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Chemistry

Analytical chemistry

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Displaying 426 - 450 of 4041

An untargeted approach to determine the authenticity of Ginkgo biloba L. plant materials and dried leaf extracts by liquid chromatography-mass spectrometry (LC-HRMS) and chemometrics.

August 5, 2020
Author(s)
Meryl B. Cruz, Benjamin Place, Laura J. Wood, Aaron A. Urbas, Werickson Rocha, Andrzej Wasik
The lack of stringent regulations regarding raw materials for herbal supplements used for medicinal purposes has been a constant challenge in the industry. Ginkgo biloba L. leaf extracts attract consumers because of the supposed positive effect on mental

The Art in Science of MicroTAS 2019†

July 28, 2020
Author(s)
Gregory A. Cooksey
The 2019 MicroTAS conference (the 23rd International Conference of Miniaturized Systems for Chemistry and Life Sciences) held in Basel, Switzerland, brought great opportunities to viewinspiring microscale compositions. Many of the best images were

Increasing the Coverage of a Mass Spectral Library of Milk Oligosaccharides Using a Hybrid- Search-Based Bootstrapping Method and Milks from a Wide Variety of Mammals

July 8, 2020
Author(s)
Concepcion A. Remoroza, Tytus D. Mak, Yuri A. Mirokhin, Sergey L. Sheetlin, Xiaoyu Yang, Stephen E. Stein, Power L. Michael, San Andres V. Joice, Yuxue Liang
This study significantly expands both the scope and method of identification for construction of a previously reported tandem mass spectral library of 74 human milk oligosaccharides (HMOs) derived from results of LC-MS/MS experiments. In the present work

Determination of molecular mass 302 polycyclic aromatic hydrocarbons in Standard Reference Material 1597a by reversed-phase liquid chromatography and constant energy synchronous fluorescence spectroscopy

July 3, 2020
Author(s)
Hugh V. Hayes, Walter B. Wilson, Anthony M. Santana, Andres D. Campiglia, Lane C. Sander, Stephen A. Wise
High-performance liquid chromatography with fluorescence detection is often used for the analysis of polycyclic aromatic hydrocarbons (PAH) in environmental extracts. Since fluorescence chromatograms are usually recorded at a single set of excitation and

IFCC working group recommendations for correction of bias caused by non-commutability of a certified reference material used in the calibration hierarchy of an end-user measurement procedure

June 1, 2020
Author(s)
Johanna Camara, W. Greg Miller, Jeffrey R. Budd, Neil Greenberg, Weykamp Cas, Harald Althaus, Heinz Schimmel, Mauro Panteghini, Vincent Delatour, Ferruccio Ceriotti, Thomas Keller, Douglas Hawkins, Robert Rej, Finlay MacKenzie, Elina van der Hagen, Hubert W. Vesper
Establishing metrological traceability to a matrix-based certified reference material (CRM) that has been validated to be commutable among a group of measurement procedures (MPs) is central to producing equivalent results for a measurand in clinical

Embracing Uncertainty: Modeling Uncertainty in EPMA - Part I

May 21, 2020
Author(s)
Nicholas Ritchie
This is the first in a series of articles which present a new framework for computing the uncertainty in electron excited X-ray microanalysis measurements. This article will discuss the framework and apply it to a handful of simple but useful sub

Infrared and Raman chemical imaging and spectroscopy at the nanoscale

May 19, 2020
Author(s)
Dmitry Kurouski, Alexandre Dazzi, Renato Zenobi, Andrea Centrone
The advent of nanotechnology, and the need to understand the chemical composition at the nanoscale, has stimulated the convergence of IR and Raman spectroscopy with scanning probe methods, resulting in new nanospectroscopy paradigms. Here we review two of
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