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Displaying 101 - 125 of 546

Reference Materials for Phase Equilibrium Studies. 1. Liquid-Liquid Equilibria (IUPAC Technical Report)

July 8, 2021
Author(s)
Ala Bazyleva, William E. Acree, Jr., Robert D. Chirico, Vladimir Diky, Glenn T. Hefter, Johan Jacquemin, Joe W. Magee, John P. O'Connell, James D. Olson, Ilya Polishuk, Kurt Schmidt, John M. Shaw, J. P. M. Trusler, Ronald D. Weir
This article is the first of three projected IUPAC Technical Reports resulting from IUPAC Project 2011-037-2-100 (Reference Materials for Phase Equilibrium Studies). The goal of that project was to select reference systems with critically evaluated

Assessment of Serum Total 25 Hydroxyvitamin D Assay Commutability of Standard Reference Materials and College of American Pathologists Accuracy Based Vitamin D (ABVD) Scheme and Vitamin D External Quality Assessment Scheme (DEQAS) Materials: Vitamin D Sta

July 1, 2021
Author(s)
Johanna Camara, Stephen A. Wise, Andrew Hoofnagle, Emma L. Williams, Graham D. Carter, Julia C. Jones, Carolyn Burdette, Grace Hahm, Federica Nalin, Adam J. Kuszak, Joyce M. Merkel, Ramon Durazo-Arvizu, Pierre Lukas, E. Cavalier, Christian Popp, Christian Beckert, Jan Schultess, Glen Van Slooten, Carole Tourneur, Camille Pease, Ravi Kaul, Alfredo Villarreal, Fiona Ivison, Ralf Fischer, Jody M. van den Ouweland, Chung S. Ho, Emmett W. Law, Jean-Nicolas Simard, Renaud Gonthier, Brett Holmquist, Marcelo C. Batista, Heather Pham, Alex Bennett, Sarah Meadows, Lorna Cox, Eugene Jansen, Dilshad A. Khan, Kimberly Robyak, Michael H. Creer, Mark Kilbane, Patrick J. Twomey, James Freeman, Neil Parker, Jinyun Yuan, Robert Fitzgerald, Sohail Mushtaq, Michael W. Clarke, Norma Breen, Christine Simpson, Christopher T. Sempos
An interlaboratory study was conducted through the Vitamin D Standardization Program (VDSP) to assess commutability of Standard Reference Materials® (SRMs) and proficiency testing/external quality assessment (PT/EQA) samples for determination of serum

Polarization Effects of X-ray Monochromators Modeled Using Dynamical Scattering Theory

July 1, 2021
Author(s)
Marcus Mendenhall, David R. Black, Donald Windover, James Cline
The difference in the diffracted intensity of the sigma-and pi-polarized components of an X-ray beam in powder diffraction has generally been treated according to equations based on dipole scattering, also known as kinematic X-ray scattering. Although this

Dynamic light scattering distributions by any means

May 21, 2021
Author(s)
Natalia Farkas, John A. Kramar
Dynamic light scattering (DLS) is an essential technique for nanoparticle size analysis and has been employed extensively for decades, but despite its long history and popularity, the choice of weighting and mean of the size distribution often appears to

A Highly-enriched 244Pu Reference Material for Nuclear Safeguards and Nuclear Forensic Measurements

January 26, 2021
Author(s)
Richard Essex, Ross W. Williams, Kerri C. Treinen, Amelie Hubert, Marc A. Humphrey, Jeremy D. Inglis, William S. Kinman, Joel Maassen, Maxim V. Penkin, Robert E. Steiner
A highly-enriched 244Pu isotope dilution reference material has been prepared and characterized for metrologically traceable measurements of very small quantities of plutonium. The amount of plutonium in samples associated with nuclear safeguards and

A new highly enriched 233U reference material for improved simultaneous determination of uranium amount and isotope amount ratios in trace level samples

January 26, 2021
Author(s)
Richard Essex, Ross W. Williams, Kayron T. Rogers, Cole R. Hexel, Tashi Parsons-Davis, Kerri C. Treinen
A highly-enriched 233U reference material (>0.99987 n(233U)/n(U)) has been prepared and characterized for use as an isotope dilution mass spectrometry spike. An ion exchange separation was performed on 1 gram of high purity 233U to further reduce trace

Certification of Standard Reference Material(R) 1992 / ERM(R)-FD305 Zeta Potential - Colloidal Silica (Nominal Mass Fraction 0.15 %)

November 24, 2020
Author(s)
Yannic Ramaye, Vikram Kestens, J. Charoud-Got, S. Mazoua, G. Auclair, Tae Joon Cho, Blaza Toman, Vincent A. Hackley, T. Linsinger
This report describes the production of SRM 1992/ERM-FD305, silica particles suspended in a borate buffer, certified for electrophoretic mobility and zeta potential by electrophoretic light scattering (ELS). This material was produced following ISO 17034

Certification of Standard Reference Material(R) 1993 / ERM(R)-FD306 Zeta Potential - Colloidal Silica (Nominal Mass Fraction 2.2 %)

November 24, 2020
Author(s)
Yannic Ramaye, Vikram Kestens, J. Charoud-Got, S. Mazoua, G. Auclair, Tae Joon Cho, Blaza Toman, Vincent A. Hackley, T. Linsinger
This report describes the production of SRM 1993/ERM-FD306, silica particles suspended in a borate buffer, certified for electrophoretic mobility and zeta potential by electrophoretic light scattering (ELS). This material was produced following ISO 17034

Lessons From the NIST Micronutrients Quality Assurance Program for Vitamin C, 1993 to 2015: Sample Stability, Assay Reproducibility, and Use of Controls to Improve Comparability

November 11, 2020
Author(s)
David L. Duewer, Jeanice M. Brown Thomas, Katherine E. Sharpless, S A. Margolis
Vitamin C is a necessary micronutrient that is involved in many biological processes. In preserved human plasma and serum, vitamin C is most meaningfully analyzed as total ascorbic acid (TAA). From 1993 through 2015, the National Institute of Standards and

The certification of electrophoretic mobility/zeta potential of silica particles in aqueous solution: ERM-FD305/SRM 1992

October 27, 2020
Author(s)
Y. Ramaye, V. Kestens, J. Charoud-Got, S. Mazoua, G. Auclair, Tae Joon Cho, Blaza Toman, Vincent A. Hackley, T. Linsinger
This report describes the production of ERM-FD305/SRM 1992, silica nanoparticles suspended in a borate buffer, certified for electrophoretic mobility and zeta potential measurements by electrophoretic light scattering (ELS). This material was produced

Development of a pregnancy-specific reference material for thyroid biomarkers, vitamin D, and nutritional trace elements in serum

October 24, 2020
Author(s)
Ashley Russell, Lisa Kilpatrick, Carolyn Burdette, Denise S. Tevis, Zachary A. Fultz, Michael Nelson, Jeff M. Jarrett, Stephen A. Wise, Brittany Kassim, Stephen E. Long
Background Concentrations of critical metabolites, hormones, and nutritional elements change significantly throughout pregnancy. Therefore, increased matrix complexity is a challenge for the measurement of these biomarkers. To provide a quality assurance

The certification of electrophoretic mobility/zeta potential of silica particles in aqueous solution: ERM-FD306/SRM 1993

October 23, 2020
Author(s)
Yannic Ramaye, Vikram Kestens, J. Charoud-Got, S. Mazoua, G. Auclair, Tae Joon Cho, Blaza Toman, Vincent A. Hackley, T. Linsinger
This report describes the production of ERM-FD306/SRM 1993, silica nanoparticles suspended in a borate buffer, certified for electrophoretic mobility and zeta potential measurements. This material was produced following ISO Guide 17034:2016 and is

Certification of Standard Reference Material(R) 955d, Toxic Elements and Metabolites in Frozen Human Blood

October 15, 2020
Author(s)
Lee L. Yu, Karen E. Murphy, Colleen E. Bryan Sallee, Thomas W. Vetter, Robert C. Hagwood, George C. Caceres, Stephen E. Long, J M. Jarrett, M A. Franklin, J Castro Georgi, D M. Jones, Robert Jones, Z Li, Y L. Sommer, D S. Tevis, K Wallon, C D. Ward, M Maras, S Erdahl, C Gilmer, M Wermers, H Woldeysus, K F. Mehigan, M Morrissette, Christopher D. Palmer, Patrick J. Parsons
Standard Reference Material (SRM) 955d is intended for use in validating analytical methods for measuring toxic elements and mercury species in human blood, and in value assigning locally produced control materials analyzed using the validated methods. A

A Diploid Assembly-based Benchmark for Variants in The Major Histocompatibility Complex

September 22, 2020
Author(s)
Justin M. Zook, Justin M. Wagner, Chen-Shan Chin, Qiandong Zeng, Alexander Dilthey, Tobias Marschall, Mikko Rautiainen, Erik Garrison, Shilpa Garg
Most human genomes are characterized by aligning individual reads to the reference genome, but accurate long reads and linked reads now enable us to construct accurate, phased de novo assemblies. We focus on a medically important, highly variable, 5

A Reference High-Pressure CH4 Adsorption Isotherm for Zeolite Y: Results of an Interlaboratory Study

September 11, 2020
Author(s)
Huong Giang T. Nguyen, Christopher M. Sims, Blaza Toman, Jarod C. Horn, Roger D. van Zee, Mathias Thommes, Riaz Ahmad, Joeri F. Denayer, Gino V. Baron, Emilio Napolitano, Marek Bielewski, Enzo Mangano, Stefano Brandani, Broom Darren, M.J. Benham, Anne Dailly, Frieder Dreisbach, Satyannarayana Edubilli, Sasidhar Gumma, Jens Mollmer, Marcus Lange, Mi Tian, Tim Mays, T. Shigeoka, S. Yamakita, M. Hakuman, Y. Nakada, K. Nakai, Junyoung Hwang, Ronny Pini, Huan Jiang, Armin Ebner, Marjorie Nicholson, James Ritter, Judit Farrando Perez, Carlos Cuadrado, Joaquin Silvestre Albero, Christos Tampaxis, Theodore Steriotis, Daniela Rimnacova, Martina Svabova, Maryna Vorokhta, Hai Wang, Eric Bovens, Nicolas Heymans, Guy de Weireld
This paper reports the results of an international interlaboratory study led by the National Institute of Standards and Technology (NIST) on the measurement of high-pressure surface excess methane adsorption isotherms on NIST Reference Material RM 8850
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