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Metrology

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Displaying 1051 - 1075 of 2718

Does Your SEM Really Tell the Truth? - How would you know? Part 1

December 16, 2013
Author(s)
Michael T. Postek, Andras Vladar
The scanning electron microscope (SEM) has gone through a tremendous evolution to become a critical tool for many and diverse scientific and industrial applications. The high resolution of the SEM is especially suited for both qualitative and quantitative

High-Accuracy Measurements of the Vapor Pressure of Ice Referenced to the Triple Point

December 6, 2013
Author(s)
Katarzyna E. Bielska, Daniel K. Havey, Gregory E. Scace, D Lisak, Allan H. Harvey, Joseph T. Hodges
The vapor pressure of hexagonal (Ih) ice was measured over the temperature range 175 K to 253.4 K and referenced to the value at the triple point of water. This experiment combined a highly accurate humidity generation system containing an ice-coated

Impact of UV Irradiation on the Surface Chemistry and Structure of Multiwall Carbon Nanotube Epoxy Nanocomposites

December 6, 2013
Author(s)
Elijah Petersen, Thomas F. Lam, Justin Gorham, Keana Scott, Chris Long, Deborah Jacobs, Renu Sharma, James Alexander Liddle, Tinh Nguyen
One of the most promising applications of nanomaterials is as nanofillers to enhance the properties of polymeric materials. However, the effect of nanofillers on polymers subject to typical environmental stresses, such as ultraviolet (UV) radiation, high

Certification of Elements in and Use of Standard Reference Material 3280 Multivitamin/Multielement Tablets

December 2, 2013
Author(s)
Gregory C. Turk, Katherine E. Sharpless, Steven J. Christopher, Danielle Cleveland, Russell D. Day, Stephen E. Long, Elizabeth A. Mackey, Anthony F. Marlow, Rick L. Paul, John R. Sieber, Rabia Oflaz, Laura J. Wood, Lee L. Yu, Rolf L. Zeisler, Stephen A. Wise, James H. Yen, E. Greene, J. Harnly, I-P Ho, Joseph M. Betz, R. Q. Thompson, Candace Jongsma
Standard Reference Material (SRM) 3280 Multivitamin/Multielement Tablets was issued by the National Institute of Standards and Technology (NIST) in 2009 and has certified and reference mass fraction values for 13 vitamins, 26 elements, and 2 carotenoids

Quantitative bottom-up proteomics depends on digestion conditions

December 2, 2013
Author(s)
Mark S. Lowenthal, Yuxue Liang, Karen W. Phinney, Stephen E. Stein
Accurate quantification is a fundamental requirement in the fields of proteomics and biomarker discovery, and for clinical diagnostic assays. To demonstrate the extent of quantitative variability in measurable peptide concentrations due to differences

Pressure-Sensitive Sampling Wands for Homeland Security Applications

December 1, 2013
Author(s)
Matthew E. Staymates, Jennifer R. Verkouteren, Jessica Grandner
This work discusses the use of Force Sensing Resistor (FSR) technology for Homeland Security applications. One area of particular focus is the optimization of wipe sampling of surfaces to facilitate enhanced trace contraband collection. Another focus area

Electro-Thermo-Mechanical Model for Bulk Acoustic Wave Resonators

November 30, 2013
Author(s)
Eduard Rocas, Juan C. Collado Gomez, Jordi Mateu, Nathan D. Orloff, James C. Booth, Robert Aigner
We present the electro-thermo-mechanical constitutive relations, expanded up to the third order, for a BAW resonator. The relations obtained are implemented into a circuit model, which is validated with extensive linear and nonlinear measurements. The

Viscosity-ratio measurements with capillary viscometers

November 27, 2013
Author(s)
Robert F. Berg, Eric F. May, Michael R. Moldover
Viscosity-ratio measurements made with capillary viscometers exploit the accurate values of the viscosity of helium calculated ab initio. Accurate values of the argon-to-helium viscosity ratio are now used for primary acoustic gas thermometry and for the

Accurate Spring Constant Calibration for very Stiff Atomic Force Microscopy Cantilevers

November 26, 2013
Author(s)
Scott Grutzik, Richard S. Gates, Yvonne B. Gerbig, Douglas T. Smith, Robert F. Cook, Alan Zehnder
There are many atomic force microscopy (AFM) applications that rely on quantifying the force between the AFM cantilever tip and the sample. The AFM does not explicitly measure force, however, so in such cases knowledge of the cantilever stiffness is

Wavelength Dependent UV Inactivation and DNA Damage of Adenovirus 2 as Measured by Cell Culture Infectivity and Long Range Quantitative PCR

November 22, 2013
Author(s)
Sara E. Beck, Roberto A. Rodriguez, Karl G. Linden, Thomas M. Hargy, Thomas C. Larason, Harold B. Wright
Adenovirus is regarded as the most resistant pathogen to ultraviolet (UV) disinfection due to its demonstrated resistance to monochromatic, low-pressure (LP) UV irradiation at 254 nm. This resistance has resulted in high UV dose requirements for all

Checking the Net Content of Packaged Goods (NIST HB 133-2014)

November 1, 2013
Author(s)
Linda D. Crown, David A. Sefcik, Lisa Warfield
This handbook has been prepared as a procedural guide for the compliance testing of net contents statements on packaged goods. Compliance testing of packaged goods is the determination of the conformance results of the packaging, distribution, and

Optical Coherence Tomography for Dimensional Metrology of Lab-on-a-chip devices

October 27, 2013
Author(s)
Darwin R. Reyes-Hernandez, Michael W. Halter, Jeeseong Hwang
Here we present a new metrology tool for the determination of the dimensions of channels from final product Lab-on-a-chip devices. Using Optical Coherence Tomography (OCT) areas of up to 12 mm x 12 mm can be imaged in less than 1 second, without the need

Diamond Sensors and Polycapillary Lenses for X-ray Absorption Spectroscopy

October 13, 2013
Author(s)
Bruce D. Ravel
Diamond sensors are evaluated as incident beam monitors for X-ray Absorption Spectroscopy experiments. These single crystal devices pose a challenge for an energyscanning experiment using hard X-rays due to the e ect of diffraction from the crystalline

Report of the Key Comparison CCPR-K5 Spectral Diffuse Reflectance

October 2, 2013
Author(s)
Yoshihiro Ohno, Maria E. Nadal, Kenneth L. Eckerle, E. A. Early
This is an official report from Consultative Committee of Photometry and Radiometry (CCPR) on the Key Comparison CCPR-K5 spectral diffuse reflectance, conducted in the framework of CIPM Mutual Recognition Arrangement (MRA). 13 national laboratories

Using a Laser Tracker to Actively Coordinate the Motion of a 3m Industrial Robot to Within 50 Microns: An ongoing effort to accurately determine and correct positioning errors.

October 1, 2013
Author(s)
David R. Novotny, Joshua A. Gordon, Jason B. Coder, Jeffrey R. Guerrieri, Michael H. Francis
We are using industrial-grade robotics guided by a metrology-grade laser tracker to perform antenna calibrations at mmWave frequencies. We are using a 3 m-reach robot to spherically scan a milli-meter Wave (mmWave) probe around an antenna under test (AUT)

Functional Constraints and the Design of a New Watt Balance

September 30, 2013
Author(s)
Leon S. Chao, Stephan Schlamminger, Jon R. Pratt
The functional constraints driving the design of the new permanent-magnet driven watt balance (NIST-4) outline the variables and compromises worthy of addressing. Construction according to these design parameters will demonstrate the high precision
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