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Search Publications by: Antonio Possolo (Fed)

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Displaying 1 - 25 of 56

Certification of Standard Reference Material(R) 1595a Tripalmitin

March 1, 2024
Author(s)
Michael Nelson, Jerome Mulloor, Brian Lang, Blaza Toman, Antonio Possolo, William Perry, Alicia Lyle
Standard Reference Material (SRM) 1595a Tripalmitin is a high purity chemical substance having a certified value for purity, expressed as a mass fraction. It is intended for use in preparing calibrants for measurement of total glyceride in clinical samples

Errors-in-variables calibration with dark uncertainty

June 16, 2022
Author(s)
Christina Cecelski, Blaza Toman, Fong-Ha Liu, Juris Meija, Antonio Possolo
A model for errors-in-variables regression is described that can be used to overcome the challenge posed by mutually inconsistent calibration data. The model and its implementation are illustrated in applications to the measurement of the amount fraction

International comparison CCQM-K10.2018: BTEX in nitrogen at 5 nmol mol-1

February 18, 2022
Author(s)
Christina Cecelski, George C. Rhoderick, Antonio Possolo, Jennifer Carney, Miroslav Vokoun, Jitka Privoznikova, Sangil Lee, Ji Hwan Kang, Yong Doo Kim, Dal Ho Kim, Tatiana Mace, Christophe Sutour, Celine Pascale, Napo Ntsasa, James Tshilongo, Mudalo Jozela, Nompumelelo Leshabane, Goitsemang Lekoto, David Worton, Paul Brewer, Fred Farrow-Dunn, Sergi Moreno, Klaus Wirtz, Volker Stummer, L.A. Konopelko, A.V. Kolobova, Y.A. Kustikov, A.Y. Klimov, O.V. Efremova, Janneke van Wijk, Adriaan van der Veen
The CCQM-K10.2018 comparison aimed to evaluate the capabilities of national metrology institutes (NMIs) to prepare and/or value assign primary reference mixtures containing benzene, toluene, ethylbenzene, p-xylene, m-xylene and o-xylene (subsequently

Pilot Comparison CCQM-P177 - Monoterpenes in Nitrogen at 2.5 nmol mol-1 Final Report

September 27, 2021
Author(s)
Christina Cecelski, George C. Rhoderick, Joseph T. Hodges, Antonio Possolo, Olaf Wilke
The growing awareness of climate change, and continuing concerns regarding tropospheric and stratospheric chemistry, will require future measurements and standards for compounds linked to these issues. To globally monitor and control the emissions of these

Metrological Tools for the Reference Materials and Reference Instruments of the NIST Material Measurement Laboratory

September 16, 2021
Author(s)
Carlos R. Beauchamp, Johanna Camara, Jennifer Carney, Steven J. Choquette, Kenneth D. Cole, Paul C. DeRose, David L. Duewer, Michael Epstein, Margaret Kline, Katrice Lippa, Enrico Lucon, John L. Molloy, Michael Nelson, Karen W. Phinney, Maria Polakoski, Antonio Possolo, Lane C. Sander, John E. Schiel, Katherine E. Sharpless, Michael R. Winchester, Donald Windover
The National Institute of Standards and Technology (NIST), formerly the National Bureau of Standards, was established by the U.S. Congress in 1901 and charged with establishing a measurement foundation to facilitate U.S. and international commerce. NIST

Metrological Traceability Frequently Asked Questions and NIST Policy

May 6, 2021
Author(s)
Sally Bruce, Antonio Possolo, Robert Watters
The NIST policy on metrological traceability (NIST P 5800.00, which became effective on May 31st, 2019) is transcribed and supplemented with a review of relevant terminology and with a list of frequently asked questions and answers. This list updates and

Decision Tree for Key Comparisons

April 27, 2021
Author(s)
Antonio Possolo, Amanda Koepke, David Newton, Michael R. Winchester
This contribution describes a Decision Tree intended to guide the selection of statistical models and data reduction procedures in key comparisons (KCs). The Decision Tree addresses a specific need of the Inorganic Analysis Working Group (IAWG) of the

Metrological Tools for the Reference Materials and Reference Instruments of the NIST Material Measurement Laboratory

July 15, 2020
Author(s)
Carlos R. Beauchamp, Johanna Camara, Jennifer Carney, Steven J. Choquette, Kenneth D. Cole, Paul C. DeRose, David L. Duewer, Michael Epstein, Margaret C. Kline, Katrice Lippa, Enrico Lucon, Karen W. Phinney, Maria Polakoski, Antonio Possolo, Katherine E. Sharpless, John R. Sieber, Blaza Toman, Michael R. Winchester, Donald Windover
The National Institute of Standards and Technology (NIST), formerly the National Bureau of Standards, was established by the U.S. Congress in 1901 and charged with establishing a measurement foundation to facilitate U.S. and international commerce. NIST

Validation of Single Particle ICP-MS for Routine Measurements of Nanoparticle Size and Number Size Distribution

November 25, 2018
Author(s)
Antonio R. Montoro Bustos, Premsagar P. Kavuri, Antonio M. Possolo, Natalia Farkas, Andras Vladar, Karen E. Murphy, Michael R. Winchester
Single particle inductively coupled plasma-mass spectrometry (spICP-MS) is an emerging technique capable of measuring nanoparticle size and number concentration simultaneously, of metal-containing nanoparticles (NPs) at environmentally relevant levels

CCQM K121 – Monoterpenes in Nitrogen at 2.5 nmol mol-1 Final Report

November 9, 2018
Author(s)
Christina E. Cecelski, George C. Rhoderick, Joseph T. Hodges, Antonio M. Possolo, Cassie A. Goodman, Yong D. Kim, Dal H. Kim, Sangil Lee, Nicholas Allen, Marivon Corbel, David Worton, Richard Brown, Paul Brewer
The growing awareness of climate change, and continuing concerns regarding tropospheric and stratospheric chemistry, will require future measurements and standards for compounds linked to these issues. To monitor and control the emissions of these species

The Effects of Laser Powder Bed Fusion Process Parameters on Material Hardness and Density for Nickel Alloy 625

August 21, 2018
Author(s)
Christopher U. Brown, Gregor Jacob, Antonio M. Possolo, Carlos R. Beauchamp, Max A. Peltz, Mark R. Stoudt, M A. Donmez
The goal of this study was to investigate the relationship between mechanical and material properties (including density) of manufactured nickel super alloy (IN625) using a laser powder bed fusion process and three process parameters: laser power, hatch

How measurement science can improve confidence in research results

April 23, 2018
Author(s)
Anne L. Plant, Chandler A. Becker, Robert J. Hanisch, Ronald F. Boisvert, Antonio M. Possolo, John T. Elliott
The concepts and methods of measurement science can help provide clarity in the definition of reproducibility and its role in the scientific process. The qualities of rigorous research include reproducibility as one component, but there are other important

Measurement of the Planck constant at the National Institute of Standards and Technology from 2015 to 2017

July 28, 2017
Author(s)
Darine El Haddad, Frank Seifert, Leon Chao, Antonio Possolo, David B. Newell, Jon R. Pratt, Carl J. Williams, Stephan Schlamminger
Researchers at the National Institute of Standards and Technology(NIST) estimate the value of the Planck constant as h = 6.62606994(10) x 10^-34 Js, hence with relative standard uncertainty 15.3 x 10^-9. This measurement result is based on over 17,000

Value Assignment of Vitamin D Metabolites in Vitamin D Standardization Program (VDSP) Serum Samples

June 16, 2017
Author(s)
Karen W. Phinney, Johanna Camara, Susan Tai, Lane C. Sander, Stephen A. Wise, Linde A. De Grande, Linda M. Thienpont, Antonio M. Possolo, Blaza Toman, Christopher T. Sempos, J. M. Betz, Paul M. Coates
Assay variability has been cited as an obstacle to establishing optimal vitamin D exposure. As part of the Vitamin D Standardization Program (VDSP) effort to standardize the measurement of total 25(OH)D, value assignment of total 25(OH)D in 50 single donor

Standardizing CT Lung Density Measure Across Scanner Manufacturers

March 1, 2017
Author(s)
Huaiyu H. Chen-Mayer, Matthew Fuld, Bernice Hoppel, Phillip Judy, Junfeng Guo, David Lynch, Antonio M. Possolo, Sean B. Fain
Computed Tomography imaging of the lung, reported in Hounsfield Units (HU), can be parameterized as a quantitative image biomarker for the diagnosis and monitoring of lung density changes due to emphysema, a type of chronic obstructive pulmonary disease

Development of a Northern Continental Air Standard Reference Material

February 18, 2016
Author(s)
George C. Rhoderick, Duane Kitzis, Michael E. Kelley, Walter R. Miller Jr., Bradley Hall, Edward Dlugokencky, Pieter Tans, Antonio M. Possolo, Jennifer Carney
The National Institute of Standards and Technology (NIST) recently began to develop standard mixtures of greenhouse gases as part of a broad program mandated by the 2009 United States Congress to support research in climate change. To this end, NIST made

Additive Manufacturing Round Robin Protocols: A Pilot Study

August 12, 2015
Author(s)
Shawn P. Moylan, Joshua Land, Antonio M. Possolo
As the number of users of additive manufacturing (AM) steadily increases, and considering their demand for material and process specifications, the need for standard protocols for round robin studies is increasing accordingly. Researchers at the National