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Metrology

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Displaying 1 - 25 of 2714

Report on the May 2025 NIST Measurement Week: Realization of an OSAC draft Interim Performance Assessment for Terrestrial Laser Scanners Used by Law Enforcement Agencies

September 17, 2025
Author(s)
Balasubramanian Muralikrishnan, Katharine Shilling, Mary Gregg, Vincent Lee, Jason Keller, Erin Casey, Eugene Liscio, Bryon O'Neil, Mike Russ, Toby Terpstra
This report describes a terrestrial laser scanner (TLS) testing event, the NIST Measurement Week, held at the National Institute of Standards and Technology (NIST) during the week of May 12-16, 2025. The Crime Scene Investigation and Reconstruction (CSIR)

Multi-facility comparison of InGaAs trap detector responsivity for optical fiber power

September 1, 2025
Author(s)
Kyle Rogers, Jeanne Houston, Zeus Ruiz Gutierrez, Matthew Spidell, Padraic Aither, Marty Gould, John Lehman
The absolute responsivity of an optical detector in a trap configuration has been investigated in the interest of high-accuracy fiber-coupled measurements for commercial optical fiber power meters and fiber-coupled single-photon detector calibrations. The

Material Needs and Measurement Challenges for Advanced Semiconductor Packaging: Understanding the Soft Side of Science

August 27, 2025
Author(s)
Ran Tao, Polette Centellas, Stian Romberg, Anthony Kotula, Gale Holmes, Amanda Forster, Christopher Soles, Bob Allen, Edvin Cetegen, William Chen, Jeff Gotro, Mark Poliks
This perspective builds upon insights from the National Institute of Standards and Technology (NIST)-organized workshop, "Materials and Metrology Needs for Advanced Semiconductor Packaging Strategies," held at the 35th annual Electronics Packaging

From ultra-noisy to ultra-stable: optimization of the optoelectronic laser lock

August 24, 2025
Author(s)
Takuma Nakamura, Yifan Liu, Naijun Jin, Haotian Cheng, Charles McLemore, Nazanin Hoghooghi, Peter Rakich, Franklyn Quinlan
We demonstrate thermal noise-limited direct locking of a semiconductor DFB laser to a sub-1 mL volume, ultrastable optical cavity, enabling extremely compact and simple ultrastable laser systems. Using the optoelectronic laser locking method, we realize

Characterizing Cell-Free Transcription and Translation Dynamics with Nucleic Acid-Based Assays

August 10, 2025
Author(s)
Fernanda Piorino Macruz de Oliveira, Chad Alan Sundberg, Elizabeth Strychalski, Eugenia Romantseva
Characterization of cell-free expression (CFE) systems must expand beyond single spectrophotometric measurements of a green fluorescent protein to provide meaningful metrics of system performance over the course of a CFE reaction and enable the development

Radio Frequency from Optical with Instabilities below 10^-15 - Generation and Measurement

August 8, 2025
Author(s)
Archita Hati, Marco Pomponio, Nicholas Nardelli, Tanner Grogan, Kyungtae Kim, Dahyeon Lee, Jun Ye, Tara Fortier, Andrew Ludlow, Craig Nelson
This paper presents a frequency synthesis that achieved exceptional stability by transferring optical signals to the RF domain at 100 MHz. These systems employ a cryogenic silicon cavity-stabilized laser at 1542 nm and an ultra-low expansion (ULE) glass

Large Area Real-Space Crystallography and Thickness Determination of Mesoscopic Semiconductor Membranes Using Zone Axis Patterns, Cold Field-Emission SEM/STEM, and Analytical S/TEM

July 25, 2025
Author(s)
Vladimir Oleshko, Glenn Holland, Daron Westly, John Villarrubia
Structural and dimensional characterization of layered structures in semiconductors is increasingly important for microelectronics manufacturing because of the continuing downward scaling of devices. Manufacturers require high-precision non-destructive

Reference Correlation of the Viscosity of Argon

July 10, 2025
Author(s)
Sofia Sotiriadou, Konstantinos Antoniadis, Marc Assael, Marcia Huber
This paper presents a new wide-ranging reference correlation for the viscosity of argon, incorporating recent ab initio dilute gas calculations and critically evaluated experimental data. The correlation is designed to be used with a high-accuracy

Advanced Metrology Suite for Linking Residual Stress to Fundamental Properties of Thermoset Packaging Materials

June 26, 2025
Author(s)
Polette Centellas, Stian Romberg, Ran Tao, Alexander Landauer, Karl Schoch, Huong Giang Nguyen, Gale Holmes, Gery Stafford, Christopher Soles
Residual stresses inevitably develop in thermosetting materials used for semiconductor packaging during the curing process and in service. Understanding the development of these deleterious stresses is necessary for improving predictive models and

The trace of heat: on the predictive power of modeling transient diffusion

June 26, 2025
Author(s)
Vijaya Holla, Timothy Redford, Philipp Kopp, Stefan Kollmannsberger
The paper at hand evaluates the validity of the transient heat equation with phase change and temperature-dependent coefficients as a model to predict the evolution of melt pools for rapid turnaround scan strategies in a laser powder bed fusion (PBF-LB)

Spin-lattice entanglement in CoPS3

June 10, 2025
Author(s)
Angela Hight Walker, Kevin Garrity, Rebecca Dally
Complex chalcogenides in the MPS3 family of materials (M = Mn, Fe, Co, and Ni) display remarkably different phase progressions depending upon the metal center orbital filling, character of the P–P linkage, and size of the van der Waals gap. There is also a

Uranium Particle Age Dating, Aggregation, and Model Age Best Estimators

June 9, 2025
Author(s)
Evan Groopman, Todd Williamson, Timothy Pope, Michael Bronikowski, Spencer M. Scott, Matthew Wellons
We present important aspects of uranium particle age dating by Large-Geometry Secondary Ion Mass Spectrometry (LG-SIMS) that can introduce bias and increase model age uncertainties, especially for small, young, and/or low-enriched particles. This metrology

Elucidating the thermal properties and anomalous transport in the 18R polytype of SnSe2

May 30, 2025
Author(s)
Oluwagbemiga Ojo, Wilarachchige D. C. B. Gunatilleke, Winnie Wong-Ng, Tieyan Chang, Yu-Sheng Chen, Joshua Martin, Adam Biacchi, George Nolas
The 18R polytype of SnSe2 possesses unique structural features that can directly impact the transport properties and potential applications of interest; however, a comprehensive understanding of the intrinsic physical properties is lacking. We grew large

Elongated particles in flow: commentary on small-angle scattering investigations

May 23, 2025
Author(s)
Guan-Rong Huang, Lionel Porcar, Ryan Murphy, Yuya Shinohara, Yangyang Wang, Jan-Michael Carrillo, Bobby G. Sumpter, Chi-Huan Tung, Lijie Ding, Changwoo Do, Wei-Ren Chen
This work thoroughly examines several analytical tools, each possessing a different level of mathematical intricacy, for the purpose of characterizing the orientation distribution function of elongated objects under flow. Our investigation places an

Towards an Understanding of Robotic Bin-Picking Throughput

May 22, 2025
Author(s)
Anirudh Krishnan Komaralingam, Prem Rachakonda, Kamel Saidi, Armin Khatoonabadi
NIST is leading and supporting multiple efforts to develop standards for 3D imaging systems used for industrial automation. There are few standards for verifying the performance of these systems and NIST is working with ASTM subcommittee E57.23 on

NIST Special Publication 260 NIST.SP.260-256 Certification of Standard Reference Material(R)s 3672a & 3673a: Organic Contaminants in Smokers' Urine (Frozen) & Organic Contaminants in Non-Smokers' Urine (Frozen)

May 14, 2025
Author(s)
Ashley Russell, Carolyn Burdette, Johanna Camara, Nathanael Heckert, Jennifer Hoguet, Kevin Huncik, Jared Ragland, Elena Wood
Standard Reference Material (SRM) 3672a Organic Contaminants in Smokers' Urine (Frozen) and SRM 3673a Organic Contaminants in Non-Smokers' Urine (Frozen) are intended for use in evaluating analytical methods for the determination of selected naturally

Certification of Standard Reference Material(R) 1989 Monodisperse Irregularly Shaped Epoxy-Based Particles (Nominal 100 mm, 150 mm, 220 mm)

May 2, 2025
Author(s)
Srivalli Telikepalli, Dean Ripple, Michael Carrier, Kristen Steffens, David Newton, Christopher Montgomery, Nicholas Ritchie, Anthony Asmar, Michael Halter
Standard Reference Material (SRM) 1989 is a NIST particle standard produced using photolithographic methods and delivers a certified value for particle size of an irregularly shaped particle. This SRM was developed to allow a more accurate monitoring of

CODATA Recommended Values of the Fundamental Physical Constants: 2022

April 30, 2025
Author(s)
Peter Mohr, David Newell, Barry N. Taylor, Eite Tiesinga
We report the 2022 self-consistent values of constants and conversion factors of physics and chemistry recommended by the Committee on Data of the International Science Council (CODATA). The recommended values can also be found at physics.nist.gov

Cannabis Laboratory Quality Assurance Program: Exercise 3 Moisture Final Report

April 28, 2025
Author(s)
Andrea Yarberry, Charles Barber, Laura Wood, Walter Wilson
NIST launched a Cannabis Laboratory Quality Assurance Program (CannaQAP) in 2020 to assist laboratories in demonstrating and improving cannabis (hemp and marijuana) measurement comparability and competence. CannaQAP provided tools that allowed analysts and

Interlaboratory Assessment of Candidate Reference Materials for Lentiviral Vector Copy Number and Integration Site Measurements

April 21, 2025
Author(s)
Hua-Jun He, Zhiyong He, Steven Lund, Barbara Paugh, Jennifer McDaniel, Justin Zook, Sierra Miller, Samantha Maragh, Simona Patange, Mahir Mohiuddin, Alessandro Tona, John Elliott, Kenneth Cole, Sheng Lin-Gibson
Reference materials are essential for accurately measuring integrated lentiviral vector (LV) copy number (VCN) and integration sites for the safety and efficacy of lentivirus-based gene therapy. We conducted an interlaboratory study on NIST candidate
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