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Materials

Materials characterization

Projects/Programs

Keyword

Organizational Unit

Nanoscale Spectroscopy for Advanced Electronics, Quantum Materials and Devices

Ongoing

Semiconductor technologies are critical to U.S. economic and national security as they are essential to modern life in communications, healthcare, energy, etc. and also underpin many emerging technologies like quantum, artificial intelligence, high power electronics and advanced wireless (6G+). The

Nature of the Threat

Ongoing

"Improving Particle Collection Efficiency of Sampling Wipes used for Trace Chemical Detection", Gillen, Greg and Lawrence, Jeffrey and Sisco, Edward and Staymates, Matthew E. and Verkouteren, Jennifer and Robinson, Elizabeth L. and Bulk, Alexander, Anal. Methods, 14, 581-587 (2022). http://dx.doi

NCAL: Diffraction Stress Measurement Under Applied Load

Ongoing

Using X-ray diffraction (XRD) techniques one can measure the full stress tensor just inside the surface of a sheet metal specimen under applied loading. This permits the measurement of biaxial stress states resulting from directly applied deformation (see NCAL: Multiaxial Material Performance) or

NCAL: Intermediate Strain Rate Testing

Ongoing

This project seeks to improve servohydraulic testing methods at intermediate strain rates by addressing the well-known problems associated with excessive stress oscillations (ringing) that currently limit our understanding of the mechanical behavior of engineering materials for loading conditions

NCAL: International Documentary Standards Activities

Ongoing

NIST Center for Automotive Lightweighting (NCAL) staff participate in many different international standards committees (e.g. ISO TC 164, ASTM E28 and D30); however, our main focus has been in the mechanical testing of metals and, to a lesser extent, composites. We work on the calibration and

Neuromorphic Device Measurements

Ongoing

One type of device that is emerging as an attractive artificial synapse is the resistive switch, or memristor. These devices, which usually consist of a thin layer of oxide between two electrodes, have conductivity that depends on their history of applied voltage, and thus have highly nonlinear

Evolution of Flat-histogram Monte Carlo Simulation

NIST Standard Reference Simulation Website

Ongoing

Molecular simulations, in particular Monte Carlo Molecular Simulation and Molecular Dynamics Simulation, are methods for computing the properties of some kind of system, for which the intermolecular interactions are specified via mathematical relationships derived from statistical mechanics. Since

Open Port Liquid Interface Mass Spectrometry

Ongoing

Rapid screening for chemical traces of explosives and narcotics is widely used to support homeland security and law enforcement. These target compounds span a range of physicochemical properties from organic to inorganic, with preferential ionization pathways in both negative and positive mode

Optical and Optoelectronic Materials Characterization

Ongoing

Today's electronics have reached a point where sheer computation power has combined form and function as the key driver of large consumer markets. The demand for portable and pervasive electronics with greater functionality promises significant changes over the next decades in how society interacts

Experimental setup for quantification of Butt welds performance at elevated temperatures.

Performance-based Design for Structures in Fire - Modeling and Validation

Ongoing

This project develops validated computational tools and technical guidance to support performance-based standards for cost-effective fire resistance design and assessment of structures.

Personal Body Armor

Completed

To quantify the impact of mechanical degradation on ballistic fibers, NIST developed a novel device for controlled folding of yarns and woven fabrics. In addition, we developed test protocols that employ single fibers to assess the effect of folding using a recently developed modified single fiber

Platforms for measuring properties of electrically addressable semiconductor nanocrystals

Ongoing

To determine electro-optical performance of nanocrystals with different surface registries in an ensemble, we have developed strategies to control two key parameters including spatial distribution and orientation of nanocrystals. This allows to electrically probe semiconductor nanocrystals from

Polymer Advanced Manufacturing and Rheology

Ongoing

The manufacture of polymeric materials, whether from virgin or reclaimed sources, occurs under highly non-equilibrium conditions where temperature and stress fields evolve rapidly. The quality of the materials made from these processes depends not only on the composition of the starting material

Polymer Formulations

Completed

Bringing new and optimized formulated products to market requires measurements that will allow rapid assessment of the structure and properties of multicomponent mixtures over large parameter spaces. To this end, we are developing microfluidic "lab on a chip" technologies that enable researchers to

Schematic of selective transport of water, ions, or molecules across a polymer membrane.

Polymer Membranes

Ongoing

We are developing and applying the following advanced tools to measure the structure, dynamics, and performance of polymer-based membranes and sorbents: Vibrational Spectroscopy We have developed a custom-built tandem quartz crystal microbalance (QCM), which measures total mass uptake of adsorbed

Picture of PBD set up for wavelength measurement

Powder Diffraction SRMs

Ongoing

This program strives to produce the highest-quality, traceable powders and other artifacts for x-ray diffraction calibration. (to be completed)

Precision X-ray Emission Line Measurements

Ongoing

Precise knowledge of the shape and position of x-ray emission lines is the basis of connecting x-ray diffraction measurements to the Système Internationale d'Unités (SI), the official worldwide standard for making any measurement. Measurements of position of x-ray emission lines have been made been

Radioanalytical Metrology

Ongoing

The Group engages in a wide range of methods applicable to the detection and characterization of nuclear materials. The work can benefit environmental studies, waste remediation, naturally occurring radioactivity detection and characterization and general radioanalytical metrology. Expertise in

Raman Metrology and Instrumentation

Ongoing

Raman spectroscopy/microscopy is a powerful optical technique for rapid, non-destructive, label-free characterization of materials. It works under ambient conditions, often without requirement of any sample preparation. Applications span microelectronics, pharmaceutical, security and fundamental

Reliability Metrologies for Advanced Electronic Interconnects

Completed

High-performance devices, such as microprocessors and memory chips, are typically composed of structures with strict dimensional tolerances and geometries and are made up of various materials, all in close proximity in a three-dimensional system. Material interactions lead to reliability issues such

Secondary Ion Mass Spectrometry Ion Source Development

Ongoing

In SIMS, a typical analysis requires <1% of the surface to be sampled, which minimizes chemical damage in the form of molecular fragmentation due to energetic ion bombardment. Cluster sources such as C 60 and Ar GCIB allow for efficient removal of the damage volume, and by operating the analysis and

Cross section of a SAC solder joint in a BGA, with sketches of potential micro specimens

Small Scale Mechanical Testing

Ongoing

Knowledge of a material’s mechanical properties is key to designing safe and reliable structural components for applications ranging in size from medical implants to large civil engineering structures. Traditionally, a material’s mechanical properties are measured by performing mechanical tests on

Standard Solution SRMs Provide Traceability for Millions of Measurements

Ongoing

Literally millions of measurements of elemental composition are performed each year worldwide. The vast majority of these measurements depend upon reference materials for establishing traceability of results to the SI. Leveraged through commercial CRM producers, the NIST SRM 3100 series provides an

Standards Development to Ensure Reliable Breath Analysis in the Field

Ongoing

Numerous volatile organic compounds (VOCs) have been identified in human breath. These compounds can be produced by the body or by organisms in the body (e.g., bacteria or viruses) and provide a non-invasive window into human health. Inexpensive point-of-care devices are being developed to diagnose

Structural Metrology of Advanced Manufacturing Processes

Ongoing

Understanding material structures in advanced manufacturing is crucial because it enables precise control over material properties, leading to improved performance, efficiency, and cost-effectiveness in production processes. However, this understanding poses many challenges, such as the

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