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Chemistry

Projects/Programs

Keyword

Organizational Unit

Engineering and Optical Characterization of Magnetic Nanoparticles (MNPs)

Ongoing

Nanomagnets by Design Nanoparticles are an important subclass of low-dimensional magnetic materials displaying size-dependent magnetic behavior. The controllable magnetocrystalline anisotropy introduced at nanoscale size regimes (as low as 3 nms in diameter) allows for MNPs of ferro/ferrimagnetic

Environmental Metabolomics

Ongoing

The application of metabolomics techniques to environmental systems biology offers a promising opportunity to achieve insights into non-model organism biology. Each biological system manifests distinctive challenges that offer insights into criteria important for rigorous study design and method

Evaluating the Quality of Cell Counting Methods: Experimental Design and Statistical Analysis

Ongoing

Related Standards/Tools ISO 20391-2:2019 Biotechnology — Cell counting — Part 2: Experimental design and statistical analysis to quantify counting method performance COMET (Counting Method Evaluation Tool) A Shiny Application that executes the statistical analysis and reporting outlined in ISO 20391

Evaluation of Independent High-Precision Assay Procedures for a High-Purity Primary Standard Reagent

Ongoing

The NIST high-purity primary standard reagent SRMs are the benchmark for a wide variety of acidimetric and oxidation-reduction titrations. This suite of SRMs includes SRM 84k Potassium Hydrogen Phthalate , SRM 350b Benzoic Acid , and SRM 973 Boric Acid , each used as a standard acid. SRM 723d Tris

Ammunition metal box with explosives sticker.

Explosives Decomposition Chemistry

Completed

Intended Impact Computational modeling and simulation will help in the invention of new explosives, the design of compounded mixtures of existing materials, and the engineering of delivered systems such as military ordnance. Objective Detailed chemistry is a necessary part of computational

Expression of Stable Isotopically Labeled Proteins for Use as Internal Standards for Mass Spectrometric Quantitation of Clinical Protein Biomarkers

Ongoing

Measurement of intact proteins by mass spectrometry can be problematic. In order to make proteins more amenable to mass spectrometric detection, the proteins are commonly digested with a proteolytic enzyme prior to analysis. Quantitation can then be performed by adding known amounts of isotopically

Photograph of SRM 2378 Fatty Acids in Human Serum showing three vials labeled Serum 1, Serum 2, and Serum 3.

Fatty Acids in Human Serum and Plasma Quality Assurance Program (FAQAP)

Completed

Interlaboratory comparison studies of the FAQAP focused on the measurement of 24 fatty acids in selected serum and plasma matrices. Frozen or freeze-dried serum or plasma samples were sent to laboratories for analysis together with control materials. Results were returned to NIST for data evaluation

Flow Cytometry Lab

Ongoing

Current Capabilities ERF value assignment measurement service for traceable ERF value assignment to microparticles, Aseptic sorting of cell lines, and primary cells Quantitative measurements of cell surface and intracellular biomarkers by estimating antibody bound per cell Accurate enumeration of

Fluid Phase Nuclear Magnetic Resonance (NMR) Spectroscopy

Ongoing

In-situ vapor-liquid equilibrium (VLE). We are applying vapor-phase NMR to measure VLE in-situ. We are currently applying this methodology to industrially important systems such as refrigerants and natural gas. The most widely used refrigerants have high global warming potential. Drop-in

Food Nutrition and Safety Measurements Quality Assurance Program (FNSQAP)

Ongoing

As part of a revamp of QAPs in 2021, NIST established the FNSQAP to support the NIST Food Safety Program and Measurements and Standards to Support Nutrition Labeling. Participants measure nutrient components (e.g., minerals, vitamins, fatty acids, dietary fiber) and contaminants (e.g., toxic

Free Energy and Advanced Sampling Simulation Toolkit (FEASST)

Ongoing

Intended Impact While flat-histogram Monte Carlo simulations have been shown to be a promising method for the direct calculation of complex fluid phase behavior with a variety of applications, most open-source Monte Carlo simulation packages do not support this method. We have therefore made FEASST

Fundamental Interaction Mechanisms of Engineered Nanomaterials with DNA

Ongoing

Intended impact Nanotechnology research has resulted in the rapid creation of engineered nanomaterials with many foreseeable applications in medical imaging/diagnosis and in drug delivery. However, there is a notable scarcity of both acute and chronic human toxicity data for these new materials

Space filling models of bent and straight alkyl chains tethered to silica that represent disordered and ordered models.

Fundamental Studies of the Conformational Phase Behavior of Chain Molecules at Interfaces

Intended Impact Predicting how the conformational phase behavior of tethered chain molecules depends on external variables is challenging. Understanding how even simple models for tethered chain molecules depend on external variables will greatly aid our understanding of tethered chain systems

Photo of broken laminated windshield glass

Glass Evidence Analysis

Ongoing

Quantitative XRF Glass Database Recent research efforts in the forensic trace field have focused on the development of databases to assign a significance to forensic evidence (i.e., to report the strength of an association or exclusion). In the forensic analysis of glass using µ-XRF, samples are

Health Assessment Measurements Quality Assurance Program (HAMQAP)

Completed

Participants in the HAMQAP measured concentrations of nutritional and toxic elements, fat- and water-soluble vitamins, fatty acids, active and/or marker compounds, and contaminants in samples distributed by NIST.   Samples that represent human intake (e.g., foods, dietary supplements, tobacco) were

High Rate Testing

Ongoing

This project involves sample geometry and metrological development for high rate servohydraulic testing. (Content to be uploaded soon)

High-Precision Isotopic Reference Materials

Ongoing

A new generation of multi-collector IRMS, utilizing both inductively coupled plasma and thermal ionization sample sources, is now capable of measuring isotope ratios with extremely high precision – a few parts in 10 6. This new measurement capability has caused a minor revolution in the use of

High-Sensitivity IR Spectroscopy of Proteins

Ongoing

Infrared (IR) absorption spectroscopy has been widely used as a non-invasive, label-free characterization method for the chemical identification and structure of complex biomolecules. Fourier-transform IR (FT-IR) technology is commonly used to characterize proteins and other biological molecules

Photograph of the exterior of the Hollings Marine Laboratory (HML), with signs designation the facility.

HML Organic Chemical Metrology Program Areas

Ongoing

The organic analytical facility, located on the second floor of the Hollings Marine Laboratory, consists of two laboratories with a combined area of approximately 215 m2. These two laboratories provide the space and instrumentation to achieve two main functions for NIST: (1) the determination of

Identification, Suitability Testing, and Property Determination from Untargeted Measurements

Ongoing

In many applications, detailed knowledge of a fluid mixture’s physical behavior is needed. This can include physical properties such as viscosity and qualitative properties such as solubility. For instance, a dissolved polymer may suddenly precipitate out of solution when exposed to saline, and if

Illicit Narcotics Detection

Ongoing

“Method for evaluating ion mobility spectrometers for trace detection of fentanyl and fentanyl-related substances”, Jennifer R Verkouteren, Jeffrey Lawrence, R Michael Verkouteren and Edward Sisco, Analytical Methods, 11(47), 6043-6052 (2019). “Discriminative potential of ion mobility spectrometry

timeline of neutron detector image spatial resolution

Imaging: Evolution of Neutron Image Detector Spatial Resolution

Ongoing

Neutron imaging has yielded valuable insight into the water content of fuel cells because minimal changes to a test section are needed. A limit of neutron imaging is the achievable spatial resolution, which is primarily dominated by the detector. Figure 1 shows the evolution of the spatial

Figure with five interlocking puzzle pieces representing different aspects of the measurement process.

Improving High-Performance Inductively-Coupled Plasma Optical Emission Spectrometry (HP-ICP-OES) Through Exact Matching

Ongoing

A thorough understanding of the analytical benefits and characteristics of the implementation of exact matching with HP-ICP-OES will enable HP-ICP-OES to be applied more effectively to a variety of NIST measurements. Such measurements include, but are not limited to, value assignment measurements

Inorganic Phase Equilibrium Data

Ongoing

Every deliberate effort to develop a new material or to improve processing begins with chemical composition and the conditions (temperature, pressure) under which pure compounds and their mixtures are stable ( an equilibrium phase diagram). In the absence of such information, materials scientists

Photograph showing Gas Pump Octane Options

International Collaborations to Improve the Accuracy of Gas Primary Standards

Ongoing

The goal is to use the results from intercomparisons to assist in determining and correcting any large differences between gas standards from different NMIs. When results are within the stated uncertainty bounds, then the NMIs gas standards are considered to be equivalent. This enables the use of

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