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Chemistry

Analytical chemistry

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Displaying 351 - 375 of 2084

Practical Guides for X-Ray Photoelectron Spectroscopy: First Steps in Planning, Conducting, and Reporting XPS Measurements

May 15, 2019
Author(s)
Cedric J. Powell, Donald R. Baer, Kateryna Artyushkova, Christopher R. Brundle, James E. Castle, Mark Engelhard, Karen Gaskell, John Grant, Richard Haasch, Matthew Linford, Peter Sherwood, Vincent Smentkowski, Alexander Shard
Over the past three decades, the use of x-ray photoelectron spectroscopy (XPS) in research and applications has grown to make XPS the most popular method of surface analysis. There has also been an increase in the number of new or inexperienced users along

Certification of Standard Reference Material 3389 Ginsenoside Calibration Solution

May 10, 2019
Author(s)
Walter B. Wilson, Lane C. Sander, Benjamin J. Place, James H. Yen
Standard Reference Material (SRM) 3389 is intended as a calibration solution for use for the determination of ginsenosides in natural matrix samples. A unit of SRM 3389 consists of two different ampule solutions: (1) four ampules of a six-component mixture

Interlaboratory Comparison of Hydrogen-Deuterium Exchange Mass Spectrometry (HDX-MS) MMeasurements of the Fab fragment of NISTmAb

May 2, 2019
Author(s)
Jeffrey W. Hudgens, Ioannis L. Karageorgos, Elyssia S. Gallagher, Kyle W. Anderson, James J. Filliben, Richard Y. Huang, Guodong Chen, Michael J. Chalmers, Benjamin T. Walters, Jennifer Zhang, John Venable, Caitlin Steckler, In Hee Park, Ansgar Brock, Xiaojun Lu, Ratnesh Pandey, Arun Chandramohan, Ganesh Srinivasan Anand, Sasidhar N. Nirudodhi, Justin Sperry, Jason C. Rouse, James A. Carroll, Kasper D. Rand, Ulrike Leurs, David D. Weis, Mohammed A. Al-Naqshabandi, Tyler S. Hageman, Patrick Wintrode, John D. Lambris, Sarah Urata, George M. Bou-Assaf, Alfonso Espada
Hydrogen-deuterium exchange mass spectrometry (HDX-MS) is an established, powerful tool for investigating protein-ligand interactions, protein folding, and protein dynamics. However, HDX-MS is still an emergent tool for quality control of

A Synchrotron X-ray Micro-Spectroscopy Study of the Explosive Melt Glass Derived From the Trinity Nuclear Test

April 28, 2019
Author(s)
Bruce Ravel, Daniel E. Crean, Daniel J. Bailey, M. C. Stennett, Claire L. Corkhill, Ryan Tappero, N. C. Hyatt
Trinitite, the explosive melt glass derived from the Trinity nuclear test, is of interest as a model material for nuclear forensics investigation. However, there remains uncertainty as to the mechanism of trinitite formation. In this study, new insight is

Review of the National Institute of Standards and Technology Research Program in Trace Contraband Detection

April 14, 2019
Author(s)
J Greg Gillen, Jennifer R. Verkouteren, R. Michael Verkouteren, Marcela Najarro, Edward Sisco, Matthew Staymates, Jessica L. Staymates, Robert A. Fletcher, Jeffrey Lawrence, Elizabeth Robinson, Alexander T. Bulk, Joe Bennett, Shin Muramoto, Thomas Forbes
Current national priorities in homeland security have led to an unprecedented level of utilization of explosives trace detection (ETD) systems for counterterrorism and law enforcement. Despite the widespread deployment of ETD instruments at airports

Examining the Relationships Between Blubber Steroid Hormone and Persistent Organic Pollutant Measurements in Common Bottlenose Dolphins

March 24, 2019
Author(s)
Thomas M. Galligan, Brian C. Balmer, Lori Schwacke, Jennie L. Bolton, Brian M. Quigley, Patricia Rosel, Gina M. Ylitalo, Ashley Russell
In this study, we use remotely collected blubber samples from common bottlenose dolphins (Tursiops truncatus) inhabiting the waters near a U.S. Environmental Protection Agency Superfund site with high local DDx concentrations, to study the impacts of DDx

SURVEY OF PEPTIDE QUANTIFICATION METHODS AND THEIR REPRODUCIBILITY COMPARISON: A CASE STUDY USING OXYTOCIN

March 20, 2019
Author(s)
Chensheng Li, Sitaram Bhavaraju, Jeremy Melanson, Andreas Blomgren, Torgny Rundlof, Eric L. Kilpatrick, Timothy Rudd, Yves Aubin, Kevin Grant, Edward Saravolac, Tursun Kerim, William Sherman, Yukari Nakagawa, Sergi Pavon, Tim Weel, Arunima Pola, Dinesh Chalasani, Stephen Walfish, Fouad Atouf
USP's peptide reference standards content is typically determined using an HPLC assay against an external standard for which the purity was determined by a mass balance approach. To explore the use of other analyti-cal methods, the USP Biologics Department

interlab: A Python module for analyzing interlaboratory comparison data

March 15, 2019
Author(s)
David A. Sheen
interlab was developed as a software tool to perform consensus analysis on spectral data from interlaboratory studies. It is designed to estimate the spread in the spectral data and to identify possible outliers among both spectral populations and

Lipidomics for wildlife disease etiology and biomarker discovery: a case study of pansteatitis outbreak in South Africa

March 5, 2019
Author(s)
John Bowden, Jeremy P. Koelmel, Candice Z. Ulmer, Susan Fogelson, Hannes Botha, Christina M. Jones, Jackie T. Bangma, Theresa M. Cantu, Matthew P. Guillette, Wilmien Luus-Powell, Joseph Sara, Willem J. Smit, Korin Albert, Harmony Miller, Berkley Olsen, Jason A. Cochran, Timothy J. Garrett, Richard A. Yost
Lipidomics is a promising tool to determine biomarkers and elucidate mechanisms associated with anthropogenic-induced stress in wildlife. Therefore, we examine the application of lipidomics for in situ studies on Mozambique tilapia (Oreochromis mossambicus

COMPOSITION DETERMINATION OF LOW-PRESSURE GAS-PHASE MIXTURES BY 1H NMR SPECTROSCOPY

March 4, 2019
Author(s)
Chris Suiter, Mark O. McLinden, Thomas J. Bruno, Jason A. Widegren
1H NMR spectroscopy was used to analyze vapor-phase mixtures of methane and propane at low to moderate pressures. The mixtures were prepared gravimetrically and had low uncertainty in their composition. The primary mixture used for this work had a methane

Analysis of Iron in Water using a Simple LED Spectrophotometer

February 15, 2019
Author(s)
Benjamin J. Place
Access to clean water is a vitally important part of the lives of all people, yet there is often a concern about the contamination of water by heavy metals. The detection and measurement of heavy metals in water can be performed using colorimetric reagents

Headspace Analysis: Purge and Trap

February 15, 2019
Author(s)
Thomas J. Bruno, Megan E. Harries
Headspace analysis is a technique for sampling and examining the volatiles in a solid or liquid sample. The term headspace refers to the volume of vapor above a condensed phase sample. Purge and trap refers to the headspace technique in which volatile

Headspace Analysis: Static

February 15, 2019
Author(s)
Thomas J. Bruno, Megan E. Harries
Headspace analysis is a technique for sampling and examining the volatiles in a solid or liquid sample. The term headspace refers to the volume of vapor above a condensed phase sample. For most headspace analyses, the sample and its associated headspace

ASTM E2677: Web-based International Standard on Limit of Detection for Explosive Trace Detectors (and More) - Opioids and Ozone

February 12, 2019
Author(s)
R M. Verkouteren, Nathanael A. Heckert, Stefan D. Leigh, Edward R. Sisco, James E. Norris, Jeffrey A. Lawrence, Amber Burns
The performance characteristics of explosive and narcotic trace detectors are mission-critical to agencies worldwide that are charged with protection of the public, defense for mass transit and infrastructure, and the safety of first responders. Commercial

A status of temporal trends of persistent organic pollutants in Arctic biota

February 1, 2019
Author(s)
Frank Riget, Anders Bignert, Birgit Braune, Maria Dam, Rune Dietz, Marlene Evans, Norman Green, Helga Gunnlaugsdottir, Katrin S. Hoydal, John Kucklick, Robert Letcher, Derek Muir, Stacy Schuur, Christian Sonne, Stern Gary, Gregg Tomy, Katrin Vorkamp, Simon Wilson
More than 1000 time-series of persistent organic pollutants (POPs) in Arctic biota from marine and freshwater ecosystems some extending back to the beginning of 1980s were analyzed using a robust statistical method. The Arctic area encompassed extended

Proceedings of the First Workshop on Standards for Microfluidics

January 28, 2019
Author(s)
Darwin R. Reyes-Hernandez, Henne van Heeren
In the last two decades, the microfluidics/lab-on-a-chip field has evolved from the concept of micro total analysis systems, where systems with integrated pretreatment and analysis of chemicals were envisioned, to what is known today as lab-on-a-chip
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