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Standards

Reference materials

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Displaying 176 - 200 of 525

Protein Adsorption and Layer Formation at the Stainless Steel - Solution Interface Mediates Shear-Induced Particle Formation for an IgG1 Monoclonal Antibody

February 9, 2018
Author(s)
Cavan K. Kalonia, Frank Heinrich, Joseph E. Curtis, Sid Raman, Maria A. Miller, Steven Hudson
Passage of specific protein solutions through certain pumps, tubing, and/or filling nozzles can result in the production of unwanted subvisible protein particles (SVP). In this work, surface mediated SVP formation was investigated. Specifically, the

Correction of an adding-doubling inversion algorithm for the measurement of the optical parameters of turbid media

January 1, 2018
Author(s)
Paul Lemaillet, Catherine C. Cooksey, Jeeseong Hwang, Heidrun Wabnitz, Dirk Grosenick, Lin Yang, David W. Allen
We present broadband measurements of the optical properties of tissue-mimicking solid phantoms using a single integrating sphere to measure the hemispherical reflectance and transmittance under a direct illumination at the normal incident angle. These

Development of a kelp powder (Thallus laminariae) Standard Reference Material

December 9, 2017
Author(s)
Lee L. Yu, Joseph Browning, Carolyn Q. Burdette, George C. Caceres, Kaitlyn Chieh, William C. Davis, MIchael Ellisor, Brittany Kassim, Stephen E. Long, Karen E. Murphy, Rabia Oflaz, Rick L. Paul, Katherine E. Sharpless, Laura J. Wood, James H. Yen, Rolf L. Zeisler
A Standard Reference Material (SRM) of seaweed, SRM 3232 Kelp Powder (Thallus laminariae) has been developed to support food and dietary supplement measurements in compliance with the Food Safety Modernization Act (FSMA) and the Dietary Supplement Health

Assessment of PGAA capability for low-level measurements of H in Ti alloy

December 1, 2017
Author(s)
Danyal J. Turkoglu, Huaiyu H. Chen-Mayer, Rick L. Paul, Rolf L. Zeisler
The accuracy of low-level hydrogen measurements with prompt gamma-ray activation analysis (PGAA) depends on identifying and accounting for all background H signal, including interfering signals. At the cold-neutron (CN)PGAA facility at the NIST Center for

Characterization of Transmission Lines with Nonlinear Dielectric Materials

November 28, 2017
Author(s)
Aaron M. Hagerstrom, Christian J. Long, Nathan D. Orloff, James C. Booth, Eric J. Marksz
Nonlinear transmission lines are interesting for two broad reasons: first, they have several direct device applications (i.e. harmonic generation, and phase shifters), and second, they provide a way to characterize nonlinear materials at mm-wave

LipidQC: Method Validation Tool for Visual Comparison to SRM 1950 Using NIST Interlaboratory Comparison Exercise Lipid Consensus Mean Estimate Values

November 17, 2017
Author(s)
Candice Z. Ulmer, Jared Ragland, Jeremy P. Koelmel, N. Alan Heckert, Christina Jones, Timothy J. Garrett, Richard A. Yost, John Bowden
As advances in analytical separation techniques, mass spectrometry instrumentation, and data processing platforms continue to spur growth in the lipidomics field, more structurally unique lipid species are detected and annotated. The lipidomics community

SARD: Thousands of Reference Programs for Software Assurance

October 31, 2017
Author(s)
Paul E. Black
A corpus of computer programs with known bugs is useful in determining the ability of tools to find bugs. This article describes the content of NIST's Software Assurance Reference Dataset (SARD), which is a publicly available collection of thousands of

Certification of SRM 2493:Standard Reference Mortar for Rheological Measurements

October 4, 2017
Author(s)
Alex Olivas, Chiara C. Ferraris, Nicos Martys, Edward Garboczi, Blaza Toman, William L. George
Rheological measurements are often performed using a rotational rheometer. In this type of rheometer, the tested fluid is sheared between two surfaces, one of which acts as the rotating surface [1]. Usually, the rotational velocity is imposed and the

Aperture Arrays for Subnanometer Calibration of Optical Microscopes

September 28, 2017
Author(s)
Craig Copeland, Craig McGray, Jon Geist, James Alexander Liddle, Robert Ilic, Samuel Stavis
We fabricate and test subresolution aperture arrays as calibration devices for optical localization microscopy. An array pitch with a relative uncertainty of approximately three parts in ten thousand enables magnification calibration with subnanometer

New thorium-229 standard reference material

July 27, 2017
Author(s)
Richard Essex, Jacqueline L. Mann, Ross W. Williams, William S. Kinman, Amelie Hubert, Megan E. Bennett
A new reference material, preliminarily designated as SRM 3059, was characterized for 229Th molality (mol•g-1) and thorium isotope amount ratios. This SRM is intended for use in nuclear forensic analyses as an isotope dilution mass spectrometry spike. The

Development of Standard Reference Material (SRM) 2973 Vitamin D Metabolites in Frozen Human Serum (High Level)

July 24, 2017
Author(s)
Susan Tai, Michael Nelson, Brian Lang, Karen W. Phinney, Lane C. Sander, James H. Yen, J. M. Betz, Christopher T. Sempos, Stephen Wise
The National Institute of Standards and Technology (NIST), in collaboration with the National Institutes of Health, Office of Dietary Supplements (NIH-ODS) and the Vitamin D Standardization Program (VDSP), has recently issued a new serum-matrix Standard

Development of NIST Standard Reference Material 2082, a Pathlength Standard for Measurements in the Ultraviolet Spectrum

July 10, 2017
Author(s)
Brian Lang, Aaron A. Urbas, Paul C. DeRose, Hung-Kung Liu, John C. Travis, Steven J. Choquette, Kenneth D. Cole
New spectrophotometers and cuvettes have been designed to allow the measurement of absorbance values from samples using microliter volume sizes. These measurements are done using short pathlengths to decrease the sample volumes required. The major

Qualitative characterization of SRM 1597a Coal Tar for polycyclic aromatic hydrocarbons and methyl-substituted derivatives via normal-phase liquid chromatography and gas chromatography/mass spectrometry

June 29, 2017
Author(s)
Walter Wilson, Hugh Hayes, Lane Sander, Andres Campiglia, Stephen Wise
A normal-phase liquid chromatography (NPLC) fractionation procedure was developed for the characterization of a complex mixture of polycyclic aromatic hydrocarbons (PAHs) from a coal tar sample (Standard Reference Material (SRM) 1597a). Using a semi

High-precision measurement of the X-ray Cu K-alpha spectrum

May 12, 2017
Author(s)
Marcus H. Mendenhall, Albert Henins, Lawrence T. Hudson, Csilla I. Szabo-Foster, Donald A. Windover, James P. Cline
The structure of the x-ray emission lines of the Cu Kα complex has been remeasured on a newly commissioned instrument, in a manner directly traceable to the Système Internationale definition of the meter. In this measurement, the region from 8000 to 8100
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