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Franziska Grohn, Y A. Akpalu, Barry J. Bauer, Eric J. Amis
Poly(amidoamine) (PAMAM) dendrimers are used to create organic-inorganic hybrid colloids in aqueous solution. The formation of gold colloids upon reduction of a gold salt precursor serves as model reaction to study influences on the resulting
Eric J. Amis, Barry J. Bauer, Alamgir Karim, Jack F. Douglas, A Topp, F I. Groehn, T J. Prosa, B D. Viers, D W. Liu, K A. Barnes, C L. Jackson, G Nisato
A M. Gabelnick, A T. Capitano, S M. Kane, J L. Gland, Daniel A. Fischer
The oxidation of propylene on the Pt(111) surface has been characterized in oxygen pressures up to 0.02 torr using fluorescence yield near -edge spectroscopy (FYNES) and temperature programmed fluorescence yield near-edge spectroscopy (TP-FYNES) above the
J A. Rodriguez, T Jirsak, J Dvorak, S Sambasivan, Daniel A. Fischer
Synchrotron-based high-resolution photoemission and x-ray absorption near-edge spectroscopy (XANES) have been used to study the interaction of NO 2 with polycrystalline surfaces of metallic zinc and zinc oxide. NO 2 exhibits a complex chemistry on metallic
Mineral fillers are added to extend and modify physical properties of polymers. To achieve porcessing control of mixing, real-time measurements are needed. Previuos work has shown that dielectric sensors can measure concentrations of fillers in non-polar
Gale A. Holmes, Donald L. Hunston, Walter G. McDonough, R C. Peterson
One of the critical factors controlling the long-term performance and durability of composites in structural applications is the interfacial shear strength (IFSS). The single fiber composite (SFC) test has been viewed by many as the best test for
Walter G. McDonough, Joy P. Dunkers, Gale A. Holmes, Richard~undefined~undefined~undefined~undefined~undefined Parnas
The objective of our research was to extend the use of the single fiber fragmentation test to include fast reacting resin systems and to determine the effect of gelation time on interfacial shear properties. To do this work, we developed a processing
Igor Levin, Leonid A. Bendersky, Robert S. Roth, Terrell A. Vanderah
Four Ca 4Nb 2O 9=Ca(Ca1/3Nb 2/3)O 3 polymorphs based on ABO 3 perovskite-like structure were identified. These polymorphs feature three different arrangements of Ca/Nb cations on B-sites of perovskite. In three of the polymorphs, cation ordering is
Ceramics are increasingly being considered for wear resistant applications. The design and prediction of ceramics wear, however are lacking behind metals. This paper addresses the ability to predict wear of ceramics by examining a large data base of four
M C. Shen, Stephen M. Hsu, John A. Tesk, A Christou
A versatile wear tester has been designed and built. The initial study showed that that with this tester, tes procedures can be developed to achieve clinically relevant simulations in a short time. With the continuously monitored force traces, this tester
C I. Lang, Frank S. Biancaniello, Stephen D. Ridder, D Shechtman
Powders for thermal spray coating were produced by gas atomization in NIST's Supersonic Inert Gas Metal Atomizer (SIGMA). Bulk speciments were produced by Hot Isostatic Press (HIP) consolidation at NIST, and plasma sprayed coatings were produced at Ames
Bruce D. Ravel, Eric J. Cockayne, E Newville, K M. Rabe
The narrow band-gap semiconductor Pb 1-xGe xTe has a low-temperature ferroelectric rhombohedral phase whose average structure is a distorted rocksalt structure. We have measured the Extended X-Ray-Absorption Fine-Structure (EXAFS) spectra of Pb 1-xGe xTe
D K. Kim, Yeon-Gil G. Jung, I M. Peterson, Brian R. Lawn
Contact damage modes in cyclic loading with spheres are investigated in three relatively brittle ceramics, soda-lime glass, porcelain and fine-grain silicon nitride, in moist environments. Initial damage at small numbers of cycles and low loads consists of
We present a technique for determining the texture of a polycrystalline material based on the measurement of the orientation of a number of individual grains. We assume that the sample has fiber texture and that the texture can be characterized by a
Structure formation during the isothermal crystallization of a linear polyethylene (M w = 32,1000 g/ mol, M w/M n = 1.1) has been monitored by simultaneous real time small-angle x-ray scattering (SAXS) and wide angle x-ray scattering (WAXS) with
T L. Lee, M Pillai, Joseph Woicik, G Labanda, P Lyman, S A. Barnett, Michael Bedzyk
X-ray standing wave measurements were used to study the strain in one monolayer of pseudobinary alloy InxGa1-xAs buried in GaAs(001). The measured In position along the [001] direction, which exhibits a linear dependence on the In concentration x, supports
R P. Jensen, William E. Luecke, N P. Padture, Sheldon M. Wiederhorn
We have characterized the high-temperature subcritical crack growth and oxidation resistance of a liquid-phase-sintered (LPS) SiC with 20% volume fraction yttrium aluminum garnet (YAG) second phase. Constant stress rate testing in air in the temperature
S S. Das, J Zhuang, A P. Andrews, S C. Greer, Kathleen M. Flynn, William R. Blair
We have studied the time development of the molecular mass distribution (MWD) of living bifunctional poly(α-methylstyrene) in tetrahydrofuran after a quench to 21 K below the polymerization temperature T p. We see an intermediate Gaussian distribution
S M. Choi, R M. Briber, Barry J. Bauer, A Topp, M Gauthier, L Tichagwa
Small angle neutron scattering was used to measure the size and shape of arborescent graft polymers as a function of generation number in solution. The radius of gyration of arborescent graft polymers was found to be almost independent of temperature in
Fully relaxed, planewave pseudopotential calculations of total energies were performed for three ordered perovskite related supercells in each of the eight different stoichiometries of A(B 1/3B' 2/3)O 3; A=Pb, Ba and B=Zn, Mg and B' = Nb, Ta; and the four