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Displaying 26 - 50 of 1814

Fabrication of Specimens for Atom Probe Tomography using a Combined Gallium and Neon Focused Ion Beam Milling Approach

August 16, 2023
Author(s)
Frances Allen, Paul Blanchard, David Pappas, Russell Lake, Deying Xia, John Notte, Ruopeng Zhang, Andrew Minor, Norman A. Sanford
We demonstrate a new focused ion beam sample preparation method for atom probe tomography. The key aspect of the new method is that we use a neon ion beam for the final tip shaping after conventional annulus milling using gallium ions. This dual-ion

Recommendations for Setting a Criterion for Assessing Commutability of Secondary Calibrator Certified Reference Materials

August 11, 2023
Author(s)
W. Greg Miller, Thomas Keller, Jeffrey Budd, Jesper Johansen, Mauro Panteghini, Neil Greenberg, Vincent Delatour, Ferruccio Ceriotti, Robert Rej, Johanna Camara, Liesbet Deprez, Finlay MacKenzie, Alicia Lyle, Eline van der Hagen, Chris Burns, Pernille Fauskanger, Sverre Sandberg
A secondary higher-order calibrator is required to be commutable with clinical samples to be suitable for use in the calibration hierarchy of an end-user clinical laboratory in vitro diagnostic medical device (IVD-MD). Commutability is a property of a

Operando photoelectron spectromicroscopy of nanodevices: Correlating the surface chemistry and transport in SnO2 nanowire chemiresistors

June 29, 2023
Author(s)
Andrei Kolmakov, Trey Diulus, Kurt D. Benkstein, Stephen Semancik, Majid Kazemian, Matteo Amati, Maya Kiskinova, Luca Gregoratti
With size reduction of active elements in microelectronics to tens of nanometers and below, the effect of surface and interface properties on overall device performance becomes crucial. High resolution spectroscopic and imaging techniques provide a

Detailed analysis of the synthesis and structure of MAX phase (Mo0.75V0.25)5AlC4 and its MXene (Mo0.75V0.25)5C4

June 27, 2023
Author(s)
Rose Snyder, Mikkel Juelsholt, Curran Kalha, Jason Holm, Elisabeth Mansfield, Tien-Lin Lee, Pardeep Thakur, Aysha Riaz, Benjamin Moss, Anna Regoutz, Christina Birkel
MAX phases with the general formula Mn+1AXn are layered carbides, nitrides and carbonitrides with varying stacking sequence of layers of M6X octahedra and the A-element depending on n. While "211" MAX phases (n = 1) are very common, MAX phases with higher

Reference Isotherms for Water Vapor Sorption on Nanoporous Carbon: Results of an Interlaboratory Study

May 26, 2023
Author(s)
Huong Giang Nguyen, Blaza Toman, Roger D. van Zee, Carsten Prinz, Matthias Thommes, Riaz Ahmad, David Kiska, Jamie Salinger, Ian Walton, Krista Walton, Darren Broom, Mike Benham, Humera Ansari, Ronny Pini, Camille Petit, Jurgen Adolphs, Andreas Schreiber, Toshihiro Shigeoka, Yuko Konishi, Kazuyuki Nakai, Matthias Henninger, Thomas Petrzik, Can Kececi, Vladimir Martis, Thomas Pasche, Enzo Mangano, Stefano Brandani

Determination of 24,25-dihydroxyvitamin D3 in Vitamin D External Quality Assessment Scheme samples using a reference measurement procedure

May 9, 2023
Author(s)
Stephen Wise, Grace Hahm, Carolyn Burdette, Susan Tai, Johanna Camara, Adam Kuszak, Emma Williams
Ninety archived human serum samples from the Vitamin D External Quality Assessment Scheme (DEQAS) were analyzed using a reference measurement procedure (RMP) based on isotope dilution liquid chromatography - tandem mass spectrometry (ID LC-MS/MS) for the

Phosphate-Functionalized MOF-808 for High Performance Li-S Batteries

May 8, 2023
Author(s)
Bingqian Liu, Avery Baumann, Megan Butala, V. Sara Thoi
Lithium–sulfur batteries are promising candidates for next-generation energy storage devices due to their outstanding theoretical energy density. However, they suffer from low sulfur utilization and poor cyclability, greatly limiting their practical

Size-exclusion chromatography

April 20, 2023
Author(s)
Andre Striegel
Over the past half-century, size-exclusion chromatography (SEC) has become the premier method by which to determine the molar mass (M) averages and the molar mass distribution (MMD) of natural and synthetic macromolecules. When coupled to a multiplicity of

A Multivariate Flexible Framework with High Usable Hydrogen Capacity in a Reduced Pressure Swing Process

April 12, 2023
Author(s)
Craig Brown, Gavin McCarver, Arijit Halder, Sarah Shulda, Philip Parilla, Hiroyasu Furukawa, C. Michael McGuirk
Step-shaped adsorption¬–desorption of gaseous payloads by a flexible metal–organic framework can facilitate the delivery of large usable capaci-ties with significantly reduced energetic penalties. This is desirable for the storage, transport, and delivery

Salts as additives: A route to improve performance and stability of n-type organic electrochemical transistors

March 9, 2023
Author(s)
David Ohayon, Lucas Flagg, Andrea Giugni, Shofarul Wustoni, Ruipeng Li, Tania Hidalgo, Abdul Hamid Emwas, Rajendar Sheelamanthula, Iain McCulloch, Lee J. Richter, Sahika Inal
Organic electrochemical transistors (OECTs) are becoming increasingly ubiquitous in a wide variety of applications at the interface with biological systems, including biosensing, neuromorphic computing, and logic circuits. The widespread use of these
Displaying 26 - 50 of 1814