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The microcalorimeter energy dispersive x-ray spectrometer, the silicon drift detector (SDD), and polycapillary x-ray optics are recent developments that have significantly advanced analytical x-ray spectrometry for electron beam instruments. The
This paper describes the development of a unique fluorescence based DNA diagnostic assay that does not require pre-labeling of the target oligomer prior to analysis. The assay uses polyacrylamide hydrogel plugs immobilized in microfluidic channels, and is
We report the technical basis for value assignments of several carbon and oxygen stable isotope reference materials distributed by NIST and the International Atomic Energy Agency (IAEA), and make recommendations regarding laboratory practices and future
The AGA8 Detail Characterization Method allows for the calculation of the compressibility factor (or pressure) for a natural gas mixture given known conditions of density and temperature. Iterative procedures can be used to calculate the density when the
John G. Gillen, Scott A. Wight, P Chi, Albert J. Fahey, Jennifer R. Verkouteren, Eric S. Windsor, D. B. Fenner
We are evaluating the use of bevel depth profiling Secondary Ion Mass Spectrometry (SIMS) for the characterization of layered semiconductor materials. In this procedure, a sub-degree angle bevel is cut into the analytical sample with an oxygen or cesium
This paper discusses methods of characterizing pore size distributions in low-k films by transmission electron microscopy (TEM), comparing both conventional TEM and high-angle annular dark-field scanning transmission electron microscopy (HAADF-STEM)
X-Ray Photoelectron Spectroscopy (XPS) is being used to an increasing extent for the characterization of new gate-oxide materials, particularly for the determination of film composition, uniformity, and thickness. A key parameter for film-thickness
Joseph M. Conny, D Klinedinst, Scott A. Wight, J L. Paulsen
The chemical, physical, and morphological complexity of atmospheric aerosol black carbon (BC) presents major problems in measurement accuracy. Methods based on thermal-optical analysis (TOA) are widely used for ambient air samples because no prior
Temperature measurement represents one of the most frequently and broadly used measurements, with a majority of products manufactured having temperature measurement devices as an esential component. The accuracy and precision of these temperature
Paper reports on the micro-Raman spectra of several high explosives heated to high temperatures, up to melting point. These spectroscopic results are correlated with the degradation and decomposition of these energetic materials.
This chapter describes the efficiency of studying temperature-dependent materials processing/property/performance relationships with MEMS-based microarrays. Varied types of microsamples (~ 100 m x 100 m in lateral dimension, and of thicknesses between ~ 10