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A round robin testing program for IEA Annex II Subtask 12 was carried out to test procedures for measurement of moisture and binder content of alumina granules. The granules provided by Japan, were produced with 1.0% binder by mass and contained
To resolve a long-standing lack of experimental data for electron impact ionization cross sections for inorganic molecules, or the availability of a reliable predictive method, we have developed a modified classical model. The model relies on the know or
X H. Zhang, Richard S. Gates, S Anders, Stephen M. Hsu
A high speed ball-on-inclined plane test method has been successfully used to evaluate the lubrication effectiveness of nanometer thick lubricant films on magnetic hard disks. The test evaluates the durability of the lubricant film and the carbon overcoat
A finite element analysis (FEA) was conducted to examine the feasibility of determining the shear modulus of an adhesive in a bonded geometry using a three-point bending test on a sandwich beam specimen. This specimen consists of two substrate bars bonded
Many applications new use different materials that are fabricated into structures to obtain the desired combination of properties or to suit particular needs. Ceramics and glasses are often combined with metallic materials for applications in the field of
Differential thermal analysis and thermogravimetric analysis (DTA/TGA) experiments have been completed in the BaF2-BaO-Y2O3-CuOx-H2O system at various oxygen pressures to determine the effect of adding BaF2 and H2O on the eutectic melting in the system BaO
Igor Levin, Julia Y. Chan, James E. Maslar, Terrell A. Vanderah, S M. Bell
Phase transitions and microwave dielectric properties in (1-x)Ca(Al0.5Nb0.5)O3 xCaTiO3 system were analyzed using X-ray and neutron powder diffraction, transmission electron microscopy, Raman spectroscopy, and dielectric measurements at microwave
P A. Netz, Francis W. Starr, H E. Stanley, M C. Barbosa
We present the results of molecular dynamics simulations of the extended simple point charge (SPC/E) model of water to investigate the thermodynamic and dynamic properties of stretched and supercooled water. We locate the liquid-gas spinodal, and confirm
Gabrielle G. Long, Lyle E. Levine, Richard J. Fields
New ultra-small-angle X-ray scattering (USAXS) facilities at 3rd generation synchrotron sources enjoy an additional 1 to 3 decades of X-ray brilliance over 2nd generation instruments, and can now quantify microstructural features from 3nm to 1.3 m in size
The determination of macroscopic properties of a material given its microscopic structure is of fundamental importance to materials science. We present an overview of two public domain programs which jointly predict macroscopic behavior, starting from an
The basic processes which control the solid state sintering of crystalline materials are reviewed. The stages of sintering are described and model which predict the evolution of the microstructure are presented. The effects of dihedral angle and pore
George D. Quinn, K Xu, R J. Gettings, J A. Salem, J Swab
New Standard Reference Material (SRM) 2100 is the first reference material in the world for the property fracture toughness for any class material. The SRM is for ceramic fracture toughness and may be used with any ceramic fracture toughness test method
An update of the NIST Standard Reference Database Number 30, the Structural Ceramics Database, has been completed. This update, designated here as Version June 2001, increases the number of reference citations from 431 to 731, and increases the number of
Benjamin P. Burton, N Dupin, S Fries, G Grimvall, A F. Guillermet, P Miodownik, W A. Oates, V Vinograd
Previous Ringberg working groups have discussed possible applications of first principles (FP) calculations to CALPHAD modeling, and have considered the problems from neglect of short range order (SRO) in CALPHAD Gibbs energy models [1]. Particular
T M. Regan, D C. Harris, R M. Stroud, J R. White, D W. Blodgett, K C. Baldwin, J A. Miragliotta, M E. Thomas, M J. Linevsky, J W. Giles, T A. Kennedy, M Fatemi, David R. Black
Neutron irradiation of sapphire with 1 1022(=1 MeV)/m2 increases the c-axis compressive strength by a factor of 3 at 600 C. The mechanism of strength enhancement is the retardation of r-plane twin propagation by radiation-induced defects. 10B and Cd
Two-phase aluminum-silicon-based alloys are widely used for premium quality castings for aerospace and automotive applications. While it is clear that silicon improves fluidity in the molten state, providing excellent castability to the alloy, and
Results are presented of lateral force measurements using the atomic force microscope (AFM) and the Surface Forces Apparatus (SFA). Two different probes are used in the AFM measurements: sharp silicon nitride tip (radius R {nearly equal to} 20 nm) and a
A preceding study of contact damage in a bilayer system consisting of a porcelain coating on a stiff Pd-alloy substrate is here expanded to investigate the role of substrate modulus and hardness. Bilayers are made by fusing the same dental porcelain onto
Effective medium theory is used to obtain a closed form expression for the porosity dependence of the bulk moduli of ceramics. The theory is illustrated with an application to data for high purity alumina that spans a volume fraction of porosity ranging
Structure and morphology development during isothermal crystallization and subsequent melting of syndiotactic polypropylene (sPP) was studied by time-resolved simultaneous small-angle X-ray scattering (SAXS) and wide-angle X-ray diffraction (WAXD) methods
William E. Wallace, Charles M. Guttman, B M. Fanconi, Barry J. Bauer
Saturated hydrocarbon polymers, polyethylene and polypropylene, are, by production volume, the most widely used of all synthetic polymers. Their molecular mass and molecular mass distribution (MMD) are critical in determining performance properties. There
The desorption/ionization process of matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOF-MS) is not completely understood. Characterization of synthetic polymers by MALDI-TOF-MS is very sensitive to the instrument and
P T. Wilson, Kimberly A. Briggman, John C. Stephenson, William E. Wallace, Lee J. Richter
Broad-bandwidth vibrationally-resolved sum frequency generation spectroscopy has been used to measure the molecular orientation distribution at polystyrene/dielectric interfaces. A novel microcavity structure allows isolation of the free or buried
In processing and end-use environments, and particularly nuclear fission reactor excursions, inorganic materials can be subjected to temperatures where liquids and vapors are significant components of the materials system. Classical characterization and
Charles C. Han, G Schmidt, A Nakatani, Alamgir Karim
The shear orientation of viscoelastic clay-polymer solutions was investigated by means of rheology, flow birefringence and small-angle neutron scattering (SANS). Oscillatory shear showed a linear visoelastic region and flow at higher stresses. With