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Barry J. Bauer, William E. Wallace, B M. Fanconi, Kathleen M. Flynn
Polyethylene and other polyolefins have not been amenable to mass spectrometric characterization of molecular mass distribution due to the ineffectiveness of conventional methods of cationization. The lack of polar groups, unsaturation, and aromaticity
Winnie K. Wong-Ng, Qingzhen Huang, Igor Levin, James A. Kaduk, J Dillingham, T J. Haugan, J Suh, Lawrence P. Cook
This paper investigates and reviews the trend of phase formation and crystal chemistry of selected series of compounds in SrO- R 2O 3-CuO x and related systems. Including in this discussion are (Ba,Sr) 2RCu 3O 6+x, where M = selected representative and
V Ferreiro, G Schmidt, Charles C. Han, Alamgir Karim
Nanocomposite polymeric materials offer unique properties such as mechanical, electrical, thermal, etc. Such property enhancements are induced not only by the physical presence of the filler but also by the interaction of the polymer with the filler and
J P. Kim, J G. Yeo, U Paik, Y S. Jung, Jinkyoo Park, Vincent A. Hackley
Ceria (CeO 2) slurry stability and oxide-to nitride selectivity in the shallow trench isolation chemical mechanical polishing (STI CMP) process were manipulated with the modification of ceria surface potentials. The electrophoretic mobility of CeO 2
Gabrielle G. Long, Andrew J. Allen, David R. Black, H E. Burdette, Daniel A. Fischer, R D. Spal, Joseph C. Woicik
Synchrotron Radiation Facilities, supported by the Materials Science and Engineering Laboratory of the National Institute of Standards and Technology, include beam stations at the National Synchrotron Light Source at Brookhaven National Laboratory and at
Charles E. Bouldin, June E. Sims, Howard Hung, J J. Rehr, A L. Ankudinov
Modeling x-ray absorption near edge structure (XANES) requires computationally intensive calculations. We show that parallel processing reduces the time required for XANES calculations by a factor of up to 50 over desktop computers. Parallel processing is
Because of its excellent osteoconductivity and bone-replacement capability, self-setting calcium phosphate cement (CPC) has been used in a number of clincal procedures. For more rapid resorption and concomitant osseointegration, methods were desired to
U Paik, J P. Kim, Y S. Yung, T Katoh, Jinkyoo Park, Vincent A. Hackley
As a silica slurry for interlayer dielectric CMP is prepared in the alkaline region to accelerate the chemical corrosion process of plasma enhanced tetraethylorthosilicate (PETEOS), Si is dissolved to the point where it will adversely affect the colloidal
The annual meeting of the American Crystallographic Association was held in Los Angeles, California, July 2126, 2001. The scientific sessions and the exhibit show were held in the Westin Bonaventure Hotel in downtownLos Angeles. The meeting was well
Electrospray ionization Fourier transform ion cyclotron resonance (ESI FTICR) mass spectrometry and matrix-assisted laser desorption/ionization time-of-flight (MALDI-TOF) mass spectrometry were applied to a complex silsesquioxane-siloxane copolymer resin
Silsesquioxanes or three-dimensional organosilicon resins, continue to generate much interest due to their unique structures and physical properties. Methyl silsesquioxanes can be formed at room temperature by simple acid catalyzed hydrolysis and
Results of Hertzian contact tests investigating the effects of superposed tangential loads on the critical conditions for radial cracking at the under-surfaces of brittle coatings on compliant substrates are reported. It is demonstrated that these effects
Scientists in the Crystallography Section at NIST/NBS made several outstanidng contributions greatly influencing the development and advancement of high pressure x-ray crystallography during the second-half of the 20th century. These milestone achievements
Walter G. McDonough, Joseph M. Antonucci, Joy Dunkers
In this study, the feasibility of using the microbond test (MBT) to probe the durability of the bond between a dental resin with differently silanized E-glass fibers was investigated. The E-glass fibers were silanized with equivalent amounts of two types
Winnie K. Wong-Ng, H F. McMurdie, C R. Hubbard, Alan D. Mighell
The Research Associateship Program of the Joint Committee on Powder Diffraction -International Centre for Diffraction Data (JCPDS-ICDD, now known as the ICDD) at NBS/NIST was a long-standing (over 35 years), successful, industry-government cooperation. The
R Chen, T Yalcin, William E. Wallace, Charles M. Guttman, L Li
Polyethylene's inert nature and difficulty to dissolve in conventional solvents at room temperature present special problems for sample preparation and ionization in mass spectrometric analysis. We present a study of ionization behavior of several
The NIST Ceramics Division maintains two materials property databases on the physical, mechanical, thermal, and other properties of high temperature superconductors and structural ceramics. Crystallographic data are featured prominently among the physical
Lawrence H. Robins, J T. Armstrong, Ryna B. Marinenko, Mark D. Vaudin, Charles E. Bouldin, Joseph C. Woicik, Albert J. Paul, W. R. Thurber, K E. Miyano, C A. Parker
The structural and optical properties of indium gallium nitride (InxGa1-xN) films with 0.04
Winnie K. Wong-Ng, Robert S. Roth, Terrell A. Vanderah, H F. McMurdie
Research in phase equilibria and crystallography has been a tradition in the Ceramics Division at NIST since the early thirties. In the early years, effort was concentrated in areas of Portland cement, ceramic glazes and glasses, instrument bearings and
Hydroxyapatite (HAP) belongs to a family of structurally and chemically related, sparingly soluble calcium phosphate (CP) salts [1], and is the structural prototype for the principal mineral component of bone and teeth [2]. Well-defined synthetic HAP has
The discretely diffracting aperiodic crystals termed quasicrystals, discovery at NBS in the early 1980s, have led to much interdisciplinary activity involving mainly materials science, physics, mathematics, and crystalography. It led to a new understanding
Winnie K. Wong-Ng, T Siegrist, G DeTitta, L Finger, H Evans, E Gabe, G Enright, J T. Armstrong, M Levenson, Lawrence P. Cook, C R. Hubbard
Through extensive international collaborations, a standard reference material, SRM 1990 (a set of 3500 units of Cr-doped Al2O3, or ruby sphere) for single crystal diffractometer alignment has been certified at NIST after a successful international round
The Versailles Project on Advanced Materials and Standards (VAMAS) was created in 1982 to support trade through international collaboration in pre-standards research in advanced materials. VAMAS has become self-sustaining through Memoranda of Understanding
N Gilra, C Cohen, R M. Briber, Barry J. Bauer, R C. Hedden, A Z. Panagiotopoulos
Small-angle neutron scattering (SANS) experiments were performed to determine the conformational behavior of unattached deuterated linear poly(dimethylsiloxane) (PDMS) chains of Mn = 58,300 g mol-1 in uncompressed and compressed end-linked protonated PDMS
Fracture mechanics often is applied in fractographic analyses in order to verigy that the correct feature has been identified as the fracture origin. This step has been codified in ASTM Standard C1322-96, Standard Practice for the Characterization of