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Materials

Materials characterization

Projects/Programs

Keyword

Organizational Unit

NIST Standard Reference Simulation Website

Ongoing

Molecular simulations, in particular Monte Carlo Molecular Simulation and Molecular Dynamics Simulation, are methods for computing the properties of some kind of system, for which the intermolecular interactions are specified via mathematical relationships derived from statistical mechanics. Since...

Open Port Liquid Interface Mass Spectrometry

Ongoing

Rapid screening for chemical traces of explosives and narcotics is widely used to support homeland security and law enforcement. These target compounds span a range of physicochemical properties from organic to inorganic, with preferential ionization pathways in both negative and positive mode...

Optical and Optoelectronic Materials Characterization

Ongoing

Today's electronics have reached a point where sheer computation power has combined form and function as the key driver of large consumer markets. The demand for portable and pervasive electronics with greater functionality promises significant changes over the next decades in how society interacts...

Experimental setup for quantification of Butt welds performance at elevated temperatures.

Performance-based Design for Structures in Fire

Ongoing

This project develops validated computational tools and technical guidance to support performance-based standards for cost-effective fire resistance design and assessment of structures.

Personal Body Armor

Completed

To quantify the impact of mechanical degradation on ballistic fibers, NIST developed a novel device for controlled folding of yarns and woven fabrics. In addition, we developed test protocols that employ single fibers to assess the effect of folding using a recently developed modified single fiber...

Platforms for measuring properties of electrically addressable semiconductor nanocrystals

Ongoing

To determine electro-optical performance of nanocrystals with different surface registries in an ensemble, we have developed strategies to control two key parameters including spatial distribution and orientation of nanocrystals. This allows to electrically probe semiconductor nanocrystals from...

Polymer Advanced Manufacturing and Rheology

Ongoing

The manufacture of polymeric materials, whether from virgin or reclaimed sources, occurs under highly non-equilibrium conditions where temperature and stress fields evolve rapidly. The quality of the materials made from these processes depends not only on the composition of the starting material...

Polymer Formulations

Completed

Bringing new and optimized formulated products to market requires measurements that will allow rapid assessment of the structure and properties of multicomponent mixtures over large parameter spaces. To this end, we are developing microfluidic "lab on a chip" technologies that enable researchers to...

Schematic of selective transport of water, ions, or molecules across a polymer membrane.

Polymer Membranes

Ongoing

In Situ Sorption Measurements We develop and apply coupled techniques to probe chemical interactions during membrane operation: Quartz Crystal Microbalance (QCM) for mass uptake Polarization Modulation Infrared Reflection Absorption Spectroscopy (PM-IRRAS) for chemical speciation In-situ...

Picture of PBD set up for wavelength measurement

Powder Diffraction SRMs

Ongoing

This program strives to produce the highest-quality, traceable powders and other artifacts for x-ray diffraction calibration. (to be completed)

Precision X-ray Emission Line Measurements

Ongoing

Precise knowledge of the shape and position of x-ray emission lines is the basis of connecting x-ray diffraction measurements to the Système Internationale d'Unités (SI), the official worldwide standard for making any measurement. Measurements of position of x-ray emission lines have been made been...

Radioanalytical Metrology

Ongoing

The Group engages in a wide range of methods applicable to the detection and characterization of nuclear materials. The work can benefit environmental studies, waste remediation, naturally occurring radioactivity detection and characterization and general radioanalytical metrology. Expertise in...

Raman Metrology and Instrumentation

Ongoing

Raman spectroscopy/microscopy is a powerful optical technique for rapid, non-destructive, label-free characterization of materials. It works under ambient conditions, often without requirement of any sample preparation. Applications span microelectronics, pharmaceutical, security and fundamental...

Reliability Metrologies for Advanced Electronic Interconnects

Completed

High-performance devices, such as microprocessors and memory chips, are typically composed of structures with strict dimensional tolerances and geometries and are made up of various materials, all in close proximity in a three-dimensional system. Material interactions lead to reliability issues such...

Secondary Ion Mass Spectrometry Ion Source Development

Ongoing

In SIMS, a typical analysis requires <1 % of the surface to be sampled, which minimizes chemical damage in the form of molecular fragmentation due to energetic ion bombardment. Cluster sources such as C 60 and Ar GCIB allow for efficient removal of the damage volume, and by operating the analysis...

Cross section of a SAC solder joint in a BGA, with sketches of potential micro specimens

Small Scale Mechanical Testing

Ongoing

Knowledge of a material’s mechanical properties is key to designing safe and reliable structural components for applications ranging in size from medical implants to large civil engineering structures. Traditionally, a material’s mechanical properties are measured by performing mechanical tests on...

Standard Solution SRMs Provide Traceability for Millions of Measurements

Ongoing

Literally millions of measurements of elemental composition are performed each year worldwide. The vast majority of these measurements depend upon reference materials for establishing traceability of results to the SI. Leveraged through commercial CRM producers, the NIST SRM 3100 series provides an...

Standards Development to Ensure Reliable Breath Analysis in the Field

Ongoing

Numerous volatile organic compounds (VOCs) have been identified in human breath. These compounds can be produced by the body or by organisms in the body (e.g., bacteria or viruses) and provide a non-invasive window into human health. Inexpensive point-of-care devices are being developed to diagnose...

Structural Metrology of Advanced Manufacturing Processes

Ongoing

Understanding material structures in advanced manufacturing is crucial because it enables precise control over material properties, leading to improved performance, efficiency, and cost-effectiveness in production processes. However, this understanding poses many challenges, such as the...

Sub-nanoscale electron microscopy of complex nanostructures

Ongoing

The properties of advance materials are becoming ever more reliant on the ability to manipulate their chemistry and structure at very fine length scales. For example, the relevant feature sizes in state-of-the-art transistors continue to decrease, even as the complexity of the architectures employed...

Surface Desorption Ambient Mass Spectrometry

Ongoing

The Surface and Trace Chemical Analysis Group maintains a range of research avenues into the characterization, analysis, and optimization of various commercial and in-house developed surface desorption ion sources. These research avenues also aim to advance our fundamental understanding of the...

Sustainable Metals Processing and Alloy Development

Ongoing

Foundational measurement science is being developed to support sustainable innovations through alloy design and optimization. The integration of experiments and computational thermodynamics and kinetics tools with mechanistic models enables the prediction of key processing-structure-property...

Synchrotron Resonant Scattering and Diffraction

Ongoing

The Resonant Scattering and Diffraction effort seeks to develop measurements that provide spatial correlations in chemical, electronic, and physical structure in advanced materials. Scattering technology is developed as part of the NIST BNL partnership at the National Synchrotron Light Source II in...

Synchrotron X-ray Absorbance Spectroscopy

Ongoing

The Absorbance Spectroscopy effort seeks to develop measurements that provide details of the local chemical, electronic, and physical structure in advanced materials. Spectrometer technology is developed as part of the NIST BNL partnership at the National Synchrotron Light Source II in Upton, NY...

Synchrotron X-ray Spectroscopic Imaging

Ongoing

Building off technologies and expertise developed in the Synchrotron X-ray Absorption Spectroscopy project, the Spectroscopic Imaging effort seeks to develop measurements that provide spatial mapping of the local chemical, electronic, and physical structure in advanced materials. Technology is...

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