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Search Publications by: Stephen Wise (Assoc)

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Displaying 26 - 50 of 413

Development of Standard Reference Material (SRM) 2973 Vitamin D Metabolites in Frozen Human Serum (High Level)

July 24, 2017
Author(s)
Susan Tai, Michael Nelson, Brian Lang, Karen W. Phinney, Lane C. Sander, James H. Yen, J. M. Betz, Christopher T. Sempos, Stephen Wise
The National Institute of Standards and Technology (NIST), in collaboration with the National Institutes of Health, Office of Dietary Supplements (NIH-ODS) and the Vitamin D Standardization Program (VDSP), has recently issued a new serum-matrix Standard

Qualitative characterization of SRM 1597a Coal Tar for polycyclic aromatic hydrocarbons and methyl-substituted derivatives via normal-phase liquid chromatography and gas chromatography/mass spectrometry

June 29, 2017
Author(s)
Walter B. Wilson, Hugh Hayes, Lane C. Sander, Andres Campiglia, Stephen A. Wise
A normal-phase liquid chromatography (NPLC) fractionation procedure was developed for the characterization of a complex mixture of polycyclic aromatic hydrocarbons (PAHs) from a coal tar sample (Standard Reference Material (SRM) 1597a). Using a semi

Revisiting Shape Selectivity in Liquid Chromatography for Polycyclic Aromatic Hydrocarbons (PAHs) - Six-Ring and Seven-Ring Cata-condensed PAH Isomers of Molecular Mass 328 Da and 378 Da

June 28, 2017
Author(s)
Jorge O. Ona Ruales, Lane C. Sander, Walter Brent Wilson, Stephen Wise
The relationship of reversed-phase liquid chromatography retention on a polymeric C18 stationary phase and the shape of polycyclic aromatic hydrocarbons (PAHs) was investigated for three-ring to seven-ring cata-condensed isomers. We report the first

Normal-phase liquid chromatography retention behavior of polycyclic aromatic hydrocarbon and their methyl-substituted derivatives on an aminopropyl stationary phase

June 16, 2017
Author(s)
Walter B. Wilson, Hugh Hayes, Lane C. Sander, Andres D. Campiglia, Stephen A. Wise
Retention indices for 124 polycyclic aromatic hydrocarbons (PAHs) and 62 methyl-substituted (Me-) PAHs were determined using normal-phase liquid chromatography (NPLC) on a aminopropyl (NH2) stationary phase. PAH retention behavior on the NH2 phase is

Development of an Improved Standard Reference Material for Vitamin D Metabolites in Human Serum

April 4, 2017
Author(s)
Karen W. Phinney, Susan S. Tai, Mary Bedner, Johanna Camara, Rosalind R. Chia, Lane C. Sander, Katherine E. Sharpless, Stephen A. Wise, James H. Yen, Rosemary L. Schleicher, Madhulika Chaudhary-Webb, Khin L. Maw, Yasamin Rahmani, Hubert W. Vesper, Joseph M. Betz, Joyce Merkel, Christopher T. Sempos, Paul M. Coates, Ramon Durazo-Arvizu, Kurtis Sarafin, Stephen P. Brooks

Retention behavior of alkyl-substituted polycyclic aromatic sulfur heterocycle isomers in gas chromatography on stationary phases of different selectivity

January 10, 2017
Author(s)
Walter B. Wilson, Lane C. Sander, Jorge O. Ona Ruales, Stephanie Mossner, Leonard M. Sidisky, Milton Lee, Stephen A. Wise
Retention indices for 10 sets of alkyl-substituted polycyclic aromatic sulfur heterocycles (PASHs) isomers (total of 80 PASHs) were determined using gas chromatography with three different stationary phases: a 50% phenyl phase, a 50% liquid crystalline

Retention behavior of isomeric polycyclic aromatic sulfur heterocycles in gas chromatography on stationary phases of different selectivity

January 10, 2017
Author(s)
Walter B. Wilson, Lane C. Sander, Jorge O. Ona Ruales, Leonard M. Sidisky, Milton Lee, Stephen A. Wise
Retention indices for 70 polycyclic aromatic sulfur heterocycles (PASHs) were determined using gas chromatography with three different stationary phases: a 50% phenyl phase, a 50% liquid crystalline dimethylpolysiloxane (LC-DMPS) phase, and an ionic liquid

The influence of the aromatic character in the gas chromatography elution order: the case of polycyclic aromatic hydrocarbons

November 8, 2016
Author(s)
Jorge O. Ona Ruales, Walter B. Wilson, Federica Nalin, Lane C. Sander, Patricia Schubert, Stephen A. Wise
A link between the aromatic character of polycyclic aromatic hydrocarbons (PAHs) and gas chromatography (GC) elution order in columns with a polysiloxane backbone in the stationary phase is reported for the first time. The aromatic character was calculated

Interlaboratory Analytical Comparison of Fatty Acid Concentrations in Serum or Plasma

September 20, 2016
Author(s)
Michele M. Schantz, Carissa Powers, Schleicher Rosemary, Joseph Betz, Stephen A. Wise
The National Institute of Standards and Technology, in collaboration with the National Institutes of Health Office of Dietary Supplements and the Centers for Disease Control and Prevention, is conducting an accuracy-based program for improving the

Summary of results from the 2014/2015 Hydrocarbon Intercalibration Experiment (HIE)

May 27, 2016
Author(s)
Christopher Reddy, Stephen Wise, Lane C. Sander, Jacolin Murray
Following an open meeting entitled, "Hydrocarbon Chemistry QA/QC," at the 2014 Gulf of Mexico Oil Spill and Ecosystem Science Conference in Mobile, Alabama, the Gulf of Mexico Research Initiative (GoMRI) initiated the Hydrocarbon Intercalibration

Gulf of Mexico Research Initiative 2014/2015 Hydrocarbon Intercalibration Experiment: Description and Results for SRM 2779 Gulf of Mexico Crude Oil and Candidate SRM 2777 Weathered Gulf of Mexico Crude Oil

April 20, 2016
Author(s)
Jacolin A. Murray, Lane C. Sander, Stephen A. Wise, Christopher M. Reddy
Following an open meeting entitled, “Hydrocarbon Chemistry QA/QC,” at the 2014 Gulf of Mexico Oil Spill and Ecosystem Science Conference in Mobile, Alabama, the Gulf of Mexico Research Initiative (GoMRI) initiated the Hydrocarbon Intercalibration

Development of Two Fine Particulate Matter Standard Reference Materials (

April 13, 2016
Author(s)
Michele M. Schantz, Danielle Cleveland, N. Alan Heckert, John Kucklick, Stefan D. Leigh, Stephen E. Long, Jennifer Lynch, Karen E. Murphy, Rabia Oflaz, Adam L. Pintar, Barbara J. Porter, Savelas A. Rabb, Stacy Schuur, Stephen Wise, Rolf L. Zeisler
Two new Standard Reference Materials (SRMs), SRM 2786 Fine Particulate Matter (

INTERLABORATORY TRIAL FOR MEASUREMENT OF VITAMIN D AND 25(OH)D IN FOODS AND A DIETARY SUPPLEMENT USING LIQUID CHROMATOGRAPHY-MASS SPECTROMETRY

April 5, 2016
Author(s)
Janet M. Roseland, Kristine Y. Patterson, Karen Andrews, Katherine M. Phillips, Melissa M. Phillips, Pamela R. Pehrsson, Guy L. Dufresne, Pavel A. Gusev, Sushma Savarala, Quynhanh V. Nguyen, Andrew J. Makowski, Guillaume P. Larouche, Stephen Wise, J. Harnly, Juhi R. Williams, Joseph M. Betz, Christine Taylor
Assessment of total vitamin D intake from foods and dietary supplements (DSs) may be incomplete if 25-hydroxyvitamin D [25(OH)D] intake is not included. However, 25(OH)D data for such intake assessments are lacking, no food or DS reference materials (RMs)

Identification and Quantification of Seven Fused Aromatic Rings C26H14 Peri-Condensed Benzenoid Polycyclic Aromatic Hydrocarbons in a Complex Mixture of Polycyclic Aromatic Hydrocarbons from Coal Tar

March 2, 2016
Author(s)
Jorge O. Ona Ruales, Ruiz-Morales Yosadara, Stephen A. Wise
A methodology for the characterization of groups of PAHs using a combination of Normal Phase Liquid Chromatography with Ultraviolet-Visible Spectroscopy (NPLC/UV-vis) and Gas Chromatography with Mass Spectrometry (GC/MS) was used for the identification and

Determination of high-molecular weight polycyclic aromatic hydrocarbons in high performance liquid chromatography fractions of coal tar standard reference material 1597a via solid-phase nanoextraction and laser-excited time-resolved Shpol’skii spectr

November 10, 2015
Author(s)
Walter B. Wilson, Bassam Alfarhani, Cristina Bisson, Stephen A. Wise, Andres Campiglia
This article presents an alternative approach for the analysis of high molecular weight – polycyclic aromatic hydrocarbons (HMW-PAHs) with molecular mass 302 Da in complex environmental samples. This is not a trivial task due to the large number of

Identification and Quantification of Six-Ring C26H16 Cata-Condensed Polycyclic Aromatic Hydrocarbons in a Complex Mixture of Polycyclic Aromatic Hydrocarbons from Coal Tar

October 8, 2015
Author(s)
Jorge O. Ona Ruales, Arun K. Sharma, Stephen A. Wise
We applied a combination of normal-phase liquid chromatography (NPLC) with ultraviolet-visible spectroscopy and gas chromatography with mass spectrometry (GC/MS) for the fractionation, identification, and quantification of six ring cata-condensed C26H16

Development of Urine Standard Reference Materials for Metabolites of Organic Chemicals Including Polycyclic Aromatic Hydrocarbons, Phthalates, Phenols, Parabens, and Volatile Organic Compounds

April 1, 2015
Author(s)
Michele M. Schantz, Bruce A. Benner Jr., Nathanael A. Heckert, Lane C. Sander, Katherine E. Sharpless, Stacy S. Schuur, Stephen A. Wise
Two new Standard Reference Materials (SRMs), SRM 3672 Organic Contaminants in Smokers’ Urine (Frozen) and SRM 3673 Organic Contaminants in Non-Smokers’ Urine (Frozen), have been developed in support of studies for assessment of human exposure to select

Certification of Elements in and Use of Standard Reference Material 3280 Multivitamin/Multielement Tablets

December 2, 2013
Author(s)
Gregory C. Turk, Katherine E. Sharpless, Steven J. Christopher, Danielle Cleveland, Russell D. Day, Stephen E. Long, Elizabeth A. Mackey, Anthony F. Marlow, Rick L. Paul, John R. Sieber, Rabia Oflaz, Laura J. Wood, Lee L. Yu, Rolf L. Zeisler, Stephen A. Wise, James H. Yen, E. Greene, J. Harnly, I-P Ho, Joseph M. Betz, R. Q. Thompson, Candace Jongsma
Standard Reference Material (SRM) 3280 Multivitamin/Multielement Tablets was issued by the National Institute of Standards and Technology (NIST) in 2009 and has certified and reference mass fraction values for 13 vitamins, 26 elements, and 2 carotenoids

Development of a Standard Reference Material for Metabolomics Research

November 4, 2013
Author(s)
Karen W. Phinney, Guillaume Ballihaut, Mary Bedner, Johanna Camara, Steven J. Christopher, William C. Davis, Nathan G. Dodder, Brian E. Lang, Stephen E. Long, Mark S. Lowenthal, Elizabeth A. McGaw, Karen E. Murphy, Bryant C. Nelson, Jocelyn L. Prendergast, Jessica L. Reiner, Catherine A. Rimmer, Lane C. Sander, Michele M. Schantz, Katherine E. Sharpless, Lorna T. Sniegoski, Susan S. Tai, Jeanice M. Brown Thomas, Thomas W. Vetter, Michael J. Welch, Stephen A. Wise, Laura J. Wood, William F. Guthrie, Robert C. Hagwood, Stefan D. Leigh, James H. Yen, Nien F. Zhang, Madhu Chaurhary-Webb, Huiping Chen, Bridgette Haynes, Donna J. LaVoie, Leslie F. McCoy, Shahzad S. Momin, Neelima Paladugula, Elizabeth C. Pendergrast, Christine M. Pfeiffer, Carissa D. Powers, Zia Fazili-Qari, Daniel Rabinowitz, Michael E. Rybak, Rosemary L. Schleicher, Mary Xu, Mindy Zhang, Arthur L. Castle, Brandi S. Benford, Gauthier Eppe