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Stress measurements in the thermally grown oxide layer of thermal barrier coatings are presented. Stresses were determined from photoluminescence measurements made through the zirconia top layer as a function of the number of thermal cycles
An update of the NIST Standard Reference Database Number 30, the Structural Ceramics Database, has been completed. This update, designated SCD Update (April 2003), increases the number of source entries by 100 citations and increases the total number of
Winnie Wong-Ng, Lawrence P. Cook, F Jiang, L Swartzendruber, P Sastry
The subsolidus phase equilibria involving the Bi-2223(Bi 2Sr 1.9Ca 2.1Cu 3O 10+x) phase in the Bi-Sr-Ca-Cu-O system (BSCCO) were investigated at 840-850The subsolidus phase equilibria involving the Bi-2223(Bi2Sr1.9Ca2.1Cu3O10+x) phase in the Bi-Sr-Ca-Cu-O
For applications of phase equilibria to coated conductor processing, phase diagrams constructed under carbonate-free conditions should be employed. Using special apparatus and a procedure for preparing carbonate-free precursors based on BaO, phase diagrams
The purpose of this document is to propose a standard procedure for measuring the thermal conductivity of insulating thin films on silicon substrates. The initial part of the assessment is a review of several measurement methods that have been used to
Creep experiments were conducted on a commercial grade of silicon nitride (AS800) over a wide range of temperatures and stresses: 1200oC to 1370oC; 50 MPa to 400 MPa. Cavitation always accompanied creep. As with other grades of silicon nitride, the rate of
Gateway to the New Millennium was the theme of the 102nd annual meeting of the American Ceramic Society which took place in St. Louis, Missouri from April 29 to May 3, 2000. A brief description of both the scientific and social program of this meeting is
The 1999 Material Research Society Fall Meeting took place in Boston Copley Plaza from November 26 to December 3. This was the first time that MRS has used the spacious Hynes Convention Center as the primary meeting site, with the Marriott Hotel as an
The 48th Annual Denver X-ray Conference took place at Sheraton Steamboat Resort, Colorado, from August 2-6, 1999. This meeting was well attended, with a combined number of 650 conference attendees and exhibitors. It was supported by the International
Development of low friction surfaces has become an important issue for the development of reliable devices with moving components. The common way to measure nanofriction is to use a sharp tip sliding on a sample surface. High contact pressure at the tip
We use the equations for steady-state diffusion-induced grain boundary motion (DIGM), derived from our phase-field model, [17] to predict the grain boundary morphology and speed of DIGM, as well as the resulting compositions profiles, when the specimen
The thermal conductivity of AIN specimens doped with Y2O3(5 wt.%) was determined using the photothermal deflection technique. The results agree within 10% of measurements previously made using the laser flash method. Thermal measurements on as-fired thin
Thermodynamics is a field of physics and chemistry. It uses mathematics to describe changes in energy and entropy (disorder) of a material that is subject to mechanical, thermal or chemical action. It is most frequently used to describe the conditions that
Long-term service life of a load-bearing ceramic component such as a turbine blade atelevated temperatures is often controlled by the rates of nucleation and growth of creepcavities at grain junctions and interfaces within the microstructure of the
Non-adhesive and water-repellent surfaces are required for many tribological applications. Wetting of patterned superhydrophobic Si surfaces is studied as a multiscale process involving the macroscale (water droplet size), microscale (surface texture size)
Julia Slutsker, V Talanov, I Smolyaninov, Igor Levin, A R. Schwartz, Alexander L. Roytburd
The response of self-assembled CoFe2O4-PbTiO3 multiferroic nanostructures to an external microwave field was analyzed using a near-field scanning microwave probe. The nanostructures, grown as thin films on single crystal SrTiO3, consisted of magnetic
The vapor pressure of Mg(g) over MgB 2(cr) for the reaction 2 MgB 2(cr) Mg(g)+MgB 4(cr) has been measured thermogravimetrically from 900 degrees celsius to 1100 degrees celsius at 0.1 mPa(1 atm) total pressure using a modified Knudsen effusion method and
J Ilavsky, P Jemain, Andrew J. Allen, Gabrielle G. Long
The USAXS facility at UNICAT Sector 33 at the Advanced Photon Source (APS) is a world-class resource for advanced materials research emphasizing full-range charactrization of nanometer-scale to micrometer-scale microstructures. Receiving photons from an
T A. Dobbins, Andrew J. Allen, J Ilavsky, Gabrielle G. Long, A Kulkarni, H Herman
Yttria-stabilized zirconia (YSZ) thermal barrier coatings (TBCs) are used to protect turbine rotor and blade components in aircraft and land-based engines from operational temperatures (exceeding 1200 oC). Traditionally, those coatings are deposited using
Stephen W. Freiman, Richard R. Cavanagh, C K. Montgomery, Thomas J. Shaffner, S Arepalli, B Files, P Nikolaev
This document is an executive summary of a workshop organized jointly by the National Aeronautics and Space Administration, Lyndon B. Johnson Space Center (NASA/JSC) and the National Institute of Standards and Technology (NIST) was held on May 27-29, 2003
Joseph Woicik, F S. Aguirre-Tostado, A Herrera-Gomez, R Droopad, Z Yu, D G. Schlom, E Karapetrova, P Zschack, P Pianetta
Polarization-dependent x-ray absorption fine structure together with x-ray diffraction have been used to study the local structure in SrTiO 3 thin films grown on Si(001). Our data indicate that below a critical thickness of approximately 80 , the in-plane
Maps of residual stress distributions arising from anisotropic thermal expansion effects in a polycrystalline alumina are generated using fluorescence microscopy. The shifts of both the R1 and R2 ruby fluorescence lines of Cr in alumina are used to create
Low temperature conductivity mechanisms are identified in acceptor doped BaTiO3 single crystals equilibrated and quenched from high temperature under different oxygen partial pressures. A range of acceptor ionization states are quenched into samples doped
Ward L. Johnson, Sudook A. Kim, Grady S. White, Jaemi Herzberger, Kirsten L. Peterson, Paul R. Heyliger
Acoustic nonlinearity of cracked and uncracked multilayer ceramic capacitors (MLCCs) was characterized through time-domain analysis of resonant waveforms following tone-burst excitation. A phase-sensitive receiver was employed to measure the phase
Fractography is a powerful tool for the analysis of fractured glasses and ceramics. It is applicable to fractures created under controlled conditions in the laboratory and to component failures in service. Fractography can identify the cause of failure and