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Aaron M. Katzenmeyer, Vladimir Aksyuk, Andrea Centrone
Photothermal Induced Resonance (PTIR) is a new technique which combines the chemical specificity of IR spectroscopy with the lateral resolution of Atomic Force Microscopy. PTIR requires a pulsed tunable laser for sample excitation and an AFM tip to measure
Jae Hyun Kim, Nathanael A. Heckert, Stefan D. Leigh, Haruki Kobayashi, Walter G. McDonough, Kirk D. Rice, Gale A. Holmes
Single fiber tensile tests using two different gripping methods were carried out on various fiber lengths. One method (the glue-tab grip) consists of mounting a fiber onto a rigid tab as specified in ASTM C1557-03 using an adhesive, while the other (the
William E. Luecke, Stephen Graham, Matthew Adler, Li Ma
Ten commercial laboratories participated in an interlaboratory study to establish the repeatability and reproducibility of compression strength tests conducted according to ASTM International Standart Test Method E9. The test employed a cylindrical
Johanna Camara, Mark S. Lowenthal, Karen W. Phinney
The National Institute of Standards and Technology (NIST) is developing a wide variety of Standard Reference Materials (SRMs) to support measurements of vitamins and other nutrients in foods. Previously, NIST has provided SRMs with values assigned for the
Sherrie R. Elzey, De-Hao D. Tsai, Lee L. Yu, Michael R. Winchester, Michael E. Kelley, Vincent A. Hackley
We report the development of a hyphenated instrument with the capacity to quantitatively characterize aqueous suspended gold nanoparticles (AuNPs) based on a combination of gas-phase size separation, particle counting, and elemental analysis. A customized
As metrologists we are typically subject matter experts (SMEs) in a technical area of measurement. However, most of us are not experts in measuring the value or impact of education and training efforts using standard models for evaluation. This paper will
Catherine A. Remley, Ryan J. Pirkl, Chih-Ming Wang, Haider Shah
We develop methods for assessing the standard uncertainty arising from various combinations of mode-stirring methods used in reverberation-chamber measurements. By use of a straightforward measurement-based technique, the combination of mode-stirring
Measurements of absorbance and fluorescence emission were carried out on aqueous suspensions of polystyrene (PS) microspheres with a diameter of 2.5 µm. Microspheres with and without green BODIPY@ dye were measured. Placing the suspension inside an
Forklifts and automated guided vehicles are useful tools for the manufacturing industry. With regard to safety of workers (and equipment) near industrial vehicles, there are issues when using either manned or automated powered industrial vehicles in
A commercial spectrometer with a 150 mm integrating sphere (IS) detector was used to measure the scattering and absorption cross sections of polystyrene monodisperse microspheres suspended in water. Absorption measurements were performed with the sample
Quantitative leak tests with vacuum technology have become an important tool in industry for safety and operational reasons and to meet environmental regulations. In lack of a relevant key comparison, so far, there are no calibration measurement
James Cline, David R. Black, Donald Windover, Albert Henins
The laboratory X-ray powder diffractometer offers several virtues that have rendered it a principal characterization device providing critical data for a range of technical disciplines. A continuous suite of hkl reflections can be collected with a single
Dazhen Gu, James P. Randa, Robert L. Billinger, Dave K. Walker
We report a verification method for noise-temperature (NT) measurements on cryogenic low-noise amplifiers (LNAs) at liquid helium temperature. The method uses a comparison between the individual measurements of the LNA and an attenuator and the joint
We compare three methods of quantifying illumination efficiency (IE). The ratio IE describes the contribution of energy emitted from a blackbody target to the total energy measured at an antenna aperture in a free-space microwave calibration target
At the National Institute of Standards and Technology a new watt balance, NIST-4, is currently being designed. This apparatus will be used to realize the unit of mass after the redefinition of the SI has taken effect. In order to ensure smooth operation
Yvonne B. Gerbig, Chris A. Michaels, Aaron M. Forster, John W. Hettenhouser, Walter E. Byrd, Dylan J. Morris, Robert F. Cook
Instrumented indentation is a widely used technique to study the mechanical behavior of materials at small length scales and thus has been exploited in particular for metals, ceramics, glasses, and polymers. Mechanical tests of bulk materials, microscopic
David Bishop, Flavio Pardo, Cris Bolle, Randy Giles, Vladimir Aksyuk
Over the last decade or so a group of us, while working at Bell Labs, have been able to develop a large number of silicon micromachines for a wide range of applications. In this article, which is part of a special volume to celebrate the career of
Yoshihiro Nakashima, Michael A. Boss, Stephen E. Russek, John M. Moreland
We have developed a nuclear magnetic resonance (NMR) microcapillary probe for the detection of single magnetic microbeads. The geometry of the probe has been optimized so that the signal from the background water has a similar magnitude compared to the
Christopher W. Meyer, W Wyatt Miller, Dean C. Ripple, Gregory E. Scace
We provide here a detailed uncertainty budget for the new Hybrid Humidity Generator (HHG) that has been constructed at the National Institute of Standards and Technology (NIST). The HHG generates frost/dew points from 70 °C to +85 °C using calibration gas
D Vega-Maza, W. Wyatt Miller, Dean C. Ripple, Gregory E. Scace
We have constructed a new humidity generator that produces gas streams of known moisture content at temperatures from 85 °C to 200 °C, absolute pressures from 0.2 MPa to 1.6 MPa, and relative humidities from 10 % to 90 %. The generator produces a moist gas
We individually characterize and provide uncertainties for a pair of WR-8 rectangular waveguide-to-coplanar waveguide (CPW) probes over a frequency range of 90 to 140 GHz utilizing two methods implemented within the NIST Microwave Uncertainty Framework
Vyacheslav B. Podobedov, George P. Eppeldauer, Thomas C. Larason
Analysis of multiple factors affecting the uncertainty of the absolute spectral responsivity of optical radiation detectors is presented. This includes both the validation of the radiometric scale of the infrared reference detectors and the scale transfer
Historically, mechanical assembly was predicted to be the dominant application domain of industrial robots; yet assembly tasks are still primarily addressed by manual labor. New advances in force control (FC), machine vision, and robot dexterity are