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Compounds of interest and their availability as well as purity of the samples in the market are discussed. Difficulties in acquiring samples of common chemicals are noted. Sample preparation procedures for GC-MS analysis along with the instrumental
John G. Gillen, Scott A. Wight, Joe Bennett, Michael J. Tarlov
Decanethiol [CH3(CH2)9SH] self-assembled monolayer films on silver substrates have been irradiated in selected areas by focused ion or electron bombardment. Subsequent immersion of the irradiated sample in a solution of a fluoromercaptan [CF3(CF2)2(CH2)2SH
Requirements to reference spectra and criteria for mass spectrum inclusion, modification and deletion are developed as a result of evaluation of thousands of spectra and analysis of encountered errors. Errors due to a sample, device and operator, data
John G. Gillen, J. Bennett, Michael J. Tarlov, Donald R. Burgess Jr.
Self-assembly of alkanethiol monolayers on gold and silver substrates is a fast, easy, and convenient method for preparing stable organic films with well-defined physical and chemical properties that can be modified by changing the terminal functional
Computer generated "Quality Index" for the selection of spectra for the inclusion to the NIST/EPA/NIH mass spectral library is abandoned. We have undertaken a program to manually examine all spectra in the database. Suspect spectra are first examined to
Robert Gregory Downing, Cynthia J. Zeissler, Heather H. Chen-Mayer
A charge injection device (CID) camera and image processing system have been used as a position sensitive detector for energetic charged particles and low energy neutrons. This video radiation detector (VRD) is simple in design but highly effective for
J Lewtas, L.D. Claxton, H.S. Rosenkranz, D. Schuetzle, M. Shelby, H. Matsushita, F.E. Wurgler, G. Lofroth, Willie E. May, D. Krewski, T. Matsushima, Y. Ohnishi, H.N. Gopalan, R. Sarin, G.C. Becking