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Displaying 1051 - 1075 of 2730

Metrological challenges introduced by new tolerancing standards

February 13, 2014
Author(s)
Ed Morse, Yue Peng, Vijay Srinivasan, Craig M. Shakarji
The recent release of ISO has provided designers with a richer set of specification tools for the size of part features, so that various functional requirements can be captured with greater fidelity [2]. However, these tools also bring new challenges and

Estimation of uncertainty in application profiles

February 3, 2014
Author(s)
David W. Flater
Application profiling tools are the instruments used to measure software performance at the function and application levels. The most powerful measurement method available in application profiling tools today is sampling-based profiling, where a

Estimation of the Limit of Detection Using Information Theory Measures

January 31, 2014
Author(s)
Alexander (. Vergara Tinoco, Fonollosa Jordi, Huerta Ramon, Santiago Marco
Definitions of the Limit of Detection (LoD) based on the probability of false positive and/or false negative errors have been proposed over the past years. Although such definitions are straightforward and valid for any kind of analytical system, the

Saponins: A sustainable surfactant. From its microwave-assisted extraction to the synthesis of monodisperse latices

January 21, 2014
Author(s)
Charlene Schnitt, Bruno Grassl, Julien C. Gigault, Vincent A. Hackley, Gaetane Lespes, Jacques Desbrieres, Virginie Pellerin, Stephanie Reynaud
Synthetic surfactants are widely used in emulsion polymerization, but it is increasingly desirable to replace them with naturally derived molecules with a reduced environmental burden. This study demonstrates the use of saponins as sustainable and

SPRITE: A modernized approach to scanning probe contact resonance imaging

January 20, 2014
Author(s)
Anthony B. Kos, Jason P. Killgore, Donna C. Hurley
We describe a system for contact resonance tracking called Scanning Probe Resonance Image Tracking Electronics (SPRITE). SPRITE can image two contact resonance frequencies simultaneously and thus can be used to acquire quantitative mechanical properties

Acoustic Gas Thermometry

January 16, 2014
Author(s)
Michael R. Moldover, Roberto M. Gavioso, James B. Mehl, Laurent Pitre, Michael de Podesta, Jintao Zhang
Primary acoustic gas thermometry (AGT) exploits the simple relationship between the speed of sound in a dilute gas u and the thermodynamic temperature T of the gas. For monatomic gases such as argon and helium, u2 = (5/3) kT/m, in the limit of zero

Liquid Flow Meter Calibrations with the 0.1 L/s and 2.5 L/s Piston Provers

January 15, 2014
Author(s)
Jodie G. Pope, John D. Wright, Aaron N. Johnson, Christopher J. Crowley
This document provides a description of the 2.5 L/s and 0.1 L/s liquid flow calibration standards operated by the National Institute of Standards and Technology (NIST) Fluid Metrology Group to provide flow meter calibrations for customers. The 0.1 L/s and

Fast and Reliable Spectral Response Measurements of PV Cells Using Light Emitting Diodes

January 1, 2014
Author(s)
Behrang H. Hamadani, John F. Roller, Brian P. Dougherty, Howard W. Yoon
We present a measurement system for absolute differential spectral responsivity of solar cells based on high-powered LED arrays coupled to an optical light guide capable of large area illumination. Two different measurement techniques were developed and

Does Your SEM Really Tell the Truth? - How would you know? Part 1

December 16, 2013
Author(s)
Michael T. Postek, Andras Vladar
The scanning electron microscope (SEM) has gone through a tremendous evolution to become a critical tool for many and diverse scientific and industrial applications. The high resolution of the SEM is especially suited for both qualitative and quantitative

High-Accuracy Measurements of the Vapor Pressure of Ice Referenced to the Triple Point

December 6, 2013
Author(s)
Katarzyna E. Bielska, Daniel K. Havey, Gregory E. Scace, D Lisak, Allan H. Harvey, Joseph T. Hodges
The vapor pressure of hexagonal (Ih) ice was measured over the temperature range 175 K to 253.4 K and referenced to the value at the triple point of water. This experiment combined a highly accurate humidity generation system containing an ice-coated

Impact of UV Irradiation on the Surface Chemistry and Structure of Multiwall Carbon Nanotube Epoxy Nanocomposites

December 6, 2013
Author(s)
Elijah Petersen, Thomas F. Lam, Justin Gorham, Keana Scott, Chris Long, Deborah Jacobs, Renu Sharma, James Alexander Liddle, Tinh Nguyen
One of the most promising applications of nanomaterials is as nanofillers to enhance the properties of polymeric materials. However, the effect of nanofillers on polymers subject to typical environmental stresses, such as ultraviolet (UV) radiation, high

Certification of Elements in and Use of Standard Reference Material 3280 Multivitamin/Multielement Tablets

December 2, 2013
Author(s)
Gregory C. Turk, Katherine E. Sharpless, Steven J. Christopher, Danielle Cleveland, Russell D. Day, Stephen E. Long, Elizabeth A. Mackey, Anthony F. Marlow, Rick L. Paul, John R. Sieber, Rabia Oflaz, Laura J. Wood, Lee L. Yu, Rolf L. Zeisler, Stephen A. Wise, James H. Yen, E. Greene, J. Harnly, I-P Ho, Joseph M. Betz, R. Q. Thompson, Candace Jongsma
Standard Reference Material (SRM) 3280 Multivitamin/Multielement Tablets was issued by the National Institute of Standards and Technology (NIST) in 2009 and has certified and reference mass fraction values for 13 vitamins, 26 elements, and 2 carotenoids

Quantitative bottom-up proteomics depends on digestion conditions

December 2, 2013
Author(s)
Mark S. Lowenthal, Yuxue Liang, Karen W. Phinney, Stephen E. Stein
Accurate quantification is a fundamental requirement in the fields of proteomics and biomarker discovery, and for clinical diagnostic assays. To demonstrate the extent of quantitative variability in measurable peptide concentrations due to differences

Pressure-Sensitive Sampling Wands for Homeland Security Applications

December 1, 2013
Author(s)
Matthew E. Staymates, Jennifer R. Verkouteren, Jessica Grandner
This work discusses the use of Force Sensing Resistor (FSR) technology for Homeland Security applications. One area of particular focus is the optimization of wipe sampling of surfaces to facilitate enhanced trace contraband collection. Another focus area

Electro-Thermo-Mechanical Model for Bulk Acoustic Wave Resonators

November 30, 2013
Author(s)
Eduard Rocas, Juan C. Collado Gomez, Jordi Mateu, Nathan D. Orloff, James C. Booth, Robert Aigner
We present the electro-thermo-mechanical constitutive relations, expanded up to the third order, for a BAW resonator. The relations obtained are implemented into a circuit model, which is validated with extensive linear and nonlinear measurements. The

Viscosity-ratio measurements with capillary viscometers

November 27, 2013
Author(s)
Robert F. Berg, Eric F. May, Michael R. Moldover
Viscosity-ratio measurements made with capillary viscometers exploit the accurate values of the viscosity of helium calculated ab initio. Accurate values of the argon-to-helium viscosity ratio are now used for primary acoustic gas thermometry and for the

Accurate Spring Constant Calibration for very Stiff Atomic Force Microscopy Cantilevers

November 26, 2013
Author(s)
Scott Grutzik, Richard S. Gates, Yvonne B. Gerbig, Douglas T. Smith, Robert F. Cook, Alan Zehnder
There are many atomic force microscopy (AFM) applications that rely on quantifying the force between the AFM cantilever tip and the sample. The AFM does not explicitly measure force, however, so in such cases knowledge of the cantilever stiffness is

Wavelength Dependent UV Inactivation and DNA Damage of Adenovirus 2 as Measured by Cell Culture Infectivity and Long Range Quantitative PCR

November 22, 2013
Author(s)
Sara E. Beck, Roberto A. Rodriguez, Karl G. Linden, Thomas M. Hargy, Thomas C. Larason, Harold B. Wright
Adenovirus is regarded as the most resistant pathogen to ultraviolet (UV) disinfection due to its demonstrated resistance to monochromatic, low-pressure (LP) UV irradiation at 254 nm. This resistance has resulted in high UV dose requirements for all
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