking resurgence, with continuing developments in methodology and hardware, as well as applications to a wide range of materials in

Assessment of intra-build variations in tensile strength in electron beam powder-bed fusion Ti-6Al-4V part 2: Effects of powder mixing

May 31, 2022
Author(s)
Nicholas Derimow, Jake Benzing, Orion Kafka, Newell Moser, Priya Pathare, Michael Walker, Frank DelRio, Nik Hrabe
In Part 2 of this paper series, high-throughput tensile testing and characterization of porosity, microstructure, and oxygen content was carried out on Ti-6Al-4V samples that were fabricated via electron beam powder-bed fusion (PBF-EB) to test our

Engineering Magnetic Anisotropy and Emergent Multidirectional Soft Ferromagnetism in Ultrathin Freestanding LaMnO 3 Films

May 24, 2022
Author(s)
Qinwen Lu, Zhiwei Liu, Qun Yang, Hui Cao, Purnima P. Balakrishnan, Qing Wang, Long Cheng, Yalin Lu, Jian-Min Zuo, Hua Zhou, Patrick Quarterman, Shinichiro N. Muramoto, Alexander Grutter, Hanghui Chen, Xiaofang Zhai
Owing to their small coercive fields and weak magnetic anisotropy, soft ferromagnetic films are extremely useful for nanoscale devices that need to easily switch spin directions. However, they are rare, particularly when a film thickness is reduced to a

Improved Accuracy for Calibrated Mass Distribution Measurements of Bimetallic Nanoparticles

May 23, 2022
Author(s)
Kaleb Duelge, George Mulholland, Antonio Montoro Bustos, Michael Zachariah, Michael Zachariah, John Pettibone
Implementation of hybrid nanoparticles (HNPs), consisting of two different metal components, into applied systems has been hindered by an incomplete understanding of structural and chemical properties responsible for their enhanced, yet inconsistent

Lattice Dynamics in the NASICON NaZr 2 (PO 4 ) 3 Solid Electrolyte from Temperature-Dependent Neutron Diffraction, NMR, and Ab Initio Computational Studies

May 10, 2022
Author(s)
Emily Morgan, Hayden Evans, Kartik Pilar, Craig Brown, Raphaele Clement, Ryo Maezono, Ram Seshadri, Bartomeu Monserrat, Anthony Cheetham
Natrium super ionic conductor (NASICON) compounds form a rich and highly chemically-tunable family of crystalline materials that are of widespread interest because they include exemplars with high ionic conductivity, low thermal expansion, and redox

Assessment of the reason for the vitrification of a wall at a hillfort. The example of Broborg in Sweden

May 9, 2022
Author(s)
Rolf Sjoblom, Eva Hjarthner-Holdar, Carolyn Pearce, Jamie Weaver, Erik Ogenhall, John McCloy, Jose Marcial, Edward Vicenzi, Michael Schweiger, Albert Kruger
It was discovered around 250 years ago that some of the rock material in the walls of some hillforts had been subjected to such high temperature that it had vitrified. This prompted a debate as to the reason for it that is still going on today: did the

Impact of Varying Side Chain Structure on Organic Electrochemical Transistor Performance: A Series of Oligoethylene Glycol-substituted Polythiophenes

April 19, 2022
Author(s)
Shinya Chen, Lucas Flagg, Jonathan Onorato, Lee J. Richter, Christine Luscombe, David Ginger
We study the electrochemical doping/dedoping kinetics, and the organic electrochemical transistor (OECT) performance of a series polythiophene homopolymers with ethylene glycol units in their side chains using both kosmotropic and chaotropic anion
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