Instrument Purpose
To provide depth-resolved structural and magnetic profiles of thin films and multilayers with sub-nanometer precision, with capabilities for full polarization in high magnetic fields, for the most demanding investigations of quantum materials and spintronic devices.
The NCNR Advantage
- Dedicated Polarization Analysis: PBR is purpose-built for Polarized Neutron Reflectometry (PNR). It can independently control the spin state of incident and reflected neutrons, allowing researchers to obtain depth profiles of both the structure and vector magnetization in multilayer films.
- High-Field Capability: PBR supports a superconducting magnet up to 3 T, enabling measurements of field-dependent magnetic transitions.
- Low-Background Cold Source: Located on the NGD cold neutron guide, the instrument benefits from a high-flux, low-noise environment, enabling the measurement of reflectivity down to 10-7, essential for probing ultra-thin films.
- In Situ Measurement Capability: PBR accommodates a wide range of sample environments, including high field magnets and low temperature refrigerators, that are optimized for in situ measurements of thin films in response to variations in temperature, magnetic field, electric field, and other stimuli.
Research Domains
- Spintronics: Mapping the profile of the vector magnetization in spin-based electronic model systems and prototypes such as Magnetic Tunnel Junctions (MTJs) and Giant Magnetoresistance (GMR) sensors.
- Quantum Materials: Probing proximity effects at interfaces in layered materials that include topological insulators, frustrated low-dimensional magnets, and Dirac and Weyl Semimetals.
- Magneto-Ionics: Characterizing the voltage-induced magnetization change in coupled magnetostrictive layers and the motion of O, H, and N ions in magneto-ionic device prototypes.
- Superconductors: Obtaining the penetration depth profile in conventional spin-singlet and unconventional spin-triplet superconducting films.
What You Can Measure
- Specular Reflectivity: Absolute determination of structural and magnetic layer thicknesses (2 nm to 200 nm), density, and roughness.
- Magnetic Depth Profiling: Determining the direction and magnitude (i.e., vector magnetization) with sub-nanometer depth resolution.
- Interface Roughness: Quantifying the "sharpness" of the structural and magnetic transitions between layers.
Technical Specifications
| Parameter | Specification |
|---|
| Source Type | Cold Neutron Guide (NGD) |
| Monochromator | Highly Oriented Pyrolytic Graphite (PG 002) |
| Wavelength (𝜆) | 4.75 Å (fixed monochromatic) |
| Polarization | Fe/Si Supermirror polarizers and Mezei flippers |
| Accessible Q-Range | 0.005 Å-1 to 0.25 Å-1 |
| Resolution (Δ Q/Q) | 1 % |
| Detector | 3He pencil detector |
| Sample Geometry | Vertical |
Specialized Sample Environments
- Magnetic Fields: Supporting a superconducting magnet up to 3 T and electromagnets up to 700 mT for magnetic thin-film studies.
- Temperature Control: Standard range of 5 K to 315 K; specialized furnaces available for higher temperatures.
- Electric Fields: Capability to apply up to 2 kV across thin-film samples during measurement.
Expertise & Support
- Instrument Scientists: Direct support from experts in magnetism and interfacial science, Dr. Julie Borchers and Dr. Charles Majkrzak.
- Software Suite:
- NICE Control: Fully scriptable instrument environment for polarization experiments.
- Reductus: Web-based application providing support for data reduction of reflectivity data.
- Refl1D: State-of-the-art Python-based modeling for simultaneous structural and magnetic refinement.
Access & Resources
Instrument Contacts
charles.majkrzak [at] nist.gov (charles[dot]majkrzak[at]nist[dot]gov)
(301) 975-5251
julie.borchers [at] nist.gov (julie[dot]borchers[at]nist[dot]gov)
(301) 975-6597