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The mission of the Ceramics Division can be stated as follows:Work with industry, standards bodies, academia, and other government agencies in providing the leadership for the Nation's measurements and standards infrastructure for ceramic materials.The
Terrell A. Vanderah, Winnie K. Wong-Ng, B H. Toby, V. M. Browning, Robert D. Shull, Richard G. Geyer, Robert S. Roth
Single crystals of Ba 6Fe 45Ti 17O 106 and BaFe 11Ti 3O 23 were obtained as major and minor co-products, respectively, by slow-cooling an off-stoichiometric BaO:Fe 2O 3:TiO 2 melt. The former compound exhibits variable stoichiometry Ba 6Fe 48-xTi 14+xO 106
Lawrence H. Robins, Albert J. Paul, C A. Parker, J C. Roberts, S M. Bedair, E L. Piner, N A. El-Masry
In xGa 1-xN films with x=0.06 to x=0.49 were characterized by optical transmittance, Raman, and photoluminescence excitation spectroscopies. Previous microstructural characterizations detected phase separation only in films with x>0.2. The transmittance
American Society for Testing and Materials (ASTM) standard test method PS 070 has been created for fracture toughness of advanced ceramics. It includes three test methods which use beams in bending: chevron notch (CNB), single-edged precracked beam (SEPB)
Amalgam creep has been identified as a key parameter associated with marginal breakdown and corrosion. Recently, a consolidated silver powder was proposed as a mercury-free alternative to amalgam. The aim of the present study was to characterize the time
Small-angle neutron scattering was used to measure the effect of water-to-cement ratio [w/c] and cement batch variation on the surface area of ordinary Portland cement [opc] paste after hydration for 28 days at room temperature, and to measure the
U Beck, Douglas T. Smith, G Reiners, S J. Dapkunas
Mechanical properties, i.e., hardness and elastic modulus, of amorphous Si 02 and Si 3N^4^ PE-CVD coatings have been studied for two coating thicknesses (0.1 υm and 1.0 υm) and two substrate materials (fused silica, i.e., Herasil, and borosilicate glass, i
A study is made of the damage resistance of silicon nitride bilayer consisting of a hard overlayer [coating] on a soft underlayer [substrate]. The two layers are fabricated with different starting powders, to provide distinctive elongate-grain
Finely dispersed systems such as emulsions and colloidal suspensions are recognized as playing a critical role in many important industrial processes. Many of these systems are quite concentrated, and significant needs exist to develop measurement
Over the past decade, a multiple small-angle neutron scattering (MSANS) formalism has been developed to enable researchers to derive microstructural parameters from multiply-scattered small-angle neutron data. The MSANS formalism is particularly useful in
Joseph C. Woicik, J O. Cross, Charles E. Bouldin, Bruce D. Ravel, J G. Pellegrino, B W. Steiner, S G. Bompadre, L B. Sorensen, K E. Miyano, J P. Kirkland
Diffraction anomalous fine-structure measurements performed at both the Ga and As K edges have determined the Ga-As bond length to be 2.442 ± 0.005 {Angstrom} in a buried, 213 {Angstrom} thick Ga^0.78^In 0.22As layer grown coherently on GaAs(001). This
Joseph C. Woicik, J A. Gupta, S P. Watkins, E D. Crozier
The bond-length strain in a series of strained, buried Ga 1-xIn xAs thin-alloy films grown coherently on InP(001) has been determined by high-resolution extended x-ray absorption fine-structure measurements. Comparison with a random-cluster calculation
A parameter that is often used in the assessment of cooling efficiency in grinding is the amount of fluid that flows through the grinding zone. This paper shows that when grinding with wheels possessing no bulk porosity, only a portion of the flow through
The development of particle characterization methods based on electroacoustic effects is reviewed and their application in various areas of ceramic powder processing is stressed. Electroacoustics is a term used to describe the coupling between electric and
An overview of hardness testing of ceramics is presented. Conventional test methods are discussed, particularly with respect to major sources of experimental error and standardization. Two NIST Standard Reference Materials (SRMs) are highlighted. Emerging
The chemical reactions and the compositional characteristics of liquids which lead to the phase formation of the Pb-2223 ((Bi,Pb):Sr:Ca:Cu:O) superconductor have been studied for a precursor composition of Bi 1.8Pb o.4Sr 2Ca 2.2Cu 3O x. The combined
The NIST WWW Structural Ceramics Database (WebSCD available at: http://www.ceramics.nist.gov/srd/scd/scdquery.htm) provides evaluated materials property data for a wide range of advanced ceramics known variously as structural ceramics, engineering ceramics
Accurate measurements of the surface area of cement based materials using small-angle neutron scattering (SANS) require determination of the neutron scattering contrast between the C-S-H gel and H6d2^O. Because the C-S-H gel has a poorly understood
In this article we review the nature and mechanics of damage induced in ceramics by spherical indenters, from the classical studies of Hertz over a century ago to the present day. Basic descriptions of continuum elastic and elastic-plastic contact stress
This NIST web site will complement ASTM standard C1322-96, Standard Practice for Fractography and Characterization of Fracture Origins in Advanced Ceramics. The objectives of the web site are to prove a thumbnail sketch of the standard, promote its usage
A world wide web (www) site focussing on NIST efforts in ultrasonic applications development for ceramic processing in fluid-based systems. This site contains information related to facilities, instrumentation, research, and ultrasonic techniques in
J Ilavsky, Gabrielle G. Long, Andrew J. Allen, L Leblanc, M Prystay, C Moreau, Alan H. Band
The microstructure of plasma-sprayed deposits [PSD] is dominated by two void systems-interlamellar pores and intralamellar cracks - each with a different anisotropy. Varying anisotropies and crack-to-pore ratios within PSDs are responsible for the
Fracture toughness data, as represented by the critical stress intensity factor, K Ic, and the fracture energy, γ, have been compiled from publicly accessible sources for a wide range of brittle materials with an emphasis on structural ceramics and closely
A recently developed model of curvature-driven, two-dimensional microstructure evolution is modified to include elastic strain energy at solid-fluid interfaces as an additional driving force for mass transport. Local phase distributions within a digital