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Search Publications by: Dr. Vincent A. Hackley (Fed)

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Displaying 101 - 125 of 153

Characterization of gold nanoparticles modified with single-stranded DNA using analytical ultracentrifugation and dynamic light scattering

August 3, 2010
Author(s)
James Falabella, Tae Joon Cho, Dean C. Ripple, Vincent A. Hackley, Michael J. Tarlov
We report the characterization of gold nanoparticles modified with thiol-terminated single stranded DNA using analytical ultracentrifugation and dynamic light scattering. Sedimentation coefficients of nominally 10 and 20 nm diameter gold nanoparticles

Competitive Adsorption of Thiolated Polyethylene Glycol and Mercaptoproprionic acid on Gold Nanoparticles Measured by Physical Characterization Methods

May 24, 2010
Author(s)
De-Hao D. Tsai, Frank W. DelRio, Robert I. MacCuspie, Tae Joon Cho, Michael R. Zachariah, Vincent A. Hackley
Adsorption kinetics between thiolated polyethylene glycol (SH-PEG) and mercaptoproprionic acid (MPA) on gold nanoparticles (Au-NP) were studied using dynamic light scattering (DLS) and electrospray differential mobility analysis (ES-DMA). Through a

Size Measurement of Nanoparticles using Atomic Force Microscopy

October 1, 2009
Author(s)
Jaroslaw Grobelny, Frank W. DelRio, Pradeep Namboodiri, Doo-In Kim, Vincent A. Hackley, Robert F. Cook
In this assay protocol, procedures for dispersing gold nanoparticles on various surfaces such that they are suitable for imaging and height measurement via intermittent contact mode AFM are first described. The procedures for AFM calibration and operation

First approaches to standard protocols and reference materials for the assessment of potential hazards associated with nanomaterials

September 19, 2009
Author(s)
Iseult Lynch, Hans Bouwmeester, Hans Marvin, Alan Casey, Gordon Chambers, Markus Berges, Martin Clift, Teresa Fernandes, Lise Fjellsbo, Lucienne Juillerat, Gert Roebben, Christoph Klein, Qinglan Wu, Vincent A. Hackley, Jean-Pierre Kaiser, Wolfgang Kreyling, C. Michael Garner, Peter Hatto, Kenneth Dawson, Michael Riediker
This report presents the outcome of the discussions of 60 experts in the field of safety assessment of manufactured NMs from academia, industry, government and non-profit organizations on some of the critical issues pertaining to the development of

ENABLING STANDARDS FOR NANOMATERIAL CHARACTERIZATION

August 13, 2009
Author(s)
Vincent A. Hackley, Martin Fritts, James F. Kelly, Anil K. Patri, Alan F. Rawle
A two-day international workshop was convened recently in order to scope out and address the urgent need for standards to accurately characterize the physico-chemical and biological properties of engineered nanomaterials. These standards are needed by

2nd Annual Tri-National Workshop on Standards for Nanotechnology - (NIST presentations)

December 10, 2008
Author(s)
Ronald G. Dixson, Jon R. Pratt, Vincent A. Hackley, James E. Potzick, Richard A. Allen, Ndubuisi G. Orji, Michael T. Postek, Herbert S. Bennett, Theodore V. Vorburger, Jeffrey A. Fagan, Robert L. Watters
A new era of cooperation between North American National Measurement Institutes (NMIs) was ushered by the National Research Council of Canada Institute for National Measurement Standards (NRC-INMS) on February 7, 2007 when the first Tri-National workshop

Preparation and Characterization of Patchy Particles

November 14, 2008
Author(s)
Thuy Chastek, Steven D. Hudson, Vincent A. Hackley
The self-assembled organization of partilces depends on the symmetry of their interactions, and strides are being made in producing nanoaparticles of controlled shape and functionalization. This paper describes the use of particles adsorption to control

Physical characterization methods for iron-oxide contrast agents encapsulated within a targeted liposome-based delivery system

April 16, 2008
Author(s)
John A. Dagata, Natalia Farkas, Cindi L. Dennis, Robert D. Shull, Vincent A. Hackley, Charles W. Yang, Kathleen F. Pirollo, Esther H. Chang
Intact liposome-based targeted nanoparticle delivery systems (NDS) are immobilized by nonselective binding and characterized by scanning probe microscopy (SPM) in a fluid imaging environment. The size, size distribution, functionality, and stability of an

Measurement of 100 nm and 60 nm Particle Standards by Differential Mobility Analysis

August 1, 2006
Author(s)
George W. Mulholland, Michelle K. Donnelly, Robert C. Hagwood, S R. Kukuck, Vincent A. Hackley, D Y. Pui
The peak particle size and expanded uncertainties (95 % confidence interval) for two new particle calibration standards are measured as 101.60 nm ? 1.02 nm and 60.68 nm ? 0.59 nm. The particle samples are polystyrene spheres suspended in filtered

Growth of Nanocrystalline Ceria Studied Using a USAXS Capillary Flow-Cell

July 1, 2006
Author(s)
Vincent A. Hackley, Andrew J. Allen, P R. Jemian, J M. Raitano, S W. Chan
Nanocrystalline ceria particles, with dimensions as small as 2 nm, have been prepared at room temperature by a soft chemical route using aqueous cerium nitrate and hexamethylenetetramine (HMT) as reactants. HMT decomposes slowly in aqueous solution