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Displaying 1 - 25 of 98

ASTM E2677: Web-based International Standard on Limit of Detection for Explosive Trace Detectors (and More) - Opioids and Ozone

February 12, 2019
Author(s)
R M. Verkouteren, Nathanael A. Heckert, Stefan D. Leigh, Edward R. Sisco, James E. Norris, Jeffrey A. Lawrence, Amber Burns
The performance characteristics of explosive and narcotic trace detectors are mission-critical to agencies worldwide that are charged with protection of the public, defense for mass transit and infrastructure, and the safety of first responders. Commercial

Characterization of Chemical Properties, Unit Cell Parameters and Particle Size Distribution of Three Zeolite Reference Materials: RM 8850 - Zeolite Y, RM 8851 - Linde Type A Zeolite and RM 8852 - Ammonium ZSM-5 Zeolite

April 4, 2017
Author(s)
Shirley Turner, Robert A. Fletcher, Eric S. Windsor, Jennifer R. Verkouteren, John R. Sieber, Thomas W. Vetter, Rolf L. Zeisler, Anthony F. Marlow, M E. Davis, G J. Kennedy, W S. Borghard, S Yang, A Navrotsky, B H. Toby, James F. Kelly, Stefan D. Leigh
Zeolites have important industrial applications including use as catalysts, molecular sieves and ion exchange materials. In this study, three zeolite materials have been characterized by the National Institute of Standards and Technology (NIST) as

Relationship Between Quantitative Dispersion and Physical Properties of PMMA/SWNT Nanocomposites

February 19, 2017
Author(s)
Takashi Kashiwagi, Jeffrey Fagan, Keith Yamamoto, A N. Heckert, Stefan D. Leigh, Jan Obrzut, F Du, Sheng Lin-Gibson, Minfang Mu, K Winey, R Haggenmueller, Jack F. Douglas
Six PMMA/SWNT(0.5 wt%) nanocomposite samples intended to have different dispersion levels were prepared by the coagulation method using six different concentrations of SWNTs in DMF from 0.05 mg/ml to 1.2 mg/ml. The morphology of the samples was determined

Development of Two Fine Particulate Matter Standard Reference Materials (

April 13, 2016
Author(s)
Michele M. Schantz, Danielle Cleveland, N. Alan Heckert, John Kucklick, Stefan D. Leigh, Stephen E. Long, Jennifer Lynch, Karen E. Murphy, Rabia Oflaz, Adam L. Pintar, Barbara J. Porter, Savelas A. Rabb, Stacy Schuur, Stephen Wise, Rolf L. Zeisler
Two new Standard Reference Materials (SRMs), SRM 2786 Fine Particulate Matter (

The Occurrence of Repeated Fiber Breaks in Microcomposites

November 10, 2015
Author(s)
Gale A. Holmes, Edward D. McCarthy, Nathanael A. Heckert, Stefan D. Leigh, Jae Hyun Kim, Jeffrey W. Gilman
The mechanical integrity of a structural composite is strongly affected by the strength and toughness of the fiber–matrix interface/interphase (Norwood, 1994), with interfacial shear strength (IFSS) considered the best quantifying metric. IFSS outputs are

The Fiber Break Evolution Process in a 2-D Epoxy/Glass Multi-Fiber Array

November 2, 2015
Author(s)
Edward D. McCarthy, Jae H. Kim, N. Alan Heckert, Stefan D. Leigh, Jeffrey W. Gilman, Gale A. Holmes
The mechanical integrity of a structural composite is strongly affected by the strength and toughness of the fiber-matrix interface/interphase [1], with interfacial shear strength (IFSS) being the accepted quanti-fying metric. However, the value of the

Development of a Standard Reference Material for Metabolomics Research

November 4, 2013
Author(s)
Karen W. Phinney, Guillaume Ballihaut, Mary Bedner, Johanna Camara, Steven J. Christopher, William C. Davis, Nathan G. Dodder, Brian E. Lang, Stephen E. Long, Mark S. Lowenthal, Elizabeth A. McGaw, Karen E. Murphy, Bryant C. Nelson, Jocelyn L. Prendergast, Jessica L. Reiner, Catherine A. Rimmer, Lane C. Sander, Michele M. Schantz, Katherine E. Sharpless, Lorna T. Sniegoski, Susan S. Tai, Jeanice M. Brown Thomas, Thomas W. Vetter, Michael J. Welch, Stephen A. Wise, Laura J. Wood, William F. Guthrie, Robert C. Hagwood, Stefan D. Leigh, James H. Yen, Nien F. Zhang, Madhu Chaurhary-Webb, Huiping Chen, Bridgette Haynes, Donna J. LaVoie, Leslie F. McCoy, Shahzad S. Momin, Neelima Paladugula, Elizabeth C. Pendergrast, Christine M. Pfeiffer, Carissa D. Powers, Zia Fazili-Qari, Daniel Rabinowitz, Michael E. Rybak, Rosemary L. Schleicher, Mary Xu, Mindy Zhang, Arthur L. Castle, Brandi S. Benford, Gauthier Eppe

Toward the Development of a High Strain Rate Testing Standard for Advanced Fibers

May 24, 2013
Author(s)
Gale A. Holmes, Jae Hyun Kim, Nathanael A. Heckert, Walter G. McDonough, Stefan D. Leigh, Kirk D. Rice
The use of advanced fibers in applications where they are subjected to extremely energetic events has necessitated the need to develop measurement tools that quantify their properties at high strain rates (HSR). The split Hopkinson tension bar (SHTB) has

An Interlaboratory Investigation of the Effect of Material Granularity and Sample Processing on Measurement Variability: Nutritional Elements in Cereals

May 9, 2013
Author(s)
Katrice A. Lippa, Laura J. Wood, Stefan D. Leigh, Nathanael A. Heckert
This interlaboratory study was uniquely designed to determine the effects of material granularity and sample processing techniques on the measurement variability (i.e. precision) of nutritional elements in various cereal materials. Participants were asked

MILK AND SERUM SRMs for MONITORING ORGANIC CONTAMINANTS IN HUMAN SAMPLES

April 24, 2013
Author(s)
Michele M. Schantz, Katherine E. Sharpless, Stephen A. Wise, Rebecca Heltsley, Jennifer Keller, John Kucklick, Stacy VanderPol, Stefan D. Leigh, Donald G. Patterson, Jr., Andreas Sjodon, Wayman E. Turner
Four new Standard Reference Materials (SRMs) have been developed to assist in the quality assurance required for human biomonitoring studies. These materials are SRM 1953 Organic Contaminants in Non-Fortified Human Milk, SRM 1954 Organic Contamiants in

Effects of fiber gripping methods on the single fiber tensile test: I. Non parametric statistical analysis

February 15, 2013
Author(s)
Jae Hyun Kim, Nathanael A. Heckert, Stefan D. Leigh, Haruki Kobayashi, Walter G. McDonough, Kirk D. Rice, Gale A. Holmes
Single fiber tensile tests using two different gripping methods were carried out on various fiber lengths. One method (the glue-tab grip) consists of mounting a fiber onto a rigid tab as specified in ASTM C1557-03 using an adhesive, while the other (the

Breakfast Cereal Sampling Study for Nutritional Elements

February 5, 2013
Author(s)
Laura J. Wood, Katrice A. Lippa, Melissa M. Phillips, Catherine A. Rimmer, Nathanael A. Heckert, Stefan D. Leigh, Amanda J. Moors, Rebecca S. Pugh
The National Institute of Standards and Technology (NIST) has established a Dietary Supplement Laboratory Quality Assurance Program (DSQAP) in collaboration with the National Institutes of Health Office of Dietary Supplements (NIH-ODS). The DSQAP designed

Certification of NIST SRM 2569 Lead Paint Films for Children's Products

October 15, 2012
Author(s)
John L. Molloy, John R. Sieber, Karen E. Murphy, Stephen E. Long, Stefan D. Leigh
SRM 2569 Lead Paint Films for Children’s Products is a new Standard Reference Material (SRM) developed for use primarily with XRF instrumentation. It consists of three paint coatings, with nominally 0 mg/kg, 90 mg/kg, and 300 mg/kg of Pb added, on

Tensile behavior of single PPTA fibers measured by the Kolsky bar using the direct fiber clamping method

June 11, 2012
Author(s)
Jae Hyun Kim, Nathanael A. Heckert, Stefan D. Leigh, Haruki Kobayashi, Walter G. McDonough, Richard L. Rhorer, Kirk D. Rice, Gale A. Holmes
The Kolsky bar test has been widely used in measuring material behavior under high strain rate conditions. In particular, this methodology has been used to characterize the high strain rate behavior of polymer and polymer composites during ballistic impact