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Kerry M. Bauer, Illarion V. Turko, Karen W. Phinney
Isotope dilution mass spectrometry involves the addition of known quantities of isotope-labeled standards, that mimic native molecules, to biological samples. We evaluated three conventional internal standard platforms (synthetic peptides, QconCAT
Keith A. Gillis, James B. Mehl, James W. Schmidt, Michael R. Moldover
With calibrations of large flow meters in mind, we established the feasibility of determining the mass Mof argon gas contained within a 0.3 m 3 commercially manufactured pressure vessel ("tank") with a relative uncertainty of u r(M) = 0.0015 at 0.6 MPa by
Aaron M. Katzenmeyer, Glenn Holland, Kevin Kjoller, Andrea Centrone
Absorption spectroscopy and mapping from visible through mid-IR wavelengths has been achieved with spatial resolution exceeding the limit imposed by diffraction, via the photothermal induced resonance technique. Correlated vibrational (chemical), and
A free-space transmission-reflection measurement method for the non-destructive electrical characterization of carbon nanotube based composites was developed. Specifically, this versatile method measures the dielectric properties of the sample in the Q
Jason A. Widegren, Allan H. Harvey, Mark O. McLinden, Thomas J. Bruno
The influence of the carrier gas on vapor pressure (psat) measurements by the gas saturation method was studied. Eicosane (C20H42) was used as the test compound. Helium (He), nitrogen (N2), carbon dioxide (CO2), and sulfur hexafluoride (SF6) were chosen as
Justin M. Gorham, Jeremiah W. Woodcock, Keana C. Scott
FOREWORD This NIST Special Publication (SP) is one in a series of NIST SPs that address research needs articulated in the National Nanotechnology Initiative (NNI) Environmental, Health, and Safety Research Strategy published in 2011 [1]. This Strategy
As part of an international project to benchmark facilities for measuring the strain dependence of critical current in ITER Nb 3Sn strands, direct measurement of local strain exerted on Nb 3Sn filaments was attempted at cryogenic temperature by means of
Aaron Hudlemeyer, Daniel S. Sawyer, Christopher J. Blackburn, Vincent Lee, Mark Meuret, Craig M. Shakarji
Interim testing of laser trackers can be problematic due to the lack of high precision, long length artifacts that maintain their calibrated lengths during measurement. Gravitational loading, fixturing forces, and changes in the atmospheric conditions can
Daniel R. Schmidt, Douglas A. Bennett, James P. Hays-Wehle, Daniel S. Swetz, Joel N. Ullom, Andrew Hoover, Mark Croce, Michael W. Rabin, Evelyn Bond, Terry Holesinger, Gerd Kunde, Laura Wolfsbereg
We have developed a new category of sensor for measurement of the 240Pu/239Pu mass ratio from aqueous solution samples with advantages over existing methods. Aqueous solution plutonium samples were evaporated and encapsulated inside of a gold foil absorber
Proposal for a Test Procedure: Animal Bedding (Bedding), also called pet or stall bedding, litter, or simply bedding is generally sold by dry volume in compressed or uncompressed packages. Based on numerous failed inspections of packaged animal bedding the
Animal Bedding (bedding), also called pet or stall bedding, litter or simply bedding, is generally sold by dry volume in compressed or uncompressed packages. Based on numerous failed inspections of packaged animal bedding, the Office of Weights and
Yvonne B. Gerbig, Chris A. Michaels, Robert F. Cook
Indentation-induced phase transformation processes were studied by in situ Raman imaging of the deformed contact region of silicon, employing a Raman spectroscopy-enhanced instrumented indentation technique. This is, to our knowledge, the first sequence of
James A. Fedchak, Karl Jousten, Kenta Arai, Janez Setina
The spinning rotor gauge (SRG) is a common transfer standard in key comparisons (KCs) and other intercomparisons for pressures in the range of 1.0 × 10-4 Pa to 1.0 Pa. To make absolute pressure measurements using a SRG, a calibration factor, known as the
Primary focus of this paper is to review existing test methods that quantify steam burn injuries and to compare bench-scale test methods that use pre-wetted samples as opposed to external steam exposures to evaluate heat and moisture transfer in protective
Stephan Schlamminger, Richard L. Steiner, Darine El Haddad, David B. Newell, Frank C. Seifert, Leon S. Chao, Ruimin Liu, Edwin R. Williams
Researchers at the National Institute of Standards and Technology have been using a watt balance, NIST-3, to measure the Planck constant h for over ten years. Two recently published values disagree by more than one standard deviation. The motivation for
Andrew J. Allen, Janos Hajdu, Anke R. Kaysser-Pyzalla
It is now one year since all International Union of Crystallography (IUCr) journals became online only, and this is just one of the developments during the International Year of Crystallography, IYCr 2014. Perhaps, most conspicuously, IUCrs new flagship
Shonali Nazare, William M. Pitts, Szabolcs Matko, Rick D. Davis
This study reports on the smoldering propensity of commercially available barrier fabrics (BFs) in a small-scale upholstered seating mock-up configuration. Most commercially available BFs are smolder resistant when tested alone over a standard flexible
Additive manufacturing (AM) processes are capable of producing highly complex and customized parts, without the need for dedicated tooling, and can produce parts directly from the part design information. These types of processes are poised to
Joshua B. Martin, Winnie K. Wong-Ng, Martin L. Green
Comparative measurements of the Seebeck coefficient are challenging due to the diversity of instrumentation and measurement protocols. With the implementation of standardized measurement protocols and the use of Standard Reference Materials (SRMs®), for
Establishing an acceptable method of sale is a critical first step in the development of a fair and competitive marketplace for any commodity. For instance, milk could be sold by volume, or it could be sold by weight. If both were allowed, the measurement
Defensive code is instructions added to software for the purpose of hardening it against uncontrolled failures and security problems. It is often assumed that defensive code causes a significant reduction in software performance, which justifies its
Justin M. Gorham, Karen E. Murphy, Jingyu Liu, Dimitri Tselenchuk, Gheorghe NMN Stan, Thao M. Nguyen, Richard D. Holbrook, Michael R. Winchester, Robert F. Cook, Robert MacCuspie, Vincent A. Hackley
FOREWORD This NIST special publication (SP) is one in a series of NIST SPs that address research needs articulated in the National Nanotechnology Initiative (NNI) Environmental, Health, and Safety Research Strategy published in 2011 [1]. This Strategy
Ferran Gibert, Miquel Nofrarias, Nico Karnesis, Lluis Gesa, Victor Martin, Ignacio Mateos, Alberto Lobo, Reinhold Flatscher, Domenico Gerardi, Johannes Burkhardt, Ruediger Gerndt, David I. Robertson, Henry Ward, Paul McNamara, Felipe Guzman, Martin Hewitson, Ingo Diepholz, Jens Reiche, Gerhard Heinzel, Karsten Danzmann
During the on-station thermal test campaign of the LISA Pathfinder, the diagnostics subsystem was tested in nearly space conditions for the first time after integration in the satellite. The results showed the compliance of the temperature measurement
Sao F. Cheung, Kyle Anderson, Meiyao Wang, Illarion Turko
Quantification by targeted proteomics has largely depended on mass spectrometry and isotope-labeled internal standards. In addition to traditionally used recombinant proteins or synthetic peptides, concatenated peptides (QconCATs) were introduced as a
We present a simple and straightforward approximate approach to removing resonant artifacts that arise in the material parameters extracted near half-wavelength resonances that arise from transmission/reflection (T/R) measurements on low-loss materials. In