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Leonid A. Bendersky, Ke Wang, William J. Boettinger, Dale E. Newbury, K. Young, B. Chao
Multi-component Zr-Ti-Ni-TM (TM=V, Cr, Mn and Co) cast alloys intended for use as negative electrodes in Ni metal hydride batteries were studied to determine the solidification microstructure and solidification path in the Part I of this paper. Part II of
William J. Boettinger, Dale E. Newbury, Ke Wang, Leonid A. Bendersky, Chun Chiu, Ursula R. Kattner, K. Young, B. Chao
The solidification microstructure of a nine-element Zr-Ni based AB(sub 2) type C14/C15 Laves hydrogen storage alloy is determined. The selected composition represents a class of alloys being examined for usage as a metal hydride electrode in nickel metal
Most nanoparticle syntheses, including those based on the Brust-Schiffrin method, produce a mixture of different metal core sizes. This report presents a new strategy for controlling the size and dispersity of ultra-small nanoclusters through selection of
Julie N. Albert, Michael J. Baney, Christopher Stafford, Jennifer Y. Kelly, Thomas H. Epps
Development of self-assembling block copolymer materials for emerging nanotechnologies requires an understanding of how surface energy and chemistry affect thin film phase behavior. Gradient methods provide an effective route to explore the role of surface
Gale A. Holmes, Walter G. McDonough, Jae H. Kim, Derek L. Ho
Failures of certified soft body armor led to a call to understand the underlying mechanisms of the failure. Research has indicated that the folding of ballistic fibers comprising the soft body armor may be a factor in the performance deterioration that has
Katie Hurst, Abram Van Der Geest, Mark T. Lusk, Elisabeth Mansfield, John H. Lehman
Photochemical changes of single-walled carbon nanotubes (SWCNTs), graphite and amorphous carbon have been investigated with a quartz crystal microbalance (QCM). The method of in-situ measurements reduces our uncertainty that is attributable to
David R. Black, Donald A. Windover, Albert Henins, James J. Filliben, James P. Cline
The National Institute of Standards and Technology (NIST) certifies a suite of Standard Reference Materials (SRMs) to address specific aspects of instrument performance of powder diffractometers. This report describes SRM 660b, the third generation of this
Jessica M. Torres, Christopher Stafford, Bryan D. Vogt
Euler wrinkling was used to determine the elastic modulus at ambient temperature of polystyrene (PS) films of varying thickness and relative molecular mass (Mn). A range of Mn from 1.2 kg/mol to 990 kg/mol was examined to determine if the molecular size
Diffusion-controlled dissolution and precipitation reactions occur in many biological systems and some non-stirred in vitro systems. Previous studies have shown that differences in the diffusion rates of ions involved in a dissolution/precipitation
Statistical analyses of companion Bogue (ASTM C150) and quantitative X-ray powder diffraction (QXRD) estimates for cement phases are used to establish the most likely linear relationship between these two measurement techniques for alite, belite, aluminate
Hiroyoshi Momida, Eric J. Cockayne, Naoto Umezawa, Takahisa Ohno
First-principles calculations were used to compute the dielectric permittivities of hypothetical [La,Sc]2O3 solid solutions in the cubic (bixbyite) and hexagonal La2O3 phases. Dielectric enhancement is predicted at small Sc concentrations due to the
Polymer coatings are dependent on strongly bonded buried interfaces to maintain adhesion and protective properties over long application lifetimes. In this work, we detail the detection of buried interfaces with deviations from perfect bonded or perfect
James R. Baker-Jarvis, Sung Kim, Luke Leschallinger, Justin Johnson, Brad Givot
The purpose of this report is to summarize the characterization of a number of high-frequency solid, liquid, and semisolid tissue-equivalent materials, from 200 MHz to 20 GHz. Carbon black and liquid mixtures were studied, but were found to be unsuitable
Kaushik Chatterjee, Sheng Lin-Gibson, William E. Wallace, Marian F. Young, Carl Simon Jr.
A combinatorial library approach was used to demonstrate that hydrogel scaffold modulus can enhance osteoblast differentiation driving formation of a 3-D graded tissue construct. Though many previous studies have focused on screening cell-material
Kil-Won Moon, S. -. Kim, Maureen E. Williams, William J. Boettinger, Gery R. Stafford
The effect of current density and Sn methane sulfonate concentration on hillock density, columnar grain size, crystallographic texture, and residual stress of bright Sn electrodeposits is measured. Correlation was found between hillock density and the
Daniel Wheeler, James A. Warren, William J. Boettinger
Recent experimental studies of molten metal droplets wetting and spreading on high temperature reactive substrates have established that the majority of triple-line motion occurs when inertial effects are dominant. In light of these studies, this paper
A model of hydride formation and dissolution has been proposed for a single spherical nano-particle and for a colletion of such particles with a given size distribution. The phase transformation strain gives rise to an elastic barrier of the transformation
Francesca M. Tavazza, Lyle E. Levine, Anne M. Chaka
Under tensile deformation, Au nanowires (NWs) elongate to form single atom chains via a series of intermediate structural transformations. These intermediate structures are investigated using semistatic density functional theory (DFT), with particular
Derek D. Hass, H. Zhao, Tabbetha A. Dobbins, Andrew J. Allen, Andrew Slifka, H. N. Wadley
A high pressure, electron-beam directed-vapor deposition process has been used to deposit partially stabilized zirconia containing 7 % yttria by mass at deposition pressures of 7.5 Pa to 23 Pa. Anisotropic ultra-small-angle X-ray scattering (USAXS) was
Paul Constantino, James J. Lee, H Chai, Bernhard Zipfel, Charles Ziscovici, Brian R. Lawn, Peter Lucas
Fossil hominin tooth enamel often exhibits antemortem edge chipping (Robinson 1954; Tobias 1967; Wallace 1973). Here we apply a simple fracture equation to estimate peak bite forces from the sizes of such chips. This equation, previously validated by
Xiaohong Gu, Guodong Chen, Minhua Zhao, Stephanie S. Watson, Paul E. Stutzman, Tinh Nguyen, Joannie W. Chin, Jonathan W. Martin
The objective of this study is to investigate the role of ZnO nanoparticles in the life cycle of a waterborne polyurethane (PU) nanocomposite during UV exposure. The effects of loadings and sizes of ZnO nanoparticles on photodegradation of ZnO/PU films
The micromechanics community has developed a large set of tools for measuring the properties of micro- and nano-scaled materials. These new tools have been successfully applied to a range of materials, most often in thin-film form, to determine the
The development of high fidelity simulations of lead-cored bullet impacts on soft body armor, motivated by the need for improved armor designs and performance standards for law enforcement, requires accurate models for both the armor and the deformable