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Chemistry

Analytical chemistry

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Displaying 176 - 200 of 4039

Errors-in-variables calibration with dark uncertainty

June 16, 2022
Author(s)
Christina Cecelski, Blaza Toman, Fong-Ha Liu, Juris Meija, Antonio Possolo
A model for errors-in-variables regression is described that can be used to overcome the challenge posed by mutually inconsistent calibration data. The model and its implementation are illustrated in applications to the measurement of the amount fraction

Spectrophotometric Measurement of Carbonate Ion in Seawater over a Decade: Dealing with Inconsistencies

June 7, 2022
Author(s)
Elisa Guallart, Noelia Fajar, Maribel Garcia-Ibanez, Monica Castano-Carrera, Rocio Santiago-Domenech, Abed El Rahman Hassoun, Fiz Perez, Regina Easley, Marta Alvarez
The spectrophotometric methodology for carbonate ion determination in seawater was first published in 2008 and has been continuously evolving in terms of reagents and formulation. Although the method proves to be fast, relatively simple and affordable

Protocols for leakage testing

June 1, 2022
Author(s)
Henne van Heeren, Matthew Davies, Armelle Keiser, Rudy Lagrauw, Darwin Reyes-Hernandez, Vania Silverio, Nicolas Verplanck
This document is written to serve as a guideline for the testing of microfluidic devices, which are devices designed to manipulate fluids that are confined in a small volume. For instance, a channel with at least one dimension smaller than 1 mm is a

Communicating Confidence of Per- and Polyfluoroalkyl Substance (PFAS) Identification via High Resolution Mass Spectrometry

May 26, 2022
Author(s)
Joseph Charbonnet, Carrie McDonough, Feng Xiao, Trever Schwichtenberg, Dunping Cao, Sarit Kaserzon, Kevin Thomas, Pradeep Dewapriya, Benjamin Place, Emma Schymanski, Jennifer Field, Damian Helbling, Christopher Higgins
Per- and polyfluoroalkyl substances (PFASs) are important environmental contaminants, yet relatively few analytical reference standards exist for this class. Nontarget analyses performed by means of high-resolution mass spectrometry (HRMS) are increasingly

Interlaboratory Studies using the NISTmAb to Advance Biopharmaceutical Structural Analytics

May 5, 2022
Author(s)
Katharina Yandrofski, Trina Mouchahoir, M. Lorna De Leoz, David L. Duewer, Jeffrey W. Hudgens, Kyle Anderson, Luke Arbogast, Frank Delaglio, Robert Brinson, John Marino, Karen W. Phinney, Michael J. Tarlov, John E. Schiel
Biopharmaceuticals such as monoclonal antibodies are required to be rigorously characterized using a wide range of analytical methods. Various material properties must be characterized and well controlled to assure that clinically relevant features and

Assessing Arsenic Species in Foods Using Regularized Linear Regression of the Arsenic K-edge X-ray Absorption Near Edge Structure

April 19, 2022
Author(s)
Evan Jahrman, Lee L. Yu, William P. Krekelberg, David Sheen, Thomas C. Allison, John L. Molloy
The toxicity and bioavailability of arsenic is heavily dependent on its speciation. Therefore, robust and accurate methods are needed to determine arsenic speciation profiles for materials related to public health initiatives, such as food safety. Here, X
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