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Chemistry

Analytical chemistry

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Displaying 726 - 750 of 2094

Raman and Infrared spectra of the ?1 band of oxirane

May 14, 2015
Author(s)
Walter J. Lafferty, Jean-Marie Flaud, F. K. Kwabia Tchana
Fourier transform spectra of oxirane (ethylene oxide, c-C2H4O) have been recorded in the 3.17 μm - 3.5 μm region with a resolution of 0.005 cm-1. In addition, a Raman spectrum covering the same spectral region was recorded at a resolution of 0.44 cm-1

Thermal Analysis of Nanoparticles: Methods, Kinetics and Recent Advances

May 4, 2015
Author(s)
Elisabeth Mansfield
This chapter will provide an overview of the thermal techniques available to study nanoparticles, including thermogravimetric analysis, calorimetry and differential scanning calorimetry. The use of thermoanalysis for the measurement of nanoparticle purity

Chemically-Sensitive Bioimaging with Coherent Raman Scattering

April 29, 2015
Author(s)
Charles H. Camp, Marcus T. Cicerone
Raman scattering provides an intrinsic fingerprint of chemical composition. Spontaneous Raman spectroscopy has been used for many decades to interrogate biological materials and systems, but is not widely used for imaging due to relatively slow signal

Electron Spin Resonance Scanning Probe Spectroscopy for Ultra-Sensitive Biochemical Studies

April 22, 2015
Author(s)
Jason P. Campbell, Jason T. Ryan, Pragya R. Shrestha, Zhanglong Liu, Canute I. Vaz, Jihong Kim, Vasileia Georgiou, Kin P. Cheung
Electron spin resonance (ESR) spectroscopy’s affinity for detecting paramagnetic free radicals, or spins, has been increasingly employed to examine a large variety of biochemical interactions. Such paramagnetic species are broadly found in nature and can

Perfluorinated Alkyl Acids in Wildlife

April 21, 2015
Author(s)
Jessica L. Reiner, Benjamin J. Place
The first measurements of perfluorinated compounds (PFCs) in wildlife from the aqueous and terrestrial environment showed their ubiquitous presence. Since the initial studies in 2001 their presence, distribution, and fate in the environment has broadly

Direct correlation of charge transfer absorption with molecular donor:acceptor interfacial area via photothermal deflection spectroscopy

April 9, 2015
Author(s)
Lee J. Richter, Dean M. DeLongchamp, Natalie Stingelin, Alberto Salleo, Martin Heeney, Aram Amassian, John deMello, James Bannock, Fiona H. Scholes, Scott Watkins, Zhuping Fei, Koen Vandewal
ABSTRACT: Here, we show that the Charge Transfer (CT) absorption signal in bulk (BHJ) solar cell blends, measured by photothermal deflection spectroscopy (PDS), is directly proportional to the density of molecular donor/acceptor interfaces. Since the

Elemental characterization of Single-Wall Carbon Nanotube (SWCNT-1) reference material by neutron and prompt gamma activation analysis

April 7, 2015
Author(s)
Rick L. Paul, Rabia Oflaz, Jan Kucera, J W Bennett, E. A. De Nadai Fernandes, M. Kubesova, M. A. Bacchi, A. J. Stopic, R. E. Sturgeon, P. Grinberg
Instrumental neutron activation analysis with both relative and k0 standardization was used in four experienced laboratories to determine element mass fractions in single-wall carbon nanotube certified reference material (CRM) SWCNT-1. Results obtained

Frequency-agile, rapid scanning cavity ring-down spectroscopy (FARS-CRDS) measurements of the (30012) --(00001) near-infrared carbon dioxide band

April 3, 2015
Author(s)
David A. Long, Szymon S. Wojtewicz, Charles E. Miller, Joseph T. Hodges
We present new high accuracy measurements of the (30012)←(00001) CO¬2 band near 1575 nm recorded with a frequency-agile, rapid scanning cavity ring-down spectrometer. The resulting spectra were fit with the partially correlated, quadratic-speed-dependent

Development of Urine Standard Reference Materials for Metabolites of Organic Chemicals Including Polycyclic Aromatic Hydrocarbons, Phthalates, Phenols, Parabens, and Volatile Organic Compounds

April 1, 2015
Author(s)
Michele M. Schantz, Bruce A. Benner Jr., Nathanael A. Heckert, Lane C. Sander, Katherine E. Sharpless, Stacy S. Schuur, Stephen A. Wise
Two new Standard Reference Materials (SRMs), SRM 3672 Organic Contaminants in Smokers’ Urine (Frozen) and SRM 3673 Organic Contaminants in Non-Smokers’ Urine (Frozen), have been developed in support of studies for assessment of human exposure to select

NGD Cold Neutron Prompt Gamma-ray Activation Analysis Spectrometer at NIST

April 1, 2015
Author(s)
Rick L. Paul, Dagistan NMN Sahin, Jeremy C. Cook, Christoph W. Brocker, Richard M. Lindstrom, Donna J. O'Kelly
A new instrument for cold neutron prompt gamma-ray activation analysis (CNPGAA) has been designed and constructed as part of the recent expansion of the cold neutron guide hall at the NIST Center for Neutron Research (NCNR). Located on neutron guide NGD

"Weighing" a Gas With Microwave and Acoustic Resonances

March 24, 2015
Author(s)
Keith A. Gillis, James B. Mehl, James W. Schmidt, Michael R. Moldover
With calibrations of large flow meters in mind, we established the feasibility of determining the mass Mof argon gas contained within a 0.3 m 3 commercially manufactured pressure vessel ("tank") with a relative uncertainty of u r(M) = 0.0015 at 0.6 MPa by

An approach for identification and determination of arsenic species in the extract of kelp

March 3, 2015
Author(s)
Lee L. Yu, Rolf L. Zeisler, Rabia Oflaz, Wei Chao, Junting Tong, Haixia Bao, Jun Wang
The National Institute of Standards and Technology is developing a kelp standard reference material (SRM) in support of dietary supplement measurements. Edible seaweeds such as kelp and laver consumed as diet or dietary supplement contain tens of mg/kg

High resolution analysis of the nu1 and nu5 bands of phosgene 35Cl2CO and 35Cl37ClCO

March 2, 2015
Author(s)
Walter J. Lafferty, Jean-Marie Flaud, F. Kwabia Tchana, L. Manceron
Fourier transform spectra of phosgene (Cl2CO) have been recorded in the 11.75 μm and 5.47 μm spectral regions using a Bruker IFS125HR spectrometer at resolutions of 0.00102 cm-1 and 0.0015 cm-1 respectively leading to the observation of the ν5 and ν1

The NIST Traceable Reference Material Program for Gas Standards

February 26, 2015
Author(s)
William D. Dorko, Michael E. Kelley, Franklin R. Guenther
A program is described by which the concentration of commercially produced gas mixtures may be related to gaseous primary standards or measurement systems maintained by the National Institute of Standards and Technology (NIST). The gaseous mixtures
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