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Chemistry

Analytical chemistry

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Displaying 326 - 350 of 4041

A new measurement of the 122Sb half-life

June 5, 2021
Author(s)
Giancarlo D'Agostino, Marco Di Luzio, Nicholas Sharp, Massimo Oddone
Following significant discrepancies observed in rescaling collected 122Sb -peak count rates to a reference time by decay corrections, we looked at the literature supporting the presently recommended 2.7238(2) d 122Sb half-life value. The reading

Combining secondary ion mass spectrometry image depth profiling and single particle inductively coupled plasma mass spectrometry to investigate the uptake and biodistribution of gold nanoparticles in Caenorhabditis elegans

May 20, 2021
Author(s)
Monique Johnson, Joe Bennett, Antonio Montoro Bustos, Shannon Hanna, Andrei Kolmakov, Nicholas Sharp, Elijah Petersen, Christopher Sims, Bryant C. Nelson, Patricia Lapasset
Analytical techniques capable of determining the spatial distribution and quantity (mass and/or particle number) of engineered nanomaterials in organisms are essential for characterizing nano-bio interactions and for nanomaterial risk assessments. Here, we

Environmental Protection Agency Blind Audit 2018

May 17, 2021
Author(s)
Christina Cecelski, Cassie Goodman, Jennifer Carney
The U.S. Environmental Protection Agency (EPA) conducted a blind audit of EPA protocol calibration gas mixtures produced by specialty gas manufactures. The objective was to determine the amount-of-substance fraction (concentration) of the analytes in the

Vitamin D Standardization Program (VDSP) intralaboratory study for the assessment of 25-hydroxyvitamin D assay variability and bias

May 17, 2021
Author(s)
Johanna Camara, Stephen Wise, Christopher T. Sempos, Pierre Lukas, Caroline LeGoff, Stephanie Peeters, Carolyn Burdette, Federica Nalin, Grace Hahm, Ramon Durazo-Arvizu, Adam J. Kuszak, Joyce M. Merkel, E. Cavalier
An intralaborabory comparison study to assess the performance of assays for the determination of serum total 25-hydroxyvitamin D [25(OH)D] was conducted in 2017 as part of the Vitamin D Standardization Program (VDSP). The intralaboratory study consisted of

Decision Tree for Key Comparisons

April 27, 2021
Author(s)
Antonio Possolo, Amanda Koepke, David Newton, Michael R. Winchester
This contribution describes a Decision Tree intended to guide the selection of statistical models and data reduction procedures in key comparisons (KCs). The Decision Tree addresses a specific need of the Inorganic Analysis Working Group (IAWG) of the

Development of an LC-MS/MS Reference Method for the Standardization of Analytical Methods to Measure Lipoprotein(a) in Plasma

April 1, 2021
Author(s)
Santica Marcovina, Noemie Clouet-Foraison, Marlys Koschinsky, Mark Lowenthal, Michael Boffa, Andrew Hoofnagle, Tomas Vaisar
Background: Use of Lipoprotein(a) levels for identification of individuals at high risk for cardiovascular disease is hampered by the high size polymorphism of apolipoprotein(a) which strongly impacts immunochemical methods resulting in discordant values
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