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Displaying 26 - 50 of 136

FTIR measurements of compositional heterogeneities

February 25, 2007
Author(s)
Shuhui Kang, B D. Vogt, Wen-Li Wu, Vivek Prabhu, David L. VanderHart, Ashwin Rao, Eric K. Lin, Karen Turnquest
A general approach to characterize compositional heterogeneity in polymer thin films using Fourier transform infrared (FTIR) spectroscopy has been demonstrated Polymer films with varying degrees of heterogeneity were prepared using a model chemically

Characterization of Compositional Heterogeneity in Chemically Amplified Photoresist Polymer Thin Films with Infrared Spectroscopy

February 9, 2007
Author(s)
Shuhui Kang, B D. Vogt, Vivek Prabhu, Eric K. Lin, Wen-Li Wu, David L. VanderHart, Ashwin Rao, Karen Turnquest
We demonstrate a general approach to characterize compositional heterogeneity in polymer thin films using Fourier transform infrared (FTIR) spectroscopy. Polymer films with varying degrees of heterogeneity were prepared using a model chemically amplified

Dielectric Study of the Anti-Plasticization of Trehalose by Glycerol

January 1, 2006
Author(s)
A Anopchenko, Tatiana Psurek, David L. VanderHart, Jack F. Douglas, Jan Obrzut
Recent measurements have suggested that the antiplasticizing effect of glycerol on trehalose can significantly increase the preservation times of proteins stored in this type of preservative formulation. In order to better understand the physical origin of

Matrix-Assisted Laser Desorption/Ionization Time-of-Flight Mass Spectrometry Interlaboratory Comparison of Mixtures of Polystyrene With Different End Groups: Statistical Analysis of Mass Fractions and Mass Moments

July 1, 2005
Author(s)
Charles M. Guttman, S Wetzel, Kathleen M. Flynn, B M. Fanconi, David L. VanderHart, William E. Wallace
A matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (MALDI-TOF MS) interlaboratory comparison was conducted on mixtures of synthetic polymers having the same repeat unit and closely matching molecular mass distributions but with

Effect of Tacticity on the Structure of Poly (1-Octadecene)

September 1, 2004
Author(s)
David L. VanderHart, E Perez, A Bello, G B. Vasquez, Manuel A. Quijada
A sample of poly(1-octadecene), synthesized with a highly active heterogeneous Ziegler-Natta catalyst, has been fractionated with n-heptane, giving soluble and insoluble fractions. Both fractions and the original polymer have been characterized by SEC

Proton NMR Determination of Miscibility in a Bulk Model Photoresist System Poly (4-Hydroxystyene) and the Photoacid Generator, Di(t-butylphenyl) Iodonium Perfluorooctane Sulfonate

July 13, 2004
Author(s)
David L. VanderHart, Vivek M. Prabhu, Eric K. Lin
The intimacy of component mixing in 2 blends of poly(4-hydroxystyrene) (PHS) and a photoacid generator (PAG), di(t-butylphenyl) iodonium perfluorooctane sulfonate (PFOS) were studied by solid state proton NMR. Mass ratios were 91/9 and 85/15 PHS/PFOS

Solid-Phase ATRP Synthesis of Peptide-Polymer Hybrids

March 1, 2004
Author(s)
Ying Mei, Kathryn L. Beers, H M. Byrd, David L. VanderHart, N. R. Washburn
A versatile methodology for preparing hybrid biomaterials by atom transfer radical polymerization from resin-supported peptides has been established. As an example, we have synthesized a GRGDS-functionalized poly(2-hydroxyethyl methacrylate). The peptide

International Interlaboratory Comparison of Mixtures of Polystyrenes With Different End Groups Obtained by Matrix Assisted Laser Desorption/Ionization Time-of-Flight Mass Spectrometry (MALDI-TOF-MS): Preliminary Results

January 1, 2004
Author(s)
Charles M. Guttman, S Wetzel, Kathleen M. Flynn, B M. Fanconi, William E. Wallace, David L. VanderHart
NIST has sponsored a MALDI-TOF-MS interlaboratory comparison of mixtures of polymers of the same repeat unit with closely matching molecular masses but with different end groups. This interlaboratory comparison was designed to see how well a group of labs
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