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Chemistry

Analytical chemistry

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Displaying 626 - 650 of 2084

High Levels of Gadolinium Deposition in the Skin of a Patient with Normal Renal Function

May 2, 2016
Author(s)
William C. Davis, Donna R. Roberts, Scott M. Lindhorst, Cynthia T. Welsh, Mary N. Herring, Adam Braun, Bruce H. Thiers
Objective: The aim of this study was to assess gadolinium deposition in the skin of a patient with normal renal function, based on estimated glomerular filtration rate (eGFR) values greater than 59 ml/min/1.73 m2, following exposure to large cumulative

Gulf of Mexico Research Initiative 2014/2015 Hydrocarbon Intercalibration Experiment: Description and Results for SRM 2779 Gulf of Mexico Crude Oil and Candidate SRM 2777 Weathered Gulf of Mexico Crude Oil

April 20, 2016
Author(s)
Jacolin A. Murray, Lane C. Sander, Stephen A. Wise, Christopher M. Reddy
Following an open meeting entitled, “Hydrocarbon Chemistry QA/QC,” at the 2014 Gulf of Mexico Oil Spill and Ecosystem Science Conference in Mobile, Alabama, the Gulf of Mexico Research Initiative (GoMRI) initiated the Hydrocarbon Intercalibration

How to measure absolute P3HT crystallinity via 13C CPMAS NMR

April 20, 2016
Author(s)
Ryan C Nieuwendaal
We outline the details of acquiring quantitative 13C cross-polarization magic angle spinning (CPMAS) NMR spectra on the most ubiquitous polymer for organic electronics (OE) applications, poly(3-hexylthiophene) (P3HT), despite other groups’ claims that

Exciton Dynamics in Monolayer Transition Metal Michalcogenides

April 19, 2016
Author(s)
Galan A. Moody, John Schaibley, Xiaodong Xu
Since the discovery of semiconducting monolayer transition metal dichalcogenides, a variety of experimental and theoretical studies have been carried out seeking to understand the intrinsic exciton population decay and valley relaxation dynamics. Reports

Development of Two Fine Particulate Matter Standard Reference Materials ( 4 mm and 10 mm) for the Determination of Organic and Inorganic Constituents

April 13, 2016
Author(s)
Michele M. Schantz, Danielle Cleveland, N. Alan Heckert, John Kucklick, Stefan D. Leigh, Stephen E. Long, Jennifer Lynch, Karen E. Murphy, Rabia Oflaz, Adam L. Pintar, Barbara J. Porter, Savelas A. Rabb, Stacy Schuur, Stephen Wise, Rolf L. Zeisler
Two new Standard Reference Materials (SRMs), SRM 2786 Fine Particulate Matter ( 4 µm) and SRM 2787 Fine Particulate Matter ( 10 µm) have been developed in support of the US Environmental Protection Agency's National Ambient Air Quality Standards for

Size-exclusion chromatography of metal nanoparticles and quantum dots

April 8, 2016
Author(s)
Leena M. Pitkanen, Andre Striegel
This review presents an overview of size-exclusion chromatographic separation and characterization of noble metal nanoparticles (NPs) and quantum dots (QDs) over the past 25 years. The properties of NPs and QDs that originate from quantum and surface

Reclamation-NIST Exploratory Research Symposium Summary Report

April 6, 2016
Author(s)
Nicholas Barbosa, Jessica Torrey
The Reclamation-NIST Exploratory Research Symposium was held on August 4-5, 2015, at the Reclamation Denver Federal Center facility in Lakewood, CO, and the NIST facility in Boulder, CO. Staff from the Bureau of Reclamation and the National Institute of

A trade-off between the mechanical strength and microwave electrical properties of functionalized and irradiated carbon nanotube sheets

April 4, 2016
Author(s)
Tiffany S. Williams, Nate Orloff, James S. Baker, Sandi G. Miller, Bharath N. Natarajan, Jan Obrzut, Linda S. McCorkle, Marisabel Lebron-Colon, James Gaier, Michael A. Meador, James Alexander Liddle
Carbon nanotube sheets are novel implementation of carbon nanotubes that enable the tailoring of electrical and mechanical properties for applications in the automotive and aerospace industries. Small molecule functionalization and/or post-processing

Mid-infrared molecular spectroscopy in the quantum noise limit

March 31, 2016
Author(s)
David A. Long, Adam J. Fleisher, Qingnan Liu, Joseph T. Hodges
A cavity ring-down spectrometer was used to reach the quantum noise limit in the mid-infrared spectral region. Quantum noise was observed not only in the individual ring-down decay events but also in the corresponding ensemble statistics with a magnitude

Behavior of molecules and molecular ions near a field emitter

March 18, 2016
Author(s)
Ann C. Chiaramonti Debay, Baptiste Gault, Michael Ashton, Susan B. Sinnott, Michael P. Moody, David W. Saxey, D. K. Schreiber
The cold emission of particles from surfaces under intense electric fields is a process which underpins a variety of applications including atom probe tomography (APT), an analytical microscopy technique with near-atomic spatial resolution. Increasingly

The I/O transform of a chemical sensor

March 14, 2016
Author(s)
Nalin Katta, Douglas C. Meier, Kurt D. Benkstein, Stephen Semancik, Baranidharan Raman
A number of sensing technologies using a variety of transduction principles have been proposed for the purpose of non-invasive chemical sensing. A fundamental problem common to all sensing technologies is determining what features of the transducer's

Identification and Quantification of Seven Fused Aromatic Rings C26H14 Peri-Condensed Benzenoid Polycyclic Aromatic Hydrocarbons in a Complex Mixture of Polycyclic Aromatic Hydrocarbons from Coal Tar

March 2, 2016
Author(s)
Jorge O. Ona Ruales, Ruiz-Morales Yosadara, Stephen A. Wise
A methodology for the characterization of groups of PAHs using a combination of Normal Phase Liquid Chromatography with Ultraviolet-Visible Spectroscopy (NPLC/UV-vis) and Gas Chromatography with Mass Spectrometry (GC/MS) was used for the identification and

The Structural Origin of Electron Injection Enhancements with Fulleropyrrolidine Interlayers

February 25, 2016
Author(s)
Lee J. Richter, Hyunbok Lee, Christopher McNeil, Eliot Gann, Lars Thomsen, S. Park, J. Jeong, Z. A. Page, Egle Puodziukynaite, Todd Emrick, Alejandro Briseno, John C. Stephenson, Dean M. DeLongchamp
Market demand for ubiquitous, increased functionality products at low cost (the internet of things) is spurring development in additive, solution processing of electronic devices. Performance in thin-film functional devices, be they transistors, diodes, or

Uranium Ion Yields from Monodisperse Uranium Oxide Particles

February 24, 2016
Author(s)
Nicholas E. Sharp, John D. Fassett, David S. Simons
Secondary ion mass spectrometry (SIMS) plays an important role in nuclear forensics through its ability to identify isotopic ratios of particles accurately and precisely from samples obtained by inspectors [1]. As the particle mass can be on the order of

Gas Sensing with Bare and Graphene-covered Optical Nano Antenna Structures

February 17, 2016
Author(s)
Bhaven Mehta, Kurt D. Benkstein, Stephen Semancik, Mona E. Zaghloul
The motivation behind this work is to study the gas phase chemical sensing characteristics of optical (plasmonic) nano antennas (ONA) and graphene/graphene oxide-covered versions of these structures. ONA are devices that have their resonating frequency in

A Description of the Clinical Proteomics Tumor Analysis Consortium (CPTAC) Common Data Analysis Pipeline

February 10, 2016
Author(s)
Jeri S. Roth, Paul A. Rudnick, Sanford Markey, Yuri Mirokhin, Xinjian Yan, Dmitrii Tchekhovskoi, Stephen Stein, Nathan J. Edwards, Ratna R. Thangudu, Karen A. Ketchum, Christopher R. Kinsinger, Mehdi Mesri, Henry Rodriguez
The Clinical Proteomic Tumor Analysis Consortium (CPTAC) has produced large proteomics datasets from the mass spectrometric interrogation of tumor samples previously studied by The Cancer Genome Atlas (TCGA) program. The availability of the genomic and
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